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Preparation method for copper nanowire toughened root-resistant waterproof coiled material covering material

A technology of copper nanowires and waterproofing membranes, which is applied in the direction of roofing, building insulation materials, roofing and other directions using flexible materials, can solve the problem that the root resistance performance cannot meet the needs of use, and achieves easy control, good crystallinity, and adhesion. Good effect on sex and coordination

Active Publication Date: 2020-02-07
HUBEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in terms of root resistance, its performance cannot meet the current use requirements.

Method used

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  • Preparation method for copper nanowire toughened root-resistant waterproof coiled material covering material
  • Preparation method for copper nanowire toughened root-resistant waterproof coiled material covering material
  • Preparation method for copper nanowire toughened root-resistant waterproof coiled material covering material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Step 1: Use 5 parts by weight of copper chloride and 5 parts by weight of ethylenediaminetetraacetic acid to prepare a solution, add 4 parts by weight of sodium hexadecylsulfonate into the solution and stir evenly, and finally add 5 to 10 parts by weight of Parts of sodium citrate, stir to mix well. The mixed solution was irradiated with a pulsed laser with a power of 10 W, a frequency of 20 Hz, and a processing time of 10 minutes. Copper nanowires were obtained by centrifugation under vacuum.

[0025] Step 2: Disperse 10 parts by weight of copper nanowires into a 1:1 mixture of 100 parts by weight of distilled water and ethanol, add 15 parts by weight of polyethylene glycol trimethoxysilyl propyl ether, control the reaction time for 8 hours, and the temperature at 40°C to obtain the modified copper nanowire fluid.

[0026] Step 3: The master batch of the coil cladding material is mainly prepared from the following raw materials according to the weight percentage of e...

Embodiment 2

[0028] Step 1: Use 10 parts by weight of copper acetate and 10 parts by weight of disodium edetate to form a solution, add 4 parts by weight of sodium lignosulfonate to the solution and stir evenly, and finally add 10 parts by weight of citric acid to the solution sodium, stir to mix well. By irradiating the mixed solution with a pulsed laser, the power of the pulsed laser is 50 W, the frequency is 50 Hz, and the processing time is 30 minutes. Copper nanowires were obtained by centrifugation under vacuum.

[0029] Step 2: Disperse 5 parts by weight of copper nanowires into a 1:1 mixture of 100 parts by weight of distilled water and ethanol, add 8 parts by weight of polyethylene glycol triethoxysilyl propyl ether, and control the reaction time for 4 hours , the temperature is 60° C., and the modified copper nanowire fluid is obtained.

[0030] Step 3: The masterbatch of the coil cladding material is mainly prepared from the following raw materials according to the weight perc...

Embodiment 3

[0032] Step 1: Use 5 parts by weight of copper sulfate and 10 parts by weight of ethylenediaminetetraacetic acid to form a solution, add 2 parts by weight of sodium dodecylsulfonate to the solution and stir evenly, and finally add 5 parts by weight of citric acid to the solution sodium, stir to mix well. By irradiating the mixed solution with a pulsed laser, the power of the pulsed laser is 10 W, the frequency is 50 Hz, and the processing time is 30 minutes. Copper nanowires were obtained by centrifugation under vacuum.

[0033] Step 2: Disperse 10 parts by weight of copper nanowires into a 1:1 mixture of 100 parts by weight of distilled water and ethanol, add 15 parts by weight of polyethylene glycol trimethoxysilyl propyl ether, and control the reaction time to be 6 hours and the temperature at 50°C to obtain the modified copper nanowire fluid.

[0034] Step 3: The master batch of the coil cladding material is mainly prepared from the following raw materials according to t...

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Abstract

The invention discloses a preparation method for a copper nanowire toughened root-resistant waterproof coiled material covering material, and solves the problems that adhesion and coordination betweena current covering material and a coiled material are poor, and root resistance needs to be further improved. The technical solution is characterized in that the method comprises the following steps:preparing a modified copper nanowire fluid: dispersing 5-10 parts by weight of copper nanowires into 100 parts by weight of 50% ethanol, adding 8-15 parts by weight of a silane coupling agent, and performing mixing to obtain the modified copper nanowire fluid; and preparing the coiled material covering material: mixing the following materials: 75-80% of high-density polyethylene, 1-5% of an auxiliary agent, 10-15% of the modified copper nanowire fluid, 1-5% of an anti-aging agent, and 1-5% of a stabilizer, and performing film processing to obtain the coiled material covering material. The method has the advantages of simple operation and high controllability, the prepared copper nanowires has good compatibility with the coiled material, the root-resistant characteristics of the material can be enhanced, the adhesion and coordination of the covering material and the coiled material can be ensured, and the method has the toughening and enhancement effects.

Description

technical field [0001] The invention relates to the field of waterproof materials, in particular to a method for preparing a waterproof roll material cladding material. Background technique [0002] At present, as the requirements for building life become more and more stringent, people's demand for building waterproofing is gradually increasing, and the demand for waterproofing in areas such as building exterior walls and roofs is more stringent. Commonly used waterproof membrane products are waterproof material products made by impregnating asphalt or polymer waterproof materials on the carcass to form membranes. It is mainly divided into asphalt waterproofing membrane, polymer modified asphalt waterproofing membrane and synthetic polymer waterproofing membrane. Waterproof membranes are required to have good water resistance, stability to temperature changes, no flow, no foaming, no confusion at high temperatures; no brittle cracks at low temperatures, certain mechanical ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/06C08L91/06C08L91/00C08K9/06C08K7/00C08K3/08E04B1/66E04D5/10
CPCC08L23/06E04B1/665E04D5/10C08K2201/011C08K2003/085C08L2207/062C08K2201/003C08K2201/006C08K2201/016C08L91/06C08K9/08C08K7/00C08K3/08C08L91/00
Inventor 陈顺于肖雷郭雅雯江友志付健健徐焰贺行洋苏英陈威杨进王迎斌毛云
Owner HUBEI UNIV OF TECH