A kind of anti-aging cerium-zirconium composite oxide and its preparation method and application
A composite oxide, anti-aging technology, applied in chemical instruments and methods, separation methods, metal/metal oxide/metal hydroxide catalysts, etc. Aging activity, uniform distribution of element lattice doping, cost reduction effect
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Embodiment 1
[0065] Example 1 provides a composition comprising CeO 2 40%, ZrO 2 50%, La 2 o 3 5%, Pr 6 o 11 5% cerium-zirconium composite oxide, prepared by the following method:
[0066] Add 419g of zirconium oxychloride, 466g of cerium ammonium nitrate, 65g of lanthanum nitrate and 58g of nitrate into 1500mL of ultrapure water, stir for 0.5h to obtain a clear solution, which is introduced into an aqueous ammonia solution to obtain the first precipitate; continue Add the remaining 279g of zirconyl chloride and 155g of ammonium cerium nitrate into 1500mL of pure water, stir for 0.5h, introduce into the above first precipitate, and adjust the pH value to 10 to obtain cerium hydroxide - zirconium hydroxide - Mixed precipitation of lanthanum hydroxide-praseodymium hydroxide.
[0067] Filter and wash the above-mentioned precipitate for at least 3 times, then put it into a 10L high-pressure reactor, and add 5L of the mixed solvent of the above-mentioned ionic liquid (salicylic acid / t...
Embodiment 2
[0073] Example 2 provides a composition comprising CeO 2 20%, ZrO 2 73%, La 2 o 3 2%, Nd 2 o 3 5% cerium-zirconium composite oxide, prepared by the following method:
[0074] Add 559g of zirconium oxychloride, 249g of cerium ammonium nitrate, 26g of lanthanum nitrate and 65g of neodymium nitrate into 1500mL of ultrapure water, stir for 0.5h to obtain a clear solution, introduce the solution into an aqueous ammonia solution to obtain the first precipitate; The remaining 461g of zirconyl chloride and 62g of cerium ammonium nitrate were added to 1500mL of pure water, stirred for 0.5h, introduced into the above-mentioned first precipitate, and adjusted to pH 10 to obtain cerium hydroxide-zirconium hydroxide-hydroxide Mixed precipitation of lanthanum-neodymium hydroxide.
[0075] Filter and wash the above-mentioned precipitate for at least 3 times, then put it into a 10L high-pressure reactor, and add 5L of the mixed solvent of the above-mentioned ionic liquid (salicylic ...
Embodiment 3
[0078] Example 3 provides a composition comprising CeO 2 25%, ZrO 2 60%, La 2 o 3 3%, Y 2 o 3 12% cerium-zirconium composite oxide, prepared by the following method:
[0079]Add 559g of zirconium oxychloride, 280g of ceric ammonium nitrate, 39g of lanthanum nitrate and 102g of yttrium nitrate into 1500mL of ultrapure water, stir for 0.5h to obtain a clear solution, introduce the solution into an aqueous ammonia solution to obtain the first precipitate; The remaining 279g of zirconium oxychloride and 109g of cerium ammonium nitrate were added to 1500mL of pure water, stirred for 0.5h, introduced into the above-mentioned first precipitate, and adjusted to pH 10 to obtain cerium hydroxide-zirconium hydroxide-lanthanum hydroxide - Mixed precipitation of yttrium hydroxide.
[0080] Filter and wash the above-mentioned precipitate for at least 3 times, then put it into a 10L high-pressure reactor, and add 5L of the mixed solvent of the above-mentioned ionic liquid (salicyli...
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