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High-alumina glass frosting liquid and preparation method thereof

A high-alumina glass and frosting liquid technology, which is applied in the field of glass surface processing, can solve the problems of unguaranteed production yield, poor stability of etching liquid, and poor etching stability, etc.

Inactive Publication Date: 2019-12-13
YICHANG NANBO DISPLAY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the prior art, patent publication numbers CN101215097A, CN1154951A and CN1400184A all use highly volatile components of hydrochloric acid, poor stability of etching solution, large changes in industrial production process, resulting in low production yield
In the patent application documents whose patent publication numbers are CN101654330A and CN103030301A, the Arabic resin used as the raw material, because the raw material is expensive, the cost of manufacturing the frosting liquid is relatively high
Compared with soda-lime glass, high-alumina glass has the advantages of good chemical stability and high mechanical strength, and the demand for high-alumina glass in the field of display covers is gradually increasing, because Al in high-alumina glass 2 o 3 The content is greater than 12%, and the hardness is relatively high. The frosting solution that can be used for soda-lime glass is not suitable for high-alumina glass. The etching stability is poor, and the production yield cannot be guaranteed.

Method used

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  • High-alumina glass frosting liquid and preparation method thereof
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  • High-alumina glass frosting liquid and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0021] High alumina glass frosting liquid, including the following components by weight: 10kg ammonium bifluoride, 2.5kg citric acid, 1.5kg barium sulfate, 1.4kg starch, 1.6kg bentonite, 4.2kg ferric chloride, 2.9kg potassium fluoride kg, potassium nitrate 2.2kg, hydrofluoric acid 1.8kg and water 4.2kg.

[0022] Its concrete preparation method is:

[0023] Weigh each raw material according to the proportion, mix water, ammonium hydrogen fluoride, citric acid, ferric chloride, potassium fluoride, potassium nitrate, hydrofluoric acid, barium sulfate, and stir evenly, add starch and bentonite, and age after stirring evenly. The curing temperature is 35-45° C., and the aging time is more than 48 hours to obtain a high-alumina glass frosting solution.

[0024] The prepared high-alumina glass frosting solution is used for anti-glare etching of high-alumina glass. The same set of frosting solution is used for anti-glare etching of high-alumina glass several times. The specific param...

Embodiment 2

[0028] High alumina glass frosting liquid, including the following components by weight: 9.5kg ammonium bifluoride, 1.6kg citric acid, 0.7kg barium sulfate, 1.3kg starch, 0.8kg bentonite, 3.2kg ferric chloride, potassium fluoride 1.6kg, potassium nitrate 2.0kg, hydrofluoric acid 0.8kg and water 3.5kg.

[0029] The preparation method is the same as in Example 1.

[0030] Weigh each raw material according to the proportion, mix water, ammonium hydrogen fluoride, citric acid, ferric chloride, potassium fluoride, potassium nitrate, hydrofluoric acid, barium sulfate, and stir evenly, add starch and bentonite, and age after stirring evenly. The curing temperature is 35-45° C., and the aging time is more than 48 hours to obtain a high-alumina glass frosting solution.

[0031] The prepared high-alumina glass frosting solution is used for anti-glare etching of high-alumina glass. The same set of frosting solution is used for anti-glare etching of high-alumina glass several times. The ...

Embodiment 3

[0035] High alumina glass frosting liquid, including the following components by weight: 13kg ammonium bifluoride, 4.2kg citric acid, 1.55kg barium sulfate, 2.8kg starch, 1.8kg bentonite, 5kg ferric chloride, 4kg potassium fluoride, Potassium nitrate 3.6kg, hydrofluoric acid 1.8kg and water 7kg.

[0036] The preparation method is the same as in Example 1.

[0037] Weigh each raw material according to the proportion, mix water, ammonium hydrogen fluoride, citric acid, ferric chloride, potassium fluoride, potassium nitrate, hydrofluoric acid, barium sulfate, and stir evenly, add starch and bentonite, and age after stirring evenly. The curing temperature is 35-45° C., and the aging time is more than 48 hours to obtain a high-alumina glass frosting solution.

[0038] The prepared high-alumina glass frosting solution is used for anti-glare etching of high-alumina glass. The same set of frosting solution is used for anti-glare etching of high-alumina glass several times. The specif...

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Abstract

The invention discloses a high-alumina glass frosting liquid and a preparation method thereof. The high-alumina glass frosting liquid comprises the following components in parts by weight: 30-45 partsof ammonium bifluoride, 5-15 parts of citric acid, 2-5 parts of barium sulfate, 4-10 parts of starch, 2-6 parts of bentonite, 10-20 parts of ferric trichloride, 5-15 parts of potassium fluoride, 6-13parts of potassium nitrate, 2-6 parts of hydrofluoric acid and 10-30 parts of water. The frosting liquid is low in manufacturing cost and high in production yield; and anti-dazzle glass prepared fromthe frosting liquid has the characteristics of high glossiness, low flash point, low roughness and good anti-dazzle effect.

Description

technical field [0001] The invention belongs to the technical field of glass surface processing, and in particular relates to a high-alumina glass frosting liquid and a preparation method thereof. Background technique [0002] AG (Anti-glare glass) glass is also called anti-glare glass. It has a special treatment on the surface of the glass, so that it has a lower reflectance than ordinary glass, reduces the reflection of the screen, and makes the display screen clearer and more realistic. The manufacture of AG glass is generally divided into three processes: spraying, coating and etching. Spraying AG glass is to apply a layer of chemical substances on the surface of the glass to form concave-convex particles to achieve anti-glare effect by means of evaporation coating; coated AG glass is to deposit a film on the surface of the glass, so that the surface can resist light reflection Substance; Etching AG glass is to etch the glass surface by chemical etching to form an uneve...

Claims

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Application Information

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IPC IPC(8): C03C15/00
CPCC03C15/00
Inventor 吕志明连乾金彪
Owner YICHANG NANBO DISPLAY
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