Composite material based on agricultural wastes as well as preparation method and application of composite material
A technology for agricultural waste and composite materials, which is applied in the field of agricultural waste-based composite materials and their preparation, can solve the problems that hinder the formation of stable entangled networks of macromolecules, the difficulty of cellulose to form entangled structures, the destruction of multi-level structures and the Crystal structure and other problems, to achieve the effect of improving the degree of dissolution that is difficult to control, good interface compatibility, and good mechanical strength
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[0057] Example 1
[0058] The selected agricultural waste material is wheat straw with a cellulose mass fraction of about 56%, and the selected cellulose material is wood pulp with a degree of polymerization of about 1300. Weigh 19.2 g of dried AMIMCl ionic liquid and 0.64 g of dried wheat straw, stir and dissolve at 120° C., after about 120 minutes, a uniform brown solution is formed. 0.16g of dried wood pulp was added to the solution, and the mixture was further stirred and dissolved at 80°C. After about 60 minutes, a uniform brown wheat straw / wood pulp / AMIMCl mixed solution was obtained. Observe with a polarizing microscope. Black, indicating that the wheat straw cellulose and wood pulp are almost completely dissolved. The mass percentage of wheat straw in the wheat straw / wood pulp / AMIMCl mixed solution is 3.2%, and the mass ratio of wood pulp to wheat straw is 1:4. Spread the mixed solution of wheat straw / wood pulp / AMIMCl evenly on the surface of the glass plate, and put it...
Example Embodiment
[0061] Example 2
[0062] The selected agricultural waste material is rice straw with a cellulose mass fraction of about 45%, and the selected cellulose material is wood pulp with a degree of polymerization of about 1300. Weigh 9.2g of dried AMIMCl ionic liquid, weigh 0.64g of dried rice straw and 0.16g of dried wood pulp, stir and dissolve together at 120℃, about 180 minutes later, a uniform brown rice straw / wood pulp is obtained The mixed solution of meal / AMIMCl is black when observed with a polarizing microscope, indicating that the rice straw cellulose and wood pulp are almost completely dissolved. The mass percentage of rice straw in the rice straw / wood pulp / AMIMCl mixed solution is 6.4%, and the mass ratio of wood pulp to rice straw is 1:4. The rice straw / wood pulp / AMIMCl mixed solution was evenly spread on the surface of the glass plate, and the mixture of AMIMCl and water was used as the coagulation bath. In the coagulation bath, the mass ratio of water to AMIMCl was 1:0...
Example Embodiment
[0063] Example 3
[0064] The selected agricultural waste material is corn stalks with a cellulose mass fraction of about 52%, and the selected cellulose raw material is wood pulp with a degree of polymerization of about 1300. Weigh 6.0g of dried BMIMAc ionic liquid and 0.64g of dried corn stalks and stir to dissolve them at 120°C. After about 120 minutes, a uniform brown solution is formed. The field of view is black when observed with a polarizing microscope, indicating that the corn stalk cellulose Almost completely dissolved. Weigh 3.2g of dried BMIMAc ionic liquid and 0.16g of dried wood pulp, stir and dissolve at 80°C. After about 60 minutes, a uniform yellow transparent solution is formed. The field of view is black when observed with a polarizing microscope, indicating that the wood pulp The meal is almost completely dissolved. The above-mentioned corn stover / BMIMAc solution and wood pulp / BMIMAc solution were mixed, and stirred at 80°C until the mixture was evenly mixed...
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