A kind of alloy-reinforced titanium carbonitride-based composite material and preparation method thereof
A technology of titanium carbonitride-based and composite materials, applied in the field of cemented carbide materials, can solve the problems of no significant improvement in material strength, poor grain size uniformity, and poor interfacial bonding. Excellent degree of degree, the effect of inhibiting agglomeration
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Embodiment 1
[0044] A preparation method of an alloy-strengthened titanium carbonitride-based composite material is carried out as follows:
[0045] Preparation of Alloy Phase Composite Powder
[0046] (1) Weigh raw materials: Weigh the corresponding cobalt oxide powder, chromium oxide, cerium oxide, niobium oxide, Zirconium (oxide purity greater than 99%);
[0047] (2) Mechanical impact mill crushing and mixing: put the weighed oxide powder and TiCN balls into a stirring ball mill tank, add absolute ethanol in an amount of 0.05L / kg, and then carry out mechanical impact crushing and mixing to form a wet slurry. The ball-to-material ratio is 3:1, the stirring ball milling speed is 300 rpm, and the crushing and mixing time is 48 hours;
[0048] (3) High-pressure spray drying: sieve the mixed wet slurry to remove balls, atomize the slurry at a pressure of 15 MPa, mix and dry the atomized slurry with hot air at 60°C to form a micro-nano alloy mixture powder;
[0049] (4) Nitrogen hydrogena...
Embodiment 2
[0055] A preparation method of an alloy-strengthened titanium carbonitride-based composite material is carried out as follows:
[0056] Preparation of Alloy Phase Composite Powder
[0057] (1) Weigh raw materials: Weigh the corresponding cobalt oxide powder, chromium oxide, cerium oxide, niobium oxide, Zirconium (oxide purity greater than 99%);
[0058] (2) Mechanical impact mill crushing and mixing: Put the weighed oxide powder and TiCN balls into a stirring ball mill tank, add absolute ethanol in an amount of 0.1L / kg, and then carry out mechanical impact crushing and mixing to form a wet slurry. The ball-to-material ratio is 5:1, the stirring ball milling speed is 500 rpm, and the crushing and mixing time is 36 hours;
[0059] (3) High-pressure spray drying: sieve the mixed wet slurry to remove balls, atomize the slurry at a pressure of 2 MPa, mix and dry the atomized slurry with hot air at 80°C to form a micro-nano alloy mixture powder;
[0060] (4) Nitrogen hydrogenati...
Embodiment 3
[0066] A preparation method of an alloy-strengthened titanium carbonitride-based composite material is carried out as follows:
[0067] Preparation of Alloy Phase Composite Powder
[0068] (1) Weigh raw materials: Weigh the corresponding cobalt oxide powder, chromium oxide, cerium oxide, niobium oxide, oxide Zirconium (oxide purity greater than 99%);
[0069] (2) Mechanical impact mill crushing and mixing: put the weighed oxide powder and TiCN balls into a stirring ball mill tank, add absolute ethanol in an amount of 0.08L / kg, and then carry out mechanical impact crushing and mixing to form a wet slurry. The ball-to-material ratio is 4:1, the stirring ball milling speed is 400 rpm, and the crushing and mixing time is 40 hours;
[0070] (3) High-pressure spray drying: sieve the mixed wet slurry to remove balls, atomize the slurry under a pressure of 10 MPa, mix and dry the atomized slurry with hot air at 70°C to form micro-nano alloy mixed powder ;
[0071] (4) Nitrogen hyd...
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