Preparation method of single-component fiber
A single-component, fiber technology, applied in the field of fiber materials, can solve the problems of poor water absorption of PBT fibers, complex modification treatment process, unfavorable fiber water absorption modification, etc., and achieves improved dyeing performance, good heat resistance, and poor air permeability. Effect
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Embodiment 1
[0023] A method for preparing single-component fibers, comprising the following steps: PBT chips are dried, and mixed evenly with PMMA powder, polyvinyl alcohol, silk peptide, graphene, polycaprolactam, isophthalic acid, and aromatic hydroxy acid according to the mass ratio , under the protection of nitrogen, through the electron beam device with a radiation dose rate of 8KGy / s, the mixture formed by irradiation is obtained, and then the mixture is added to the twin-screw granulation extruder for granulation and extrusion, and the mixture granules are obtained , and then carry out hot-melt extrusion of the obtained particles, after metering, drawing, cooling, oiling, drawing, and winding, the porous PBT fiber POY filaments are made, and the filaments are balanced, clustered, drawn in an oil-immersed water bath, steamed Stretching, oiling, cutting and relaxation heat setting, the relaxation heat setting temperature is 120°C to obtain PBT fibers;
[0024] Add triethylamine, chlo...
Embodiment 2
[0027] A method for preparing single-component fibers, comprising the following steps: PBT slices are dried, mixed evenly with PMMA powder, cellulose, graphene, polycaprolactam, isophthalic acid, and aromatic hydroxy acids according to the mass ratio, and then placed under nitrogen protection , through an electron beam device with a radiation dose rate of 8KGy / s, the mixture formed by irradiation is obtained, and then the mixture is added to a twin-screw granulation extruder for granulation and extrusion to obtain a mixture granule, and then the obtained The particles are hot-melt extruded, and after metering, spinning, cooling, oiling, drawing, and winding, the porous PBT fiber POY filaments are made. , cutting and relaxation heat setting, the relaxation heat setting temperature is 125°C to obtain PBT fibers;
[0028] Add triethylamine, chloroform, and 4-dimethylaminopyridine (DMAP) into the reaction dish according to the mass ratio of 1: 25: 38, ultrasonically disperse for 3...
Embodiment 3
[0031] A method for preparing single-component fibers, comprising the following steps: PBT slices are dried and mixed with PMMA powder, cellulose, polyvinyl alcohol, silk fibroin peptide, graphene, polycaprolactam, isophthalic acid, and aromatic hydroxy acids according to the mass Mix evenly, under the protection of nitrogen, through the electron beam device with a radiation dose rate of 8KGy / s, obtain the mixture formed by irradiation, then put the mixture into a twin-screw granulation extruder for granulation and extrusion, and obtain Mix the pellets, and then hot-melt extrude the obtained pellets, measure, spin, cool, oil, draw, and wind to make porous PBT fiber POY filaments, which are balanced, clustered, and pulled in an oil-immersed water bath. Stretching, steam stretching, oiling, cutting and relaxation heat setting, the relaxation heat setting temperature is 130°C to obtain PBT fibers;
[0032] Add triethylamine, chloroform, and 4-dimethylaminopyridine (DMAP) into the...
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