Preparation method of medical protective clothing fabric
A technology for protective clothing and fabrics, which is applied in the field of preparation of medical protective clothing fabrics, can solve the problems that the advantages of rutile titanium dioxide cannot be well utilized, and achieve the effect of reducing temperature and increasing comfort.
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[0032]Example 1
[0033]The medical protective clothing fabric provided in this embodiment is prepared by the following steps:
[0034](1) The chitosan and sulfuric acid were dissolved in water, and in the three flasks, the constant temperature was maintained after stirring to 50 ° C, and the HI aqueous solution was added to the three flasks at a 5 ml / min, and the drip completion After the constant temperature reaction is 1 hour, then the temperature is lowered to -8 ° C, and the yellow crystal A is obtained, wherein the chitosan, H2SO4Hi, water mass ratio is 1: 0.6: 0.3: 4, with the following reaction equation:
[0035]
[0036]Wherein is 30 to 60.
[0037](2) Crystal A is dissolved in diethyl ether, and the newly cut metal magnesium is cut into small pieces, and the diethyl ether solvent is added to be stirred at room temperature for 3 hours, then the solvent is removed at 30 ° C, and the remaining solution is heated to 60 ° C, The filtration was filtered, then the filtrate was cooled to -5 ° ...
Example Embodiment
[0044]Example 2
[0045]The medical protective clothing fabric provided in this embodiment is prepared by the following steps:
[0046](1) The chitosan and sulfuric acid were dissolved in water, and the three flasks were added, and after the stirring was heated to 55 ° C, the constant temperature was maintained, and the Hi aqueous solution was dripped with a 5.5 ml / min to three flasks, dripping After completing, the constant temperature reacts for 1.5 hours, then cooling to -9 ° C, and is pale yellow crystal A. Among them, chitosan, H2SO4Hi, water mass ratio is 1: 0.7: 0.35: 4.5.
[0047](2) Crystal A is dissolved in diethyl ether, and the newly cut metal magnesium is cut into small pieces, and the diethyl ether solvent is added, stirred at room temperature for 3.5 hours, then the solvent is removed at 35 ° C, and the remaining solution is heated to 65 ° C, The heat was filtered, then the filtrate was cooled to -6 ° C, and the solid B was obtained. Among them, the mass ratio of crystal A, ...
Example Embodiment
[0051]Example 3
[0052]The medical protective clothing fabric provided in this embodiment is prepared by the following steps:
[0053](1) The chitosan and sulfuric acid were dissolved in water, and in the three flasks, the constant temperature was maintained after heating to 60 ° C, and the Hi aqueous solution was added to the three flasks of 6 ml / min, and the added completion After the constant temperature reaction is 2 hours, then the temperature is lowered to -10 ° C, and the yellow crystal A is obtained. Among them, chitosan, H2SO4Hi, water mass ratio is 1: 0.8: 0.4: 5.
[0054](2) The crystal A is dissolved in diethyl ether, and the newly cut metal magnesium is cut into a small piece, and the diethyl ether solvent is added, stirred at room temperature for 4 hours, then the solvent is removed at 35 ° C, and the remaining solution is heated to 70 ° C, The filtrate was filtered, then the filtrate was cooled to -7 ° C to achieve the firm body B. The mass ratio of crystal A, magnesium and...
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