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120 results about "Carbon sulfide" patented technology

Carbon sulfide may refer to: Carbon disulfide Carbon monosulfide Carbon subsulfide

Method for preparing lithium sulfide at low temperature by microwave molten salt assisted carbon disulfide-lithium salt reaction

The invention relates to a method for preparing lithium sulfide at low temperature by microwave molten salt assisted carbon disulfide-lithium salt reaction, and belongs to the technical field of key materials of lithium-sulfur batteries and solid-state batteries. The technical problems of high energy consumption, difficulty in inhibiting by-products, insufficient purity and crystal phase stability, difficulty in continuous amplification and the like in the existing lithium sulfide preparation process are solved. Comprising the following steps: step 1, performing crushing, screening and grading treatment on lithium source powder; step 2, placing the treated lithium source powder and molten salt in a closed reactor, and introducing CS2 in a gas or liquid form; 3, applying microwave radiation, and reacting at a gas-solid-liquid multiphase interface to generate lithium sulfide; and 4, cooling the material after the reaction to room temperature, separating and recovering the fused salt to obtain the lithium sulfide powder. The method is low in reaction temperature, low in energy consumption, high in reaction rate, high in product purity and suitable for continuous and industrial production.
Owner:山西铁峰化工有限公司

High-strength energetic compound based on polydopamine and thiourea polymer and preparation method

PendingCN120208737ANon-explosive fillers/gelling/thickening agentsNitrated aromatic explosive compositionsPolymer scienceExplosive Agents
The invention discloses a high-strength energetic compound based on a polydopamine and thiourea polymer and a preparation method of the high-strength energetic compound, and the energetic compound is composed of energetic crystal 1, 3, 5-triamino-2, 4, 6-trinitrobenzene, the polydopamine and the thiourea polymer. The preparation method comprises the following steps: modifying an energetic crystal 1, 3, 5-triamino-2, 4, 6-trinitrobenzene through polydopamine in advance; the polythiourea is obtained through reaction of 2, 2 '-(ethylene dioxygen) diethylamine, carbon disulfide and trimethylolpropane tripolypropylene glycol ether, and the addition amount is 2.5 wt.%-10 wt.%; and mixing the two components by a kneading method, and drying to obtain the energetic compound. The obtained compound has the characteristics of strengthening and toughening, the Brazil mechanical strength reaches 14.76 MPa, and the fracture strain reaches 0.474%. By introducing polyphenol polydopamine and polythiourea to achieve a synergistic effect, the mechanical property of the explosive is greatly improved, and a technical support can be provided for the application of the explosive; meanwhile, the preparation method is simple, mild in reaction condition and easy for large-scale production.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

Lactobacillus brevis SMF L6 for improving characteristic flavor of fermented fish and application of lactobacillus brevis SMF L6

The invention discloses a lactobacillus brevis SMF L6 strain for improving the characteristic flavor of fermented fish and application thereof, and belongs to the technical field of aquatic product processing. According to the method disclosed by the invention, low-temperature fermentation is carried out by utilizing a sake lactobacillus wide cloth SMF L6 direct vat set fermentation inoculant to regulate and control the flavor; the method can effectively promote the production of flavor substances such as n-hexyl alcohol, eudesmol, 2-ethylhexyl alcohol, 4-platycladi alcohol, linalool, 4-terpene alcohol, alpha-terpilenol, piperonone, beta-myrcene, alpha-terpinene, D-limonene, beta-phellandrene, gamma-terpinene and the like in the fermented fish. The content of pungent smell and fishy smell substances such as acetic acid, p-xylene, o-xylene, trimethylamine, methyl mercaptan and carbon disulfide is reduced.
Owner:INST AGRO PROD PROCESSING ANHUI ACADEMY AGRI SCI

Heating furnace for carbon disulfide production

ActiveCN120022848ACarbon disulfideOxy/sulfo carbidesCombustion chamberCarbon sulfide
The invention relates to a heating furnace for carbon disulfide production, and relates to the technical field of carbon disulfide production, the heating furnace comprises a furnace body comprising an outer furnace box body, an inner furnace box body and a supporting pipe; the sulfur supply assembly comprises a combustion chamber, a liquid sulfur pipe and a spray head; the methane supply assembly comprises a methane gas pipe, a transfer piece, a communicating pipe and a mixing plate; the mixing assembly comprises a rotating blade, a driving fan blade, a bevel gear ring, a bevel gear and a flow guide fan blade; the exhaust assembly comprises a first exhaust pipe, a second exhaust pipe, a third exhaust pipe and a fourth exhaust pipe; by uniformly introducing gaseous sulfur and methane gas into the inner furnace box body and stirring and turning the gaseous sulfur and methane gas through the mixing plate, sulfur and methane are easily and uniformly mixed, the yield of carbon disulfide can be increased, and efficient production of carbon disulfide is facilitated. The method has the effect of improving the mixing degree of sulfur and methane.
Owner:SHANXI XINTU CHEM CO LTD

Preparation method and application of modified PVC adsorbent for gold extraction of carbonaceous gold ore

The invention provides a preparation method and application of a modified PVC adsorbent for gold extraction of carbonaceous gold ore, and belongs to the technical field of organic polymer materials and resource utilization. Based on construction of a hydroxylation-xanthate esterification reaction and bifunctional adsorption sites, a series of chemical modification paths of acetate nucleophilic substitution-hydrolysis-carbon disulfide alkali treatment are established, and xanthate functional groups with high reaction activity are accurately constructed on an inert PVC framework. Sulfur atoms in xanthate groups of the modified PVC are excellent electron donors and can generate strong chemical adsorption with metal impurities or polar sites on the surface of carbon, meanwhile, Van der Waals interaction between a main chain of the modified PVC and the carbon is reserved, and unmodified PVC or single hydroxylated PVC does not have the synergism of chemical adsorption and physical adsorption, so that the modified PVC can be used for preparing the carbon-modified PVC composite material, and the carbon-modified PVC composite material can be used for preparing the carbon-modified PVC composite material. And leap-type improvement of the adsorption capacity and selectivity of organic carbonaceous in minerals is realized.
Owner:CHANGCHUN GOLD RES INST

Rapid enrichment equipment for light hydrocarbon oil, medium hydrocarbon oil and crude phenol in medium and low temperature coal tar

ActiveCN223047456UTar working-up by distillationTar working-up by solvent extractionCarbon sulfidePhenol
The utility model provides rapid enrichment equipment for light hydrocarbon oil, medium hydrocarbon oil and crude phenol in medium and low temperature coal tar, which adopts five solvent storage tanks to store and take recovered solvents (acetone, carbon disulfide, petroleum ether, methanol and acetonitrile) in each step so as to be recycled in cycles; carrying out deliming treatment on the medium-low temperature coal tar by using an acetone / carbon disulfide mixed solvent; petroleum ether and methanol, petroleum ether and acetonitrile, and methanol and carbon disulfide are used for carrying out step-by-step double-solvent layered extraction on the de-ashed tar. The device disclosed by the utility model realizes rapid enrichment of target components in medium and low temperature coal tar, provides extract oil which is simple in composition and easy to process for subsequent secondary upgrading, and solves the problems of high energy consumption, difficulty in large-scale commercialization and the like in the prior art.
Owner:YULIN UNIV +1

Mechanically stabilized dual-sourced sulfur electrodes

PendingUS20250259993A1Active material electrodesSulfur electrodeMolecular adsorption
Described are electrodes composed of a carbonaceous matrix with sulfurized carbon particles. These particles feature sulfur atoms covalently bonded to carbon atoms, internal pores, and sulfur molecules both adsorbed and contained within these pores. The structure includes electrically conductive filaments and particle agglomerates fused to a subset of these filaments, which possess specific length and width dimensions and extend as anchor segments to connect adjacent particles. Additionally, the electrode incorporates yarns made from a second subset of filaments, characterized by lengths and widths exceeding those of the initial filaments, spanning between the particle agglomerates. The resultant electrode shows unique electrochemical behavior that enhances its energy density over other carbonaceous sulfurized carbon materials.
Owner:ZETA ENERGY CORP

Efficient gas-solid reaction process and integrated industrial system

PendingCN120885143ACarbon disulfideChemical/physical processesGas solidSolid reaction
The invention relates to an efficient gas-solid reaction process and an integrated industrial system, and belongs to the technical field of gas-solid reaction in chemical production. The process flow comprises the following steps: crushing and drying coke by a pulverizing unit, preheating the coke and sulfur steam to be greater than or equal to 550 DEG C, and jointly entering a gas-solid reaction unit; and the product enters a gas-solid separation unit, is subjected to two-stage gas-solid separation at a high temperature of 450-680 DEG C and a low temperature of less than or equal to 200 DEG C, and then is The integrated industrial system based on the efficient gas-solid reaction process is applied to carbon disulfide production through a coke method, the problems of external heat supply and byproduct generation control in the reaction process of coke and sulfur are solved, and the system is simple in process chain, easy and convenient to operate, compact in structure and suitable for continuous and closed carbon disulfide production requirements through the coke method.
Owner:BEIJING HANGHUA ENERGY SAVING ENVIRONMENTAL PROTECTION TECH CO LTD

A method for recycling a promoter m tar

The present application belongs to the technical field of fine chemical industry, and relates to a recycling method of accelerator M tar. In the waste M tar produced in M production, a catalyst is added, high-temperature decomposition is carried out under nitrogen protection, and recycled raw materials aniline, carbon disulfide and intermediate benzothiazole and the like are obtained, most of which are recycled. The present application adopts common equipment and unit operations, the catalyst can be reused, and the treatment of production waste is easy to realize industrial production.
Owner:CHINA PETROLEUM & CHEMICAL CORP +2

Method for removing sulfur-containing compounds in C3 fraction of cracking gas prepared from crude oil

The invention discloses a method for removing sulfur-containing compounds in a crude oil-prepared cracked gas C3 fraction. The method comprises the following steps: contacting the crude oil-prepared cracked gas C3 fraction with a supported desulfurizer, wherein the load type desulfurizing agent comprises a carrier and a main active component loaded on the carrier; the main active component comprises alkali metal and / or alkaline earth metal; the carrier comprises elementary substances Ag, Ag2O, elementary substances Re and ReOx; reOx is a mixture of a plurality of Re oxides, x = n / 2, and n is 4, 6 or 7; the molar content of the elementary substance Re accounts for 30-45% of the total molar weight of Re in the carrier. The method provided by the invention can effectively remove low-carbon thioether and / or low-carbon mercaptan in the C3 fraction of the crude oil-prepared pyrolysis gas, has the advantages of low removal temperature, simple process, no additional reaction, no influence on downstream hydrogenation and separation processes, and energy consumption saving, and the desulfurizer can be repeatedly regenerated and used, and has long-period stable operation capability.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Quinazoline-4-one compounds containing 1,2,4-triazole [3,4-b] [1,3,4] thiadiazole and preparation and use thereof

The invention discloses a quinazoline-4-one compound containing 1,2,4-triazole [3,4-b] [1,3,4] thiadiazole, a preparation method thereof and antibacterial activity thereof. The compound is represented by general formula (I), and quinazoline-4-one, 1,2-dibromoethane, methyl 4-piperidinate, 80% hydrazine hydrate, potassium hydroxide, carbon disulfide and different aromatic acids are used as raw materials to prepare the target compound through a five-step reaction. The invention introduces an active 1,2,4-triazole [3,4-b] [1,3,4] thiadiazole unit into the quinazoline-4-one structure, and synthesizes a series of quinazoline-4-one compounds containing 1,2,4-triazole [3,4-b] [1,3,4] thiadiazole units, and the compounds have good antibacterial activity.
Owner:GUIZHOU UNIV

High-purity hydrogen sulfide purification process and system adopting two-stage low-temperature condensation coupling compression separation

The invention belongs to the technical field of chemical separation, and discloses a two-stage low-temperature condensation coupling compression separation high-purity hydrogen sulfide purification process and system. The system consists of a two-stage low-temperature condensation unit, a hydrogen sulfide compression unit and a hydrogen sulfide collection unit, the two-stage low-temperature condensation unit comprises a hydrogen sulfide liquid separation tank, a hydrogen sulfide low-temperature cooler, a hydrogen sulfide low-temperature liquid separation tank, a hydrogen sulfide heat exchanger and a hydrogen sulfide saline water liquid separation tank. Hydrogen sulfide raw material gas containing carbon disulfide impurities is sequentially introduced into a two-stage low-temperature condensation unit, carbon disulfide is liquefied and separated out preferentially, low-temperature water is adopted in the first stage, and materials subjected to cryogenic compression throttling are adopted in the second stage for heat exchange; pressurizing and compressing the primarily purified hydrogen sulfide gas-phase component, and then condensing and separating to remove trace carbon disulfide and recover cold energy, thereby finally obtaining the high-purity hydrogen sulfide with the purity of more than or equal to 99.95%. According to the invention, a low-temperature two-stage low-temperature condensation-pressurized compression condensation coupling separation technology is adopted, and deep removal of carbon disulfide is realized under the condition that a third component is not introduced.
Owner:新疆兴发化工有限公司

Microreactor device for preparing liquid isopropyl xanthate

The invention relates to the technical field of medicament synthesis, and particularly discloses a microreactor device for preparing liquid isopropyl xanthate, the microreactor device comprises a workbench, the top of the workbench is fixedly connected with a mixing tank through a support, and the two sides and one end of the mixing tank are communicated with feeding pipes; the end, away from the mixing tank, of the feeding pipe communicates with a discharging port of a metering pump, the bottom of the metering pump is fixedly connected with the top of the workbench, the inner wall of the mixing tank is rotationally connected with a mixing device, and the part, located below the mixing tank, of the top of the workbench is fixedly connected with a first motor. According to the microreactor device for preparing the liquid isopropyl xanthate, the mixing device is arranged, so that the mixing efficiency of isopropanol, carbon disulfide and liquid caustic soda before reaction can be improved, and the dosing mechanism is arranged, so that the mixing efficiency of isopropanol, carbon disulfide and liquid caustic soda before reaction can be improved. Therefore, the reaction efficiency of the mixed solution of isopropanol, carbon disulfide and caustic soda liquid during reaction can be improved.
Owner:NORTH MINING CHEM TECH (CANGZHOU) CO LTD

Methods for reducing formation of carbon disulfide in steam cracking processes to produce olefins

Methods for producing olefins through hydrocarbon steam cracking include passing a hydrocarbon feed that includes one or more hydrocarbons to a hydrocarbon cracking unit and passing one or more sulfur-containing compounds to the hydrocarbon cracking unit. The sulfur-containing compounds include at least hydrogen sulfide gas, and a flow rate of the sulfur-containing compounds to the hydrocarbon cracking unit is sufficient to produce a molar concentration of elemental sulfur in the hydrocarbon cracking unit of from 10 ppm to 200 ppm. The methods include cracking the hydrocarbon feed in the hydrocarbon cracking unit to produce a cracker effluent and contacting the cracker effluent with a quench fluid in a quench unit to produce at least a cracked gas and a first pygas. The first pygas has a concentration of carbon disulfide less than 50 ppmw based on the total mass flow rate of the first pygas.
Owner:DOW GLOBAL TECHNOLOGIES LLC

Viscose staple fiber cooking device

The invention relates to the technical field of viscose staple fiber processing, in particular to a viscose staple fiber cooking device which comprises a fiber feeding groove frame, a dispersing groove and a cooking groove are formed above the fiber feeding groove frame, the connecting position of the dispersing groove and the cooking groove is through, a dispersing guide plate and a distribution assembly are arranged in the dispersing groove, and the dispersing guide plate is connected with the cooking groove. The device has the beneficial effects that the dispersing tank and the cooking tank are designed, viscose staple fibers are cooked through steam, the fibers are carded in the cooking process in cooperation with the fixing frame, meanwhile, the broken staple fibers are intercepted, blockage and accumulation are avoided, the fibers can be fully cooked and loosened through sprayed steam, residual CS2 is fully cooked and removed, and the quality of the viscose staple fibers is improved. And the space above the cooking tank is covered by the steam rising area sealing cover, and rising steam carrying carbon disulfide can be connected with a condensation recovery separation workshop through a carbon disulfide recovery pipe, so that the carbon disulfide is effectively recovered, the environmental pollution is reduced, and the resource utilization rate is improved.
Owner:SAIDELI (JIANGSU) FIBER CO LTD

Carbon disulfide cooling system

The utility model provides a carbon disulfide cooling system. The carbon disulfide cooling system comprises a first-stage condenser, a second-stage condenser and a third-stage condenser which are arranged at the gas phase outlet end of a sulfur and carbon catcher. The liquid phase output ends of the first-stage condenser and the second-stage condenser are connected with a crude carbon disulfide buffer tank, and the liquid phase output end of the third-stage condenser is connected with a reflux buffer tank. The output end of the reflux buffer tank is connected with a sulfur capture reflux pump, and the sulfur capture reflux pump is connected with the liquid phase input end of the sulfur and carbon capture device through a reflux pipeline. And the outlet end of the crude carbon disulfide buffer tank is provided with a liquid phase recovery pipeline communicated with the separation tower. A material inlet is formed in the side part of the sulfur and carbon capturing device, and external mixed gas enters from the material inlet. A material outlet is also formed in the bottom of the sulfur and carbon capturing device and is used for discharging excessive sulfur. According to the utility model, the energy consumption of the refrigerating machine required by the subsequent three-stage condenser is reduced, the temperature of the gas phase outlet of the sulfur and carbon capturing device is also reduced, and the cooling recovery of CS2 is more facilitated.
Owner:山西铁峰化工有限公司

Monomer polymerization with sulfur and carbon nanotubes

PCT designated stageWO2026064449A9Electrode thermal treatmentMicroscopic fiber electrodesPolymer scienceAcrylonitrile
A method for producing sulfurizcd-carbon cathode materials for electrochemical cells involves mixing carbon nanofibers, sulfur, and a monomer (e.g., acrylonitrile) to form a mixture, polymerizing the monomer to encapsulate the nanofibers and sulfur within a polymer matrix (e.g., polyacrylonitrile), and pyrolyzing the matrix to chemically bond carbon from the polymer to the nanofibers and sulfur, yielding sulfurized-carbon particles fused to the nanofibers. The pyrolyzed material forms a fluffy powder that is compressed into a free-standing dry film, wherein the nanofibers and longer nanofiber yarns create a three-dimensional conductive network enhancing mechanical stability and electrical conductivity. The film is laminated to a current collector to form a cathode. Optional pore- loading with molecular sulfur improves capacity and cycle life, achieving >70% sulfur utilization without wet processing solvents.
Owner:ZETA ENERGY CORP

Methods and systems for generating carbon disulfide

PCT designated stageWO2026055366A1Carbon disulfideThiol preparationCarbon sulfideMethane
The present application pertains to a method of making carbon disulfide. The method comprises reacting methane and sulfur under conditions sufficient to produce carbon disulfide, hydrogen disulfide, and heat. At least a portion of the produced hydrogen disulfide is reacted with methane under conditions sufficient to produce a mixture comprising carbon disulfide and hydrogen. Advantageously, at least a portion of the heat from reacting methane and sulfur is employed in the reacting of at least a portion of the produced hydrogen disulfide with methane.
Owner:CHEVRON USA INC +5

Production device for synthesizing TBTD in one step

The utility model provides a production device for synthesizing TBTD in one step, which comprises a reaction kettle, a di-n-butylamine adding pipeline, a hydrogen peroxide adding pipeline, a carbon disulfide adding pipeline, a soft water adding pipeline, a carbon disulfide gas discharging pipeline and a nitrogen pipeline are arranged at the top end of the reaction kettle, and the carbon disulfide gas discharging pipeline is connected with a gas inlet of a condenser. A condensate outlet pipeline of the condenser is connected with a carbon disulfide receiving tank, a bottom outlet pipeline of the carbon disulfide receiving tank is connected with a carbon disulfide adding pipeline, and the carbon disulfide adding pipeline is further connected with a carbon disulfide transfer pump; hydrogen peroxide is adopted as an oxidizing agent, so that high-salinity wastewater discharge is reduced; the reaction liquid is washed with water for many times to remove residual alkali liquor and byproducts, water is used as a solvent to replace a traditional methanol / ethanol system, and emission of VOCs is reduced; the metering pump is used for dropwise adding materials, so that automatic sealing feeding is realized, and harm to bodies of workers is reduced; carbon disulfide is recycled for next reaction, so that the material loss is reduced, and the pollution problem in the subsequent treatment process is reduced.
Owner:CHONGQING LIFE TECHNOLOGY & NEW MATERIALS IND GROUP CO LTD

Method for preparing light calcium carbonate and co-producing sulfuric acid by decomposing ardealite

This invention relates to the field of phosphogypsum resource utilization, specifically disclosing a method for preparing light calcium carbonate and co-producing sulfuric acid by decomposing phosphogypsum. The method includes the following steps: adding a deagglomerating agent to phosphogypsum, followed by flotation and water washing to obtain purified phosphogypsum; drying and heating the purified phosphogypsum in a preheating furnace; mixing the dried phosphogypsum with carbon sulfide and adding it to a first-stage airlift circulating reactor, while introducing sulfur gas; conveying the reacted material to a second-stage airlift circulating reactor, where the reaction yields calcium oxide and a mixture of sulfur dioxide and carbon dioxide; catalytically oxidizing and absorbing the carbon dioxide mixture to obtain sulfuric acid and carbon dioxide gas; dissolving calcium oxide in water and introducing carbon dioxide gas to obtain a calcium carbonate suspension; filtering and drying the calcium carbonate suspension to obtain light calcium carbonate. This invention solves the problems of low purity and high decomposition temperature of calcium oxide products in existing technologies, achieving closed-loop material circulation and full component utilization.
Owner:YUNNAN PHOSPHATE CHEM GROUP CORP

A star-shaped block copolymer for low-rank coal slurry and preparation method thereof

The invention discloses a star-shaped block copolymer for low-rank coal slurry and a preparation method thereof. The method comprises the following steps: uniformly mixing tripotassium phosphate, 1-butyl mercaptan, carbon disulfide and acetone, heating the mixture to room temperature and keeping the temperature, adding 1,3,5-tri(bromomethyl)benzene at 5 to 0°C, stirring the mixture, heating the mixture to room temperature and keeping the temperature, separating the product to obtain an intermediate product I; subjecting the intermediate product I, an initiator, styrene and dioxane to a RAFT controlled radical polymerization reaction under vacuum, and then removing unreacted monomers to obtain M n =10000-20000 intermediate product II; the intermediate product II, initiator, methoxy polyethylene glycol acrylate and dioxane are subjected to RAFT controlled radical polymerization under vacuum, and then the unreacted monomer is removed to obtain M n = Star-shaped block copolymer with a molecular weight of 20,000 to 40,000.
Owner:SHAANXI UNIV OF SCI & TECH

Optimized natural gas / sales gas / sour gas reforming employing a novel catalytic process at the industrial scale

PCT designated stageWO2025160160A1Carbon disulfideHydrogen separation at low temperatureLiquid hydrogenIndustrial scale
A system for hydrogen production including a first separation system (10), a first purification unit (17), a second purification unit (19), an oxygen scavenger (25), a catalytic reactor (29), a second separation system (33), and a liquefier (39). A method for hydrogen production including separating oxygen-containing components from a feed (5) also containing hydrogen sulfide and methane. The method further includes separating the hydrogen sulfide from the methane and feeding the hydrogen sulfide (13) to a first purification unit (17). The method includes feeding the methane (15) to a second purification unit (19). The method further includes feeding the purified hydrogen sulfide and methane to an oxygen scavenger unit (25) to remove residual oxygen before reacting the two streams in a catalytic reactor (29). The method includes separating the gaseous hydrogen and liquid carbon disulfide (31) exiting the catalytic reactor (29) and then purifying and liquefying the gaseous hydrogen stream (34) to produce a purified liquid hydrogen stream (41).
Owner:SAUDI ARABIAN OIL CO +1

Continuous reaction system and method for co-producing solid sodium ethyl xanthate and liquid sodium ethyl xanthate

The invention discloses a continuous reaction system and method for co-producing solid and liquid sodium ethyl xanthate, and relates to the technical field of sodium ethyl xanthate production. The system comprises a reaction kettle, a stirring motor, a raw material discharging pipe, an alkali liquor discharging pipe, a discharging pipe, a circulating liquid outlet pipeline, a centrifugal machine, a drying machine, a xanthate storage tank, a plurality of groups of control valves and a plurality of groups of backflow pipelines, which form a closed-loop reaction and separation system. The method comprises the following steps: feeding ethanol, carbon disulfide and caustic soda liquid with the concentration of more than or equal to 40% according to a molar ratio of 1: (0.9-1.2): (1.0-1.2), carrying out an initial reaction at 30-36 DEG C for 2.5-4.5 h, carrying out circulating separation, mother liquor recycling and continuous alkali supplementation to realize continuous production, and simultaneously producing liquid sodium ethyl xanthate and solid xanthate obtained by drying at 40-60 DEG C for 0.5-2.5 h. According to the method, reaction balance is promoted through high-concentration alkali, the raw material conversion rate is increased, the problem of solid precipitation is solved through the process of reaction-separation-recycling, product diversification is achieved, batch reaction is upgraded to continuous production, the productivity and stability are improved, and different market requirements are met.
Owner:JINCHUAN GROUP CO LTD +1

A heating furnace for carbon disulfide production

ActiveCN120022848BCarbon disulfideOxy/sulfo carbidesCombustion chamberCarbon sulfide
This application relates to a heating furnace for carbon disulfide production, belonging to the technical field of carbon disulfide production. It includes: a furnace body, including an outer furnace box body, an inner furnace box body and support pipes; a sulfur supply assembly, including a combustion chamber, a liquid sulfur pipe and a nozzle; a methane supply assembly, including a methane gas pipe, a transfer piece, a connecting pipe and a mixing plate; a mixing assembly, including a rotating blade, a driving fan blade, a bevel gear ring, a bevel gear and a guiding fan blade; an exhaust assembly, including a first discharge pipe, a second discharge pipe, a third discharge pipe and a fourth discharge pipe; by uniformly introducing gaseous sulfur and methane gas into the inner furnace box body and stirring and turning the gaseous sulfur and methane gas through the mixing plate, the sulfur and methane are easily mixed evenly, which can increase the output of carbon disulfide and is conducive to the efficient production of carbon disulfide. This application has the effect of improving the mixing degree of sulfur and methane.
Owner:SHANXI XINTU CHEM CO LTD

Tetraethylthiuram disulfide production reaction device

The utility model discloses a tetraethylthiuram disulfide production reaction device which comprises a reaction kettle, a stirring structure is arranged in the reaction kettle, a jacket is arranged outside the reaction kettle, and an ethanol solution adding pipeline, a diethylamine adding pipeline, a hydrogen peroxide adding pipeline and a carbon disulfide adding pipeline are arranged at the top end of the reaction kettle. The ethanol solution adding pipeline is connected with a liquid outlet of the ethanol solution static mixer, an ethanol inlet pipeline and a soft water inlet pipeline are arranged on the ethanol solution static mixer, and the carbon disulfide gas discharging pipeline is connected with a gas inlet of the condenser; a condensate outlet pipeline of the condenser is connected with a carbon disulfide receiving tank, a bottom outlet pipeline of the carbon disulfide receiving tank is connected with a carbon disulfide adding pipeline, the carbon disulfide adding pipeline is further connected with a carbon disulfide transfer pump, and a carbon disulfide metering pump is arranged on the carbon disulfide adding pipeline. One-step safe production of tetraethylthiuram disulfide can be realized, and the production efficiency is improved.
Owner:CHONGQING LIFE TECHNOLOGY & NEW MATERIALS IND GROUP CO LTD

Quinazolinone derivative containing oxadiazole unit as well as preparation method and application of quinazolinone derivative

The invention belongs to the field of pesticides, and discloses a compound with a structure as shown in a formula I. A preparation method of the compound comprises the following steps: reacting anthranilic acid with formamide, and then reacting with 1, 4-dibromobutane under the action of sodium hydride to obtain 3-(4-bromobutyl) quinazoline-4 (3H)-ketone; then, phenylacetic acid sequentially reacts with methyl alcohol, hydrazine hydrate, potassium hydroxide, carbon disulfide and 3-(4-bromobutyl) quinazoline-4 (3H)-ketone, and the quinazolinone derivative containing the oxadiazole unit is obtained. The quinazolinone derivative containing the oxadiazole unit is a novel compound, has an inhibiting effect on fusarium graminearum, rhizoctonia solani and botrytis cinerea, and can be used for preventing and treating plant diseases caused by fungi.
Owner:JIANGSU OCEAN UNIV

Preparation method and application of carbon-based sulfur hydrolysis catalyst

The invention relates to the technical field of gas purification and chemical catalysts, and discloses a preparation method and application of a carbon-based sulfur hydrolysis catalyst, and the preparation method comprises the following steps: preparing the carbon-based sulfur hydrolysis catalyst from sulfolane, monopropanolamine, tripropanolamine and water through temperature-controlled mutual dissolution and precise filtration; the application method of the carbon-based sulfur hydrolysis catalyst comprises the following steps: spraying the carbon-based sulfur hydrolysis catalyst into an absorption tower, and constructing a double-temperature area in the absorption tower; maintaining high temperature in the lower area of the absorption tower, and catalyzing carbon disulfide and carbon sulfide to hydrolyze by utilizing monopropanolamine; the upper area of the absorption tower is kept at low temperature, tripropanolamine is used for absorbing hydrogen sulfide and carbon dioxide, the carbon-based sulfur hydrolysis catalyst absorbing gas is conveyed to a desorption tower, hydrogen sulfide and carbon dioxide are desorbed through high temperature and negative pressure to serve as product gas, and a regenerated solution is recycled. The method provided by the invention solves the contradiction between carbon disulfide hydrolysis and product absorption, and realizes conversion and resource recovery of organic sulfur.
Owner:XIAMEN ADIT ENVIRONMENTAL PROTECTION TECH CO LTD

Desulfurization method, desulfurization apparatus, hydrogen generation apparatus, and fuel cell system

To provide a technique suitable for desulfurization of a gas containing carbon sulfide.SOLUTION: The desulfurization process includes first contacting the source gas 50 with an amine-bearing agent 102 to reduce carbon sulfides in the source gas 50. The amine-bearing agent 102 has an amine as a functional group. The desulfurization method includes reducing hydrogen sulfide generated by the first contact in the source gas 50.SELECTED DRAWING: Figure 2
Owner:PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO LTD