A preparation method of polymer composite flocculant for printing and dyeing sewage
A composite flocculant, printing and dyeing sewage technology, applied in chemical instruments and methods, biological water/sewage treatment, water/sludge/sewage treatment, etc., can solve the problems of high operator requirements, high cost, low efficiency, etc. Good processing effect and good combination effect
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Embodiment 1
[0025] A preparation method of a polymer composite flocculant for printing and dyeing sewage, comprising the following steps:
[0026] A, put sodium carboxymethyl cellulose into the reactor, then add sodium chloride solution and stir to form a constant temperature water bath reaction system;
[0027] B, adding vinyl polyamine, internal initiator and crosslinking agent into the reaction kettle, stirring and reacting at constant temperature for 6.5 hours, and standing at constant temperature for 2.5 hours to obtain a viscous liquid;
[0028] C, open the reaction kettle, add acrylamide, carry out a constant temperature heating reaction under nitrogen conditions for 4 hours, and at the same time add the lye of the external initiator dropwise, stir for 2.5 hours after the reaction, and let stand for cooling;
[0029] D. On the basis of step C, add an activator, and after stirring evenly, slowly add an amino acid solution with a mass ratio of 2.2%, stir in a constant temperature wat...
Embodiment 2
[0040] A preparation method of a polymer composite flocculant for printing and dyeing sewage, comprising the following steps:
[0041] A, put sodium carboxymethyl cellulose into the reactor, then add sodium chloride solution and stir to form a constant temperature water bath reaction system;
[0042] B, adding vinyl polyamine, internal initiator and cross-linking agent into the reaction kettle, stirring and reacting at constant temperature for 8 hours, and standing at constant temperature for 2 hours to obtain a viscous liquid;
[0043] C, open the reaction kettle, add acrylamide, carry out a constant temperature heating reaction under nitrogen conditions for 5 hours, and add the lye of the external initiator dropwise at the same time, stir for 1 hour after the reaction, and let stand for cooling;
[0044] D. On the basis of step C, add an activator, and after stirring evenly, slowly add an amino acid solution with a mass ratio of 2.7%, and stir in a constant temperature water...
Embodiment 3
[0055] A preparation method of a polymer composite flocculant for printing and dyeing sewage, comprising the following steps:
[0056] A, put sodium carboxymethyl cellulose into the reactor, then add sodium chloride solution and stir to form a constant temperature water bath reaction system;
[0057] B, adding vinyl polyamine, internal initiator and cross-linking agent into the reaction kettle, stirring and reacting at constant temperature for 6 hours, and standing at constant temperature for 4 hours to obtain a viscous liquid;
[0058] C, open the reaction kettle, add acrylamide, carry out a constant temperature heating reaction under nitrogen conditions for 3 hours, and at the same time add the lye of the external initiator dropwise, stir for 3 hours after the reaction, and let stand to cool;
[0059] D. On the basis of step C, add an activator, and after stirring evenly, slowly add an amino acid solution with a mass ratio of 1.8%, and stir in a constant temperature water ba...
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