Carbon disulfide removal method based on low-temperature plasma reactor and coupling catalyst
A low-temperature plasma and low-temperature plasma technology, applied in the directions of heterogeneous catalyst chemical elements, separation methods, chemical instruments and methods, etc., can solve the problems of reduced carbon disulfide catalytic removal effect, short catalyst activity time, and poor industrial applicability, etc. To achieve the effect of no attenuation of removal effect, stable catalytic performance and long-lasting catalytic effect
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Embodiment 1
[0039] A method for removing carbon disulfide based on a low-temperature plasma reactor and a coupled catalyst, comprising modified powder preparation, modified powder spraying, coupled catalyst preparation, and low-temperature plasma treatment.
[0040] The preparation of the modified powder includes: pretreatment, shearing, calcining and loading.
[0041] For the pretreatment, 30-mesh titanium dioxide powder was put into 5 times the volume of 3% zirconium nitrate solution, the stirring speed was 60 RPM, the stirring time was 20 minutes, and then stood still for 30 minutes. Then drop in 5% phosphoric acid, stir for 1h, and filter out the solid powder.
[0042]The weight ratio of titanium dioxide powder: phosphoric acid is 1:0.08.
[0043] For the shearing, high-speed shearing is performed on the solid powder at a shearing speed of 6000 RPM until the solid particle diameter D50 is 90 μm.
[0044] For the calcination, under the protection of an inert gas, the sheared solid po...
Embodiment 2
[0060] A method for removing carbon disulfide based on a low-temperature plasma reactor and a coupled catalyst, comprising modified powder preparation, modified powder spraying, coupled catalyst preparation, and low-temperature plasma treatment.
[0061] The preparation of the modified powder includes: pretreatment, shearing, calcining and loading.
[0062] For the pretreatment, 35-mesh titanium dioxide powder was put into 5 times the volume of 4% zirconium nitrate solution, the stirring speed was 100 RPM, the stirring time was 20 minutes, and then stood still for 30 minutes. Then drop in 7% phosphoric acid, stir for 1h, and filter out the solid powder.
[0063] The ratio of titanium dioxide powder: phosphoric acid in parts by weight is 1:0.11.
[0064] For the shearing, high-speed shearing is performed on the solid powder at a shearing speed of 7000 RPM until the solid particle diameter D50 is 100 μm.
[0065] For the calcination, under the protection of an inert gas, the s...
Embodiment 3
[0081] A method for removing carbon disulfide based on a low-temperature plasma reactor and a coupled catalyst, comprising modified powder preparation, modified powder spraying, coupled catalyst preparation, and low-temperature plasma treatment.
[0082] The preparation of the modified powder includes: pretreatment, shearing, calcining and loading.
[0083] For the pretreatment, 40-mesh titanium dioxide powder was put into 5 times the volume of 5% zirconium nitrate solution, the stirring speed was 120 RPM, the stirring time was 30 minutes, and then stood still for 30 minutes. Then drop in 7% phosphoric acid, stir for 1h, and filter out the solid powder.
[0084] The titanium dioxide powder: the weight ratio of phosphoric acid is 1: 0.17.
[0085] For the shearing, high-speed shearing is performed on the solid powder at a shearing speed of 7500 RPM until the solid particle diameter D50 is 120 μm.
[0086] For the calcination, under the protection of an inert gas, the sheared ...
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