Liquid catalyst for room-temperature catalytic ozonolysis as well as preparation method and application thereof
A liquid catalyst, ozone decomposition technology, applied in the direction of catalyst activation/preparation, metal/metal oxide/metal hydroxide catalyst, physical/chemical process catalyst, etc., to achieve the effect of low cost, wide application range and simple process
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0038] Mix 7.55g manganese sulfate with 1.46g EDTA, 2.75×10 -3 g sodium pyrophosphate plus 22.7mL water to form a solution, put it in a 70°C water bath and stir for 20min, add 37.8mL water and absolute ethanol mixture (volume ratio 1:1) after cooling and transfer to a crystallization kettle, place at 180°C Crystallize in an oven for 3 hours, and then carry out suction filtration after cooling to room temperature. Add 55mL of ethanol to the obtained solid to disperse, and obtain a concentration of 5×10 -2 g / mL manganese oxide room temperature ozonolysis liquid catalyst.
Embodiment 2
[0040] 6.30g manganese chloride, 10.10g ferric nitrate and 6.75g oxalic acid, 8.29×10 -2 g sodium tripolyphosphate plus 49.2mL water to form a solution, placed in a 90°C water bath and stirred for 30min, after cooling, added 164mL water and ethylene glycol mixture (volume ratio 1:1) and transferred to a crystallization kettle, placed at 120°C Crystallize in an oven for 8 hours, and after cooling to room temperature, carry out suction filtration, add 4140mL of water to the obtained solid to disperse, and obtain a concentration of 1×10 -3 g / mL ferromanganese binary composite oxide liquid catalyst for ozonolysis at room temperature.
Embodiment 3
[0042] 14.32g manganese nitrate, 8.08g ferric nitrate, 1.09g cerium nitrate and 12.0g citric acid, 7.32×10 -2g sodium hexametaphosphate plus 2.3mL water to form a solution, add 164.4mL of absolute ethanol and transfer to a crystallization kettle, place in a 140°C oven for crystallization for 4 hours, cool to room temperature and perform suction filtration, and add 180mL of acrylic acid to the obtained solid Alcohol is dispersed to obtain a concentration of 2×10 -2 g / mL manganese-iron-cerium ternary composite oxide liquid catalyst for ozonolysis at room temperature.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com