A method for extracting and separating pigment from purple lucidum waste
A waste and pigment technology, applied in food extraction, function of food ingredients, chemical instruments and methods, etc., can solve the problems of inability to meet the quality requirements of food or health food, difficult dissolution of purple zhi pigment complex, and high cost. The effect of simple and easy extraction and separation methods
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specific Embodiment 1
[0036] 1. 5 kg of the waste extracted from the fruiting body of Zizhi lucidum was subjected to steam explosion pretreatment to obtain explosives. The pressure during steam explosion was 2Mpa, and the treatment time was 600s;
[0037] 2 The explosives are extracted with 100kg of alkali-alcoholic solution, the alkali is food additive sodium hydroxide or potassium hydroxide, the solvent is 20% ethanol solution prepared by 95% edible grade ethanol and purified water, the final pH of the alkali-alcohol solution is 10, and the extraction temperature is 50°C, the extraction time is 2 hours; the filter mesh is 200 mesh, and about 100kg of alkali extraction solution is obtained by filtration;
[0038] 3 Adjust the pH of the alkali extraction solution to neutral with food additive hydrochloric acid, the final pH is 6, centrifuge to separate the solid phase and the liquid phase, the separation factor is 10,000 during centrifugation, the turbidity of the liquid phase is below 100NTU, and t...
specific Embodiment 2
[0043] 1. 5kg of the wastes extracted from the fruiting body of Zizhi lucidum were subjected to steam explosion pretreatment to obtain explosives. The pressure during steam explosion was 3Mpa, and the treatment time was 450s;
[0044] 2 The explosives are extracted with 100kg of alkali-alcoholic solution, the alkali is food additive sodium hydroxide or potassium hydroxide, the solvent is 20% ethanol solution prepared by 95% edible grade ethanol and purified water, the final pH of the alkali-alcohol solution is 10, and the extraction temperature is 55°C, the extraction time is 1.5h; the filter mesh is 200 mesh, and about 100kg of alkali extraction solution is obtained by filtration;
[0045] 3 Adjust the pH of the alkali extraction solution to neutral with food additive hydrochloric acid, the final pH is 6, centrifuge to separate the solid phase and the liquid phase, the separation factor is 10,000 during centrifugation, the turbidity of the liquid phase is below 100NTU, and the...
Embodiment 3
[0049] 1. 5 kg of the waste extracted from the fruiting body of Zizhi lucidum was subjected to steam explosion pretreatment to obtain explosives. The pressure during steam explosion was 3.5Mpa, and the treatment time was 300s;
[0050] 2 The explosives are extracted with 100kg of alkali-alcoholic solution, the alkali is food additive sodium hydroxide or potassium hydroxide, the solvent is 20% ethanol solution prepared by 95% edible grade ethanol and purified water, the final pH of the alkali-alcohol solution is 10, and the extraction temperature is 60°C, the extraction time is 1h; the filter mesh is 200 mesh, and about 100kg of alkali extraction solution is obtained by filtration;
[0051] 3. Adjust the pH of the alkali extraction solution to neutral with food additive hydrochloric acid, and the final pH is 7. Centrifuge to obtain a solid phase and a liquid phase. The separation factor during centrifugation is 10,000, and the turbidity of the liquid phase is below 100 NTU. The ...
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