Seawater desalination material based on polyurethane foams and preparation method thereof
A technology of polyurethane foam and polyurethane sponge, which is applied in seawater treatment, general water supply saving, heating water/sewage treatment, etc., can solve the problem of low evaporation efficiency, achieve simple operation, reduce cost, and improve heat absorption performance
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[0028] A preparation method of seawater desalination material based on polyurethane foam, comprising the following steps:
[0029] 1) Preparation of polyurethane sponge grafted with reduced graphene oxide;
[0030] 1-1) Add graphene oxide into a three-necked flask, then add deionized water, and ultrasonically disperse to obtain solution A;
[0031] 1-2) Put the polyurethane sponge in absolute ethanol for ultrasonic treatment, then place it in deionized water for ultrasonic treatment after drying, and then dry; add the pretreated polyurethane sponge to solution A, and heat Stir in a constant temperature water bath for 30-40min to coagulate;
[0032] 1-3) Raise the temperature of the constant temperature water bath to 95-105°C, and add 20 μl of hydrazine hydrate per mg of graphene oxide for in-situ reduction for 1-1.2 hours;
[0033] 1-4) Take out the polyurethane sponge and dry it at 50-55°C for 24-30 hours to obtain a polyurethane sponge grafted with reduced graphene oxide; ...
Embodiment 1
[0041] A preparation method of seawater desalination material based on polyurethane foam, comprising the following steps:
[0042] Step 1. Add 0.1 g of graphene oxide into a 250 mL three-necked flask, add 80 ml of deionized water, and ultrasonically disperse the mixed solution for 10 minutes to obtain solution A;
[0043] Put the polyurethane sponge in absolute ethanol for ultrasonic treatment, after drying, put it in deionized water for ultrasonic treatment, and then dry;
[0044] Add three dried sponges (about 0.5 g) to solution A, and stir in a constant temperature water bath at 30°C for 30 min to coagulate;
[0045] Raise the temperature of the constant temperature water bath to 100°C, and add 20 μl hydrazine hydrate per mg of graphene oxide for in-situ reduction for 1 hour;
[0046] Take out the polyurethane sponge, put it in a low-temperature drying oven at 50°C for 24 hours to dry, and obtain a polyurethane sponge grafted with reduced graphene oxide;
[0047] Step 2. ...
Embodiment 2
[0052] A preparation method of seawater desalination material based on polyurethane foam, comprising the following steps:
[0053] Step 1. Add 0.1 g of graphene oxide into a 250 mL three-necked flask, add 80 ml of deionized water, and ultrasonically disperse the mixed solution for 10 minutes to obtain solution A;
[0054] Put the polyurethane sponge in absolute ethanol for ultrasonic treatment, after drying, put it in deionized water for ultrasonic treatment, and then dry;
[0055] Add three dried sponges (about 0.5 g) to solution A, and stir in a constant temperature water bath at 30°C for 30 min to coagulate;
[0056] Raise the temperature of the constant temperature water bath to 100°C, and add 20 μl hydrazine hydrate per mg of graphene oxide for in-situ reduction for 1 hour;
[0057] Take out the sponge, put it into a low-temperature drying oven at 50°C for 24 hours to dry, and obtain a polyurethane sponge grafted with reduced graphene oxide;
[0058] Step 2. Dissolve 0.25...
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