A metal packaging coating cured by electron beam and preparation method thereof
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Embodiment 1
[0041] Embodiment 1: An electron beam cured metal packaging coating, the components and their corresponding parts by weight are shown in Table 1, and are prepared through the following steps:
[0042] Step 1, preparing modified novolac epoxy acrylate: mixing novolac epoxy resin and acrylic acid with a molar ratio of 1:0.25 and adding to toluene, adding 2% N,N-dimethylaniline in parts by weight, and React at 75°C for 3 hours, after natural cooling, extract 4 times with anhydrous ether to obtain a viscous substance, dry the viscous substance in vacuum at 50°C for 24 hours to obtain the product;
[0043] Step 2, stirring 1 / 4 of the total amount of modified novolac epoxy acrylate, triethoxysilane, titanium dioxide, carbon black, and sodium lauryl sulfate to form a mixture;
[0044] Step 3, placing the uniformly stirred mixture in step 2 in a grinder for grinding and dispersing to obtain a color paste;
[0045] Step 4, mix the color paste prepared in step 3 with the remaining 30 p...
Embodiment 2-6
[0047] Embodiment 2-6: An electron beam cured coating for metal packaging. The difference from Embodiment 1 is that each component and its corresponding parts by weight are shown in Table 1.
[0048] Each component and parts by weight thereof in Table 1 Embodiment 1-6
[0049]
Embodiment 7
[0050] Embodiment 7: a kind of preparation method of the metal packaging coating of electron beam solidification, and the difference of embodiment 1 is, in step one, prepare modified novolac epoxy acrylate: the phenolic ring that molar ratio is 1:1 Oxygen resin and acrylic acid were mixed and added to toluene, 2% by weight of N,N-dimethylaniline was added, reacted at 90°C for 2 hours, cooled naturally, extracted 4 times with anhydrous ether to obtain viscous Thick material, the viscous material was vacuum-dried at 50°C for 24 hours to obtain.
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