This invention discloses a homogeneous
corundum mullite brick and its preparation process, belonging to the field of
refractory materials technology. The process employs a
sol-gel assisted microscopic in-situ homogenization method: a precursor
sol film is formed on the submicron-level
bauxite surface by constructing a homogeneous
lanthanum ion solution and performing colloidal-level contact
grinding; a
salt bridge network is formed by
spray drying and
granulation; finally,
sintering is carried out under an oxidizing
atmosphere, inducing
lanthanum ions to preferentially react with impurities to generate high-melting-point
lanthanum ferrite or
lanthanum titanate-like crystalline phases. This process blocks impurities from participating in the formation of low-melting-point glass phases at the
microscopic scale, resulting in clean grain boundaries within the
brick and the absence of continuous glass phases. The obtained product exhibits a high-temperature
creep rate of less than [value missing] and a load
softening temperature of [value missing], achieving a breakthrough in the preparation of high-end
refractory materials using low-grade raw materials.