Method for improving electrochemical performance of lithium battery positive electrode coating material
A coating material and cathode material technology, applied in the field of lithium ion battery cathode material preparation, can solve problems such as affecting battery specific capacity, affecting lithium ion transmission, losing protection effect, etc., to improve cycle life, improve charge and discharge efficiency, reduce The effect of energy consumption
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[0028] Example 1:
[0029] A method for preparing a conductive-enhanced lanthanum titanate-coated lithium nickel manganate positive electrode material, comprising the following steps:
[0030] (1) take by weighing lanthanum hydroxide and titanium tetrachloride in a molar ratio of 1:1;
[0031] (2) dissolving lanthanum hydroxide and tetrabutyl titanate in triethylene glycol, and heating to 60° C. to fully dissolve them to obtain mixed solution A;
[0032] (3) under the condition that the temperature of the mixed solution A is 60°C and the rotational speed of the agitator is 200 r / min, mechanical stirring is performed for 30 minutes to obtain the mixed suspension B;
[0033] (4) Under the condition of mechanical stirring at 60°C and 300r / min, add ammonia water to the mixed suspension B, and the amount of ammonia water is 5 times the weight of lanthanum hydroxide.
[0034] (5) Continue stirring the mixed suspension in step (4) at 160° C. and 300 r / min for 4 hours to obtain a la...
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[0037] Example 2:
[0038] A preparation method of a conductive zinc oxide-coated lithium nickel manganate positive electrode material, comprising the following steps:
[0039] (1) take by weighing sodium hydroxide and zinc acetate by the mol ratio of 1:1;
[0040] (2) dissolving zinc acetate in methanol, heating to 60° C. to fully dissolve to obtain solution A; dissolving sodium hydroxide in methanol and stirring to obtain solution B;
[0041] (3) under the condition that the temperature of the mixed solution A is 60°C and the rotating speed of the agitator is 200r / min, the solution B is slowly added to the solution A, and mechanically stirred for 30 minutes to obtain the zinc oxide sol;
[0042] (4) at room temperature, under the mechanical stirring condition of 200r / min, according to the concentration of zinc oxide sol, take by weighing the powder of lithium nickel manganese oxide according to the molar ratio of zinc oxide: lithium nickel manganate is 0.5:9.5, The powder ...
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