8 results about "Zirconium hydroxide" patented technology

A method for forming a dehydration catalyst may comprise peptizing a catalyst precursor with an acid, a cellulose ether, or both, thereby forming a catalyst precursor sol, wherein the catalyst precursor comprising a tungstated support of tungsten and at least one of zirconium oxides, zirconium hydroxides, or titanium oxides; subjecting the catalyst precursor sol to kneading and extrusion to form one or more catalyst precursor extrudates; calcining the one or more catalyst precursor extrudates to form a calcined catalyst precursor; and cooling the calcined catalyst precursor to form the dehydration catalyst.

A method for forming a dehydration catalyst may comprise peptizing a catalyst precursor with an acid, a cellulose ether, or both, thereby forming a catalyst precursor sol, wherein the catalyst precursor comprising a tungstated support of tungsten and at least one of zirconium oxides, zirconium hydroxides, or titanium oxides; subjecting the catalyst precursor sol to kneading and extrusion to form one or more catalyst precursor extrudates; calcining the one or more catalyst precursor extrudates to form a calcined catalyst precursor; and cooling the calcined catalyst precursor to form the dehydration catalyst. The catalysts of the examples have platinum or palladium impregnated on a tungstated zirconia support.

The present invention discloses a method for preparing and using a heavily coated cobalt oxide. First, spherical cobalt hydroxide particles are synthesized by a co-precipitation method. Then, the spherical cobalt hydroxide particles are dried, dehydrated, and uniformly mixed with zirconium alkyl carboxylate / aluminum alkyl carboxylate and zirconium hydroxide / aluminum hydroxide. The mixture is then heated to react with the cobalt hydroxide on the particle surface, causing it to adhere closely to the surface of the spherical cobalt hydroxide particles. Finally, the particles are calcined to remove organic matter, resulting in spherical cobalt oxide particles with a strong coating on their surface.In the present invention, the coating layer and the base material are connected through chemical bonds, which makes the two adhere to each other more closely, so that the coating layer is not easy to spray off and peel off, greatly extending the service life of the coating layer, and improving the cycle performance of the material.

This invention discloses a method for crystallizing sodium nitrate in the field of inorganic salt crystallization technology. The method involves dissolving sodium nitrate raw material in deionized water and filtering. Magnesium-aluminum-silicon-boron composite layered oxygen hydroxyl compound nanosheets anchored with fluorine-containing cerium-zirconium hydroxide-hydrated oxides are added to the filtrate. The mixture is then dispersed under heat, cooled in stages, seeded with sodium nitrate under reduced pressure, evaporated under reduced pressure, crystallized under heat, centrifuged, washed with a saturated sodium nitrate solution, and dried to obtain sodium nitrate crystals. The fluorine-containing cerium-zirconium hydroxide-hydrated oxide-anchored magnesium-aluminum-silicon-boron composite layered oxygen hydroxyl compound nanosheets are obtained through co-precipitation of magnesium, aluminum, cerium, and zirconium nitrates, heat treatment with fluorine-containing water, silicon-boron composite modification, and heat-treated grinding and spray drying. This invention can regulate the nucleation and growth of sodium nitrate crystals, improve crystal particle size uniformity, reduce mother liquor entrainment, and improve crystal separation and drying effects.

The present disclosure relates to a method for preparing an electrolytic hydrogen production diaphragm, wherein the method comprises: mixing inorganic oxidized particles, metal hydroxide, binder and pore-forming agent to obtain a mixed slurry; coating the mixed slurry on one side or both sides of a porous base film to obtain a nascent film; soaking the nascent film in an extraction liquid and then performing a drying treatment; wherein the porous base film comprises a metal mesh; the metal hydroxide comprises one or more of nickel hydroxide, nickel oxyhydroxide, zirconium hydroxide, cerium hydroxide and yttrium hydroxide. The method provided by the present disclosure effectively improves the temperature resistance and high-temperature dimensional stability of the electrolytic hydrogen production diaphragm prepared by the method, while effectively improving the affinity of the diaphragm to the electrolyte, reducing the diaphragm resistance. Using the electrolytic hydrogen production diaphragm provided by the present disclosure in an alkaline electrolytic hydrogen production device can realize the operation of the electrolytic hydrogen production device at a temperature above 110 DEG C, and effectively improve the electrolysis efficiency.

This method for producing a positive electrode active material for secondary batteries is characterized by including: an oxidation step of adding at least one hydroxide selected from the group consisting of aluminum hydroxide, strontium hydroxide, titanium hydroxide, bismuth hydroxide, zirconium hydroxide, and barium hydroxide to an Ni-containing compound, and performing oxidation treatment by heating the mixture; a firing step of mixing an oxide obtained in the oxidation step with an Li-containing compound, and firing the mixture; a water-washing step of mixing a fired product obtained in the firing step with water or an aqueous solution, and washing the mixture with water; and a drying step of drying the wet powder obtained in the water-washing step to obtain a lithium transition metal composite oxide, wherein the heating temperature in the oxidation step is 250°C-650°C inclusive.

The application provides a method for preparing high-dispersion zirconium dioxide, comprising the following steps: dissolving a zirconium salt in water, adding a composite directing agent, and mixing to obtain a precursor solution; the composite directing agent comprises an imidazole ionic liquid and a non-ionic surfactant; dropwise adding the precursor solution into a mixed bottom solution containing an alkaline precipitator and a cationic surfactant, maintaining the pH of the reaction system at 10.5-11.5 to form a zirconium hydroxide precipitate, and obtaining a zirconium hydroxide slurry; filtering and washing the zirconium hydroxide slurry to remove impurity ions, and then replacing and dispersing with a low-carbon alcohol to obtain an alcohol gel precursor; dispersing the alcohol gel precursor in an azeotrope agent to perform azeotrope rectification, removing the azeotrope agent and the solvent, and obtaining a dry powder; and mixing the dry powder with an inorganic salt, and then performing a step-by-step controlled calcination treatment to obtain high-dispersion zirconium dioxide.