Porous carbon material with high specific surface area prepared by virtue of fungal pretreatment as well as method and application thereof

A high specific surface area, porous carbon technology, applied in the field of porous carbon materials, can solve the problems of complex process conditions, secondary pollution and high cost, and achieve the effects of simple process, no secondary pollution and low production cost

Pending Publication Date: 2019-04-05
SOUTH CHINA UNIV OF TECH
View PDF4 Cites 11 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The method of the present invention is simple, and can effectively solve the problems of complex process conditions, high cost, and secondary pollution in the preparation method

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Porous carbon material with high specific surface area prepared by virtue of fungal pretreatment as well as method and application thereof
  • Porous carbon material with high specific surface area prepared by virtue of fungal pretreatment as well as method and application thereof
  • Porous carbon material with high specific surface area prepared by virtue of fungal pretreatment as well as method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0035] Example 1

[0036] The method for preparing microporous high specific surface area porous carbon by treating cellulose degrading bacteria includes the following steps:

[0037] (1) Dilute the lyophilized Trichodermaviride powder by 10000 times with sterilized deionized water, pipette 0.2 mL of the dissolved dry powder bacteria liquid and inoculate it on the solid potato medium, spread it evenly, and put it in the culture Incubate at 30°C for 6 days; then drip sterile deionized water into the cultured plate, stir gently with an inoculation needle, and filter with gauze to obtain a T.viride spore suspension, which is sealed and stored in a refrigerator at 6°C for later use ;

[0038] (2) The lotus leaf biomass is washed, dried at 90°C, and cut into fragments of 0.5-1.5 cm to obtain pretreated raw materials;

[0039] (3) Take 200g of peeled potatoes, wash and cut into small pieces, add 1L of deionized water and boil for 30min to obtain the filtrate; make up the filtrate to 1L, th...

Example Embodiment

[0044] Example 2

[0045] The method for preparing mesoporous porous carbon with high specific surface area by treating lignin degrading bacteria includes the following steps:

[0046] (1) Dilute the freeze-dried Phanerochaetechrysosporium powder by 10000 times with sterilized deionized water. Use a pipette to suck 0.2 mL of the dissolved dry powder and inoculate it on the PDA medium. Spread evenly and put it in Incubate at 30°C for 6 days in an incubator; then drip sterile deionized water into the cultured plate, stir gently with an inoculating needle, and filter with gauze to obtain a spore suspension of P. chrysosporium spores. Liquid, sealed and stored in a refrigerator at 6°C for later use;

[0047] (2) The lotus leaf biomass is washed, dried at 90°C, and cut into fragments of 0.5-1.5 cm to obtain pretreated raw materials;

[0048] (3) Take 200g of peeled potatoes, wash and cut into small pieces, add 1L of deionized water and boil for 30min to obtain the filtrate; make up the fi...

Example Embodiment

[0053] Example 3

[0054] The method for preparing micro-mesoporous porous carbon material with high specific surface area by treating hemicellulose degrading bacteria includes the following steps:

[0055] (1) Dilute the lyophilized dry powder of Aspergillus tubingensis by 10000 times with sterilized deionized water, pipette 0.4 mL of the dissolved dry powder bacteria liquid and inoculate it on Chase agar medium, spread it evenly, and put it in the culture Incubate at 30°C for 6 days in a box, then drip sterile deionized water into the cultured plate, stir gently with an inoculating needle, and filter with gauze to obtain A. tubingensis spore suspension, sealed and stored in a refrigerator at 6°C for later use ;

[0056] (2) The lotus leaf biomass is washed, dried at 90°C, and cut into fragments of 0.5-1.5 cm to obtain pretreated raw materials;

[0057] (3) Take 30g of Cha's liquid culture medium into 1L of deionized water, dissolve, sterilize, and cool to room temperature to obtain...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Specific surfaceaaaaaaaaaa
Micropore specific surface areaaaaaaaaaaa
Mesopore specific surface areaaaaaaaaaaa
Login to view more

Abstract

The invention belongs to the technical field of preparation of porous carbon materials, and discloses a porous carbon material with a high specific surface area by virtue of fungal pretreatment as well as a method and application thereof. The method comprises the following steps: (1) drying and crushing waste biomass to obtain crushed waste biomass; 2) carrying out the constant-temperature oscillation reaction for the crushed waste biomass and fungal spore suspension in a liquid culture medium, filtering, washing, and drying to obtain a carbonization precursor; carrying out the high-temperature carbonization treatment to obtain a primary carbonized substance; and 3) activating the primary carbonized substance and an activator in inert atmosphere to obtain the porous carbon material with ahigh specific surface area. According to the invention, the porous carbon material is prepared by virtue of the regulation of fungal treatment, so that the waste biomass is effectively utilized, the preparation process is simple, the production cost is low, and the method is environment-friendly; and the obtained porous carbon material is high in specific surface area and unique in aperture distribution and capable of obtaining micro-porous, mesoporous or micro-mesoporous carbon materials. The porous carbon material is applied to the field of adsorption.

Description

technical field [0001] The invention belongs to the technical field of porous carbon materials, and in particular relates to a carbon material with a high specific surface area and a method for preparing a specific pore structure (microporous, mesoporous or micro-mesoporous) by fungal pretreatment and its application in the field of adsorption. in the application. Background technique [0002] with O 3 Extreme air pollution such as photochemical smog pollution and haze caused by PM2.5 have seriously affected the quality of the air environment and human health. Volatile organic compounds (VOCs) as O 3 It is one of the key precursors for the formation of PM2.5 and its effective control and reduction is crucial to improving air quality. At present, the adsorption technology using common porous carbon materials as adsorbents has been widely used in the adsorption of VOCs due to its advantages of low cost and wide adaptability. However, such adsorbents have problems such as l...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C01B32/324C01B32/348B01D53/02
CPCB01D53/02C01B32/324C01B32/348B01D2257/70
Inventor 黄皓旻张伟霞成海荣叶代启
Owner SOUTH CHINA UNIV OF TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap