Ionothermal synthesis method of hierarchical pore AlPO-34 molecular sieve
An ionothermal synthesis, alpo-34 technology, applied in the direction of molecular sieve characteristic aluminum phosphate, molecular sieve and base exchange phosphate, phosphorus compound, etc., can solve the problems of expensive organic templates, shorten the synthesis time, reduce energy consumption, reduce The effect of production costs
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Embodiment 1
[0034] Prepare the hierarchical porous AlPO-34 molecular sieve as follows:
[0035] (1) Dissolve aluminum isopropoxide, phosphoric acid, hydrofluoric acid, and cyclohexylamine in 1-butyl-3-methylimidazolium bromide ionic liquid in an oil bath, and the molar ratio is 2:2:3: 3:80, stir evenly until the solid is completely dissolved, then carry out the aging operation, the aging temperature is 50°C, the aging time is 120min, the stirring speed is 200rpm, and the AlPO-34 molecular sieve synthetic liquid is obtained;
[0036] (2) Pour the synthesis solution obtained in step (1) into a microwave reactor, and heat it with microwaves. The synthesis temperature is 150° C., and the synthesis time is 2 hours. After the synthesis is completed, the solid product is obtained by static centrifugation, and the solid product is repeatedly washed with ethanol until there is no ionic liquid;
[0037] (3) Dry the washed solid product obtained in step (2), place the dried solid in a muffle furnac...
Embodiment 2
[0041] By the same operation as in Example 1, only using phosphorous acid as the P source, the resulting hierarchically porous AlPO-34 zeolite molecular sieve is effective for Cr in sewage 3+ The adsorption rate is 98.9%, and the distribution coefficient is 1.67×10 4 mg / L.
Embodiment 3
[0043] The same operation as in Example 1 was carried out, except that the microwave reaction temperature was 180° C., and the synthesis time was 1 h. The prepared zeolite molecular sieve membrane was applied to the adsorption of heavy metal ions, and was applied to Cu in sewage 2+ The adsorption temperature is 25°C, the initial metal ion concentration is 800ppm, and the adsorption time is 30min. The absorption and extraction rate is 97.1%, and the distribution coefficient is 8.93×10 3 mg / L.
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