Preparation method of S-carboxymethyl-L-cysteine
A technology of cysteine and carboxymethyl, which is applied in the field of amino acid preparation, can solve the problems of large specific surface area of crystals, easy adsorption of solution impurities, difficult purification process, etc., and achieve the effect of improving purity
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Embodiment 1
[0039] A preparation method of S-carboxymethyl-L-cysteine, characterized in that: comprising the following steps,
[0040] Step 1. Dissolve 1mol of L-cysteine hydrochloride monohydrate in 450mL of distilled water, place in ice brine to cool down to 0-5°C, and adjust the pH to 9-10 with 20% sodium hydroxide solution , to obtain solution (a);
[0041] Step 2: Add 1.2 mol of chloroacetic acid into 400 ml of distilled water, stir to dissolve, adjust the pH to 6-7 with 20% sodium hydroxide solution, and obtain solution (b);
[0042] Step 3. Under the protection of nitrogen, drop the solution (b) into the solution (a), and control the temperature in the ice-salt water to 0-5°C. After the dropping, the solution (c) is obtained;
[0043] Step 4: Use 20% sodium hydroxide solution to adjust the pH of the solution (c) to 8, then heat up to 55-60°C, and keep it warm for 1 hour;
[0044] Step 5, the solution (c) is lowered to room temperature, and the pH of the solution (c) is adjusted...
Embodiment 2
[0050] A preparation method of S-carboxymethyl-L-cysteine, characterized in that: comprising the following steps,
[0051] Step 1. Dissolve 1mol of L-cysteine hydrochloride monohydrate in 450mL of distilled water, place in ice brine to cool down to 0-5°C, and adjust the pH to 9-10 with 20% sodium hydroxide solution , to obtain solution (a);
[0052] Step 2: Add 1.3mol of chloroacetic acid into 400ml of distilled water, stir to dissolve, adjust the pH to 6-7 with 20% sodium hydroxide solution, and obtain solution (b);
[0053] Step 3. Under the protection of nitrogen, drop the solution (b) into the solution (a), and control the temperature in the ice-salt water to 0-5°C. After the dropping, the solution (c) is obtained;
[0054]Step 4: Use 20% sodium hydroxide solution to adjust the pH of the solution (c) to 8, then heat up to 55-60°C, and keep it warm for 1 hour;
[0055] Step 5, the solution (c) is lowered to room temperature, and the pH of the solution (c) is adjusted to...
Embodiment 3
[0061] A preparation method of S-carboxymethyl-L-cysteine, characterized in that: comprising the following steps,
[0062] Step 1. Dissolve 1mol of L-cysteine hydrochloride monohydrate in 450mL of distilled water, place in ice brine to cool down to 0-5°C, and adjust the pH to 9-10 with 20% sodium hydroxide solution , to obtain solution (a);
[0063] Step 2: Add 1.4mol of chloroacetic acid into 400ml of distilled water, stir to dissolve, adjust the pH to 6-7 with 20% sodium hydroxide solution, and obtain solution (b);
[0064] Step 3. Under the protection of nitrogen, drop the solution (b) into the solution (a), and control the temperature in the ice-salt water to 0-5°C. After the dropping, the solution (c) is obtained;
[0065] Step 4: Use 20% sodium hydroxide solution to adjust the pH of the solution (c) to 8, then heat up to 55-60°C, and keep it warm for 1 hour;
[0066] Step 5, the solution (c) is lowered to room temperature, and the pH of the solution (c) is adjusted t...
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