Preparation method of modified polyacrylic resin and modified polyacrylic resin
A polyacrylic resin, modified technology, applied in the field of coatings, can solve problems such as mildew and bacterial growth
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Embodiment 1
[0020] Prepare a modified polyacrylic acid resin:
[0021] Step 1: Prepare the solution
[0022] Acrylic acid, methyl acrylate, and Manuka essential oil were measured at a volume ratio of 1:10:5 and mixed with ultrasonic waves, and recorded as solution A;
[0023] Take by weighing ammonium persulfate, chitosan hydrochloride and be made into aqueous solution, wherein, the concentration of described ammonium persulfate is 20g / L, and the concentration of described chitosan hydrochloride is 30g / L, denoted as B 1 solution;
[0024] The preparation concentration is the sodium lauryl sulfate aqueous solution of 25g / L, denoted as B 2 solution;
[0025] Step 2: Mix nano-silver, nano-titanium dioxide, and n-butyl acrylate according to the weight ratio of 0.4:0.2:20 with ultrasonic waves, and record it as liquid C;
[0026] Step 3: First add 12 volume parts of C liquid into the reaction kettle, then add 6 volume parts of A solution and 15 volume parts of B 2 Solution, mix evenly; he...
Embodiment 2
[0028] Prepare a modified polyacrylic acid resin:
[0029] Step 1: Prepare the solution
[0030] Measure acrylic acid, methyl acrylate, and Manuka essential oil at a volume ratio of 1:10:10 and mix them with ultrasonic waves, and record it as solution A;
[0031] Take by weighing ammonium persulfate, chitosan hydrochloride and be made into aqueous solution, wherein, the concentration of described ammonium persulfate is 18g / L, and the concentration of described chitosan hydrochloride is 25 / L, denoted as B 1 solution;
[0032] The preparation concentration is the sodium lauryl sulfate aqueous solution of 22g / L, denoted as B 2 solution;
[0033] Step 2: Mix nano-silver, nano-titanium dioxide, and n-butyl acrylate according to the weight ratio of 0.4:0.3:25 with ultrasonic waves, and record it as liquid C;
[0034] Step 3: First add 12 volume parts of C liquid into the reaction kettle, then add 8 volume parts of A solution and 20 volume parts of B 2 solution, mix evenly; heat...
Embodiment 3
[0036] Prepare a modified polyacrylic acid resin:
[0037] Step 1: Prepare the solution
[0038] Acrylic acid, methyl acrylate, and Manuka essential oil were measured at a volume ratio of 1:15:5 and mixed with ultrasonic waves, and recorded as solution A;
[0039] Take by weighing ammonium persulfate, chitosan hydrochloride and be made into aqueous solution, wherein, the concentration of described ammonium persulfate is 25g / L, and the concentration of described chitosan hydrochloride is 35g / L, denoted as B 1 solution;
[0040] The preparation concentration is the sodium lauryl sulfate aqueous solution of 25g / L, denoted as B 2 solution;
[0041] Step 2: Mix nano-silver, nano-titanium dioxide, and n-butyl acrylate according to the weight ratio of 0.6:0.3:25 with ultrasonic waves, and record it as liquid C;
[0042] Step 3: First add 15 parts by volume of solution C to the reactor, then add 6 parts by volume of solution A and 15 parts by volume of B 2 Solution, mix evenly; h...
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