Hydrophobic carbon-coated copper microsphere as well as preparation method and application thereof
A hydrophobic, carbon-coated technology, applied in electrolytic organic production, electrolytic components, electrodes, etc., which can solve the problems of CO2 leakage, hindering the commercialization of large-scale CCS deployment, high energy consumption of carbon capture and storage technology, and achieving mild conditions. , is conducive to large-scale industrial applications, and is conducive to the effect of popularization and application
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0034] Step 1, preparation of hydrophobic carbon-coated copper microspheres
[0035]Dissolve 0.435 g of copper nitrate trihydrate and 0.676 g of polyvinylpyrrolidone in 15 mL and 30 mL of ethylene glycol, respectively. Subsequently, the copper nitrate solution was slowly dropped into the polyvinylpyrrolidone solution under vigorous stirring, and finally 0.322 g of chitosan was added. The solution was transferred to a polytetrafluoroethylene-lined steel jacket, and heated in an oven at 180° C. for 2 hours. After naturally cooling to room temperature, they were centrifuged and washed with deionized water and ethanol, and dried in a vacuum oven at 60 °C to obtain hydrophobic multilayer core-shell structure composite microspheres Cu x O@C.
[0036] Step 2. Performance Characterization Test
[0037] Through CHI660 electrochemical workstation, standard three-electrode system, CO 2 Saturated 0.1M KHCO 3 Solution (pH=6.8) was used as the electrolyte to support the glassy carbon e...
Embodiment 2
[0050] Dissolve 0.2 g of copper nitrate trihydrate and 0.3 g of polyvinylpyrrolidone in 5 mL and 10 mL of ethylene glycol, respectively. Subsequently, the copper nitrate solution was slowly dropped into the polyvinylpyrrolidone solution under vigorous stirring, and finally 0.2 g of chitosan was added. Transfer the solution to a polytetrafluoroethylene-lined steel jacket, and heat it in an oven at 210° C. for 1 hour. After naturally cooling to room temperature, they were centrifuged and washed with deionized water and ethanol, and dried in a vacuum oven at 60 °C to obtain hydrophobic multilayer core-shell structure composite microspheres Cu x O@C. Features and properties are similar to Example 1.
Embodiment 3
[0052] Dissolve 0.6 g of copper nitrate trihydrate and 0.9 g of polyvinylpyrrolidone in 30 mL and 60 mL of ethylene glycol, respectively. Then the copper nitrate solution was slowly dropped into the polyvinylpyrrolidone solution under the condition of vigorous stirring, and finally 0.6 g of chitosan was added. Transfer the solution to a polytetrafluoroethylene-lined steel jacket, and heat it in an oven at 150° C. for 4 hours. After naturally cooling to room temperature, they were centrifuged and washed with deionized water and ethanol, and dried in a vacuum oven at 60 °C to obtain hydrophobic multilayer core-shell structure composite microspheres Cu x O@C. Features and properties are similar to Example 1.
PUM
| Property | Measurement | Unit |
|---|---|---|
| Diameter | aaaaa | aaaaa |
| Size | aaaaa | aaaaa |
| Thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More