Palmitoleic amide type water-based gas-phase antirust concentrate and preparation and use methods thereof
A palm oleic acid amide type and palm oleic acid amide technology are applied in the palm oleic acid amide water-based vapor phase anti-rust concentrate and its anti-rust application field, which can solve the surface defects of precision metal products of metal products, affect the surface quality and Accuracy, no gas phase anti-rust performance and other problems, to achieve the effects of excellent contact anti-rust ability, easy cleaning and easy operation
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[0025] Preparation of palmitoleic acid amide compound antirust agent:
[0026] Accurately weigh 30 grams of purified palmitoleic acid and add it to a four-necked flask filled with nitrogen, add 0.05 grams of catalyst PB, heat to 140 ° C under nitrogen atmosphere, and then slowly add maleic anhydride in batches under stirring conditions 12 grams to ensure that there is no white mist overflowing from the reaction bottle mouth, raise the temperature to 150°C, and keep it warm for 4 hours; lower the temperature of the reaction solution to 140±5°C, slowly add 17.1 grams of diethanolamine, 1.5 grams of KOH, and 17.1 grams of diethanolamine , raised the temperature to 170°C for 3 hours, slowly added 3.8 grams of diethanolamine for amination reaction for 0.5 hours, naturally cooled to below 100°C, added 28 grams of deionized water, and obtained palmitoleic acid amide compound rust inhibitor 1.
[0027] Accurately weigh 28 grams of purified palmitoleic acid and add it to a four-necked ...
Embodiment 1-6
[0029]
[0030]The preparation method of the water-based vapor-phase antirust concentrate listed in the examples in the table above comprises the following steps: adding water accounting for 80% of the total water into the reactor and heating it to 50-60°C; adding nitrobenzene according to the ratio Alcohol amine salt of formic acid to make it completely dissolve, then add palmitoleic acid amide compound antirust agent, hexamethylenetetramine, benzoic acid monoethanolamine to make it completely dissolve according to the ratio, and then add amino acid triazine antirust according to the ratio agent, vapor phase corrosion inhibitor, special water-based rust inhibitor, keep the solution at 50-60°C to dissolve it completely; add 20% of the total water, keep the solution at 50-60°C and stir for 2 hours, and then mix according to the stated ratio Add metal complexing agent, defoamer, and film-forming agent in sequence, continue to stir for 30 minutes, and cool down to room temperat...
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