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Cobalt chromium molybdenum tungsten alloy fine spherical powder and preparation method thereof

A spherical powder, tungsten alloy technology, applied in metal processing equipment, transportation and packaging, additive processing, etc., can solve the problems affecting the popularization and application of SLM technology, high oxygen content, low sphericity, etc., and is conducive to market promotion. , Excellent mechanical properties, high relative density

Inactive Publication Date: 2019-08-06
佛山市岁之博新材料科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] SLM technology has high requirements for metal powder. In addition to good plasticity, it must also meet the requirements of fine powder particle size, narrow particle size distribution, high sphericity, good fluidity and high bulk density. At present, domestically produced Cobalt-chromium-molybdenum-tungsten alloys basically have disadvantages such as large particle size, low sphericity, and high oxygen content, which cannot be used for SLM forming, which in turn affects the promotion and application of SLM technology in the biomedical field.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Embodiment 1: A cobalt-chromium-molybdenum-tungsten alloy fine spherical powder comprises the following components by weight:

[0030] Cobalt 61%; Chromium 25.73%;

[0031] Molybdenum 5.9%; Tungsten 5.6%;

[0032] Silicon 1.5%; the balance is impurities.

[0033] Then prepare according to the following method, step S1, accurately weigh according to the proportion of the required formula, mix the raw materials obtained by weighing into an intermediate frequency induction furnace for melting to obtain alloy melt; step S2, use the gas heating system to heat the inert gas Heating; step S3, pour the melt obtained in step S1 into a tundish, and flow it into the atomizing nozzle through a catheter, and use hot gas to supersonically atomize the molten metal to obtain powder; step S4, to obtain The powder is sieved to obtain cobalt-chromium-molybdenum-tungsten alloy fine spherical powder with a particle size of less than 30 μm.

[0034] The preferred scheme is adopted during ...

Embodiment 2

[0036] Embodiment 2: a kind of fine spherical powder of cobalt chromium molybdenum tungsten alloy comprises following composition by weight:

[0037] Cobalt 60%; Chromium 27%;

[0038] Molybdenum 5%; Tungsten 6%;

[0039] Silicon 1.2%; the balance is impurities.

[0040] Then prepare according to the following method, step S1, accurately weigh according to the proportion of the required formula, mix the raw materials obtained by weighing into an intermediate frequency induction furnace for melting to obtain alloy melt; step S2, use the gas heating system to heat the inert gas Heating; step S3, pour the melt obtained in step S1 into a tundish, and flow it into the atomizing nozzle through a catheter, and use hot gas to supersonically atomize the molten metal to obtain powder; step S4, to obtain The powder is sieved to obtain cobalt-chromium-molybdenum-tungsten alloy fine spherical powder with a particle size of less than 30 μm.

[0041] The preferred scheme is adopted during...

Embodiment 3

[0043] Embodiment 3: A cobalt-chromium-molybdenum-tungsten alloy fine spherical powder comprises the following components by weight:

[0044] Cobalt 65%; Chromium 24%;

[0045] Molybdenum 5%; Tungsten 5%;

[0046] Silicon 0.5%; the balance is impurities.

[0047] Then prepare according to the following method, step S1, accurately weigh according to the proportion of the required formula, mix the raw materials obtained by weighing into an intermediate frequency induction furnace for melting to obtain alloy melt; step S2, use the gas heating system to heat the inert gas Heating; step S3, pour the melt obtained in step S1 into a tundish, and flow it into the atomizing nozzle through a catheter, and use hot gas to supersonically atomize the molten metal to obtain powder; step S4, to obtain The powder is sieved to obtain cobalt-chromium-molybdenum-tungsten alloy fine spherical powder with a particle size of less than 30 μm.

[0048] The preferred scheme is adopted during the pre...

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Abstract

The invention discloses cobalt chromium molybdenum tungsten alloy fine spherical powder. The cobalt chromium molybdenum tungsten alloy fine spherical powder is characterized by comprising the following components in percentage by mass: 60-66% of cobalt, 24-27% of chromium, 5-6% of molybdenum, 5-6% of tungsten, 0-1.5% of silicon, and the balance of impurities. The preparation comprises the following steps: (S1) the precise weighing is performed according to the ratio of the needed formula; weighed raw materials are mixed in a medium-frequency induction furnace for smelting to obtain molten alloys; (S2) inert gas is heated by using a gas heating system; (S3) the molten alloys obtained in the step (S1) are poured in a tundish, and flow into an atomization nozzle through a liquid guide pipe; and the supersonic-speed gas atomization is performed on the molten metal by using hot air to obtain powder; and (S4) the obtained powder is screened to obtain the cobalt chromium molybdenum tungsten alloy fine spherical powder with the particle size of smaller than 30 microns. The cobalt chromium molybdenum tungsten alloy fine spherical powder achieves high relative density and excellent mechanical performances under the condition of relative lower cost, facilitates the popularization and the application of the SLM technology in the biomedical field, and achieves higher practicability.

Description

technical field [0001] The invention belongs to the field of material preparation, and in particular relates to a cobalt-chromium-molybdenum-tungsten alloy fine spherical powder and a preparation method thereof. Background technique [0002] Caries and periodontal disease are the most common oral diseases. The Chinese population suffers from caries slightly higher, and the oral health situation is not optimistic. Therefore, it is of great significance to study the preparation of dental substitute products and provide better restorations for patients with dental diseases. social benefits. [0003] Cobalt-chromium-molybdenum-tungsten alloy has good biocompatibility, strong metal-ceramic bonding and corrosion resistance, and is relatively cheap. It is widely used in the field of oral restoration. Due to the complex structure of oral restorations, traditional casting or Forming by forging method, the process is cumbersome, the cycle is long, the cost is high, and it is easy to ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F1/00B22F9/08B33Y70/00C22C19/07
CPCB22F9/082B33Y70/00C22C19/07B22F1/065
Inventor 肖志瑜班乐温利平朱权利陈进
Owner 佛山市岁之博新材料科技有限公司
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