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A kind of preparation method of s-la-ni/foam nickel cathode material

A cathode material, nickel foam technology, applied in electrodes, electrolysis components, electrolysis process, etc., can solve the problem of low threshold, and achieve the effect of high hydrogen evolution activity and optimal adsorption and dissociation performance.

Active Publication Date: 2022-01-04
山东海氢能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] In addition, as mentioned above, the key to the preparation of beauty water lies in electrification, relying on electrons to reduce hydrogen gas at the cathode, leaving hydroxyl groups, and obtaining weakly alkaline electrolytic reduced water. Cathode electrodes for electrolysis of reduced water

Method used

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  • A kind of preparation method of s-la-ni/foam nickel cathode material
  • A kind of preparation method of s-la-ni/foam nickel cathode material
  • A kind of preparation method of s-la-ni/foam nickel cathode material

Examples

Experimental program
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Effect test

Embodiment 1

[0068] A method for preparing a negative electrode for weakly alkaline beauty water, comprising the following preparation method:

[0069] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 5A / dm 2 , temperature 40 o C, time 30minh, inert gas atmosphere.

[0070] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 30wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1, accompanied by ultrasound Stirring 30kHz, temperature 30 o c.

[0071] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment. The heat treatment takes 12 hours and the temperature is 450 o c.

[0072] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0073] Nickel salt i...

Embodiment 2

[0079] A method for preparing a negative electrode for weakly alkaline beauty water, comprising the following preparation method:

[0080] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 10A / dm 2 , temperature 45 o C, time 2h, inert gas atmosphere.

[0081] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 32.5wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.25, accompanied by Ultrasonic stirring 35kHz, temperature 33 o c.

[0082] (3) Place the cathode that has been heat-treated in step (2) under inert gas conditions for heat treatment. The heat treatment takes 18 hours and the temperature is 600 o c.

[0083] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0084] Nic...

Embodiment 3

[0090] A method for preparing a negative electrode for weakly alkaline beauty water, comprising the following preparation method:

[0091] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 15A / dm 2 , temperature 50 o C, time 4h, inert gas atmosphere.

[0092] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 35wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.5, accompanied by ultrasound Stirring 40kHz, temperature 35 o c.

[0093] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment, the heat treatment time is 24 hours, and the temperature is 650 o c.

[0094] (4) Washing and drying: washing with deionized water and air drying in cold air.

[0095] Nickel salt...

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Abstract

The invention discloses a method for preparing a cathode for weakly alkaline beauty water. The cathode uses porous nickel-based hydrogen-evolving electrode foam metal as a substrate, electrolytically deposits a S-La-Ni alloy through an ionic liquid, and then corrodes it in an alkaline solution. Treatment removes aluminum to obtain a porous electrode, and then undergoes sulfur modification by heat treatment. When electrolyzing water to prepare weakly alkaline beauty water, it shows extremely high catalytic activity and chemical stability.

Description

technical field [0001] The invention relates to a method for preparing a S-La-Ni / foam nickel cathode material, which is a cathode for weakly alkaline beauty water, belongs to electrolyzing water to prepare weakly alkaline ionized water, and particularly relates to a method for preparing a cathode electrode in an electrolysis process . Background technique [0002] Electrolyzed reduced water is a kind of safe drinking water, which is weakly alkaline (pH>7); the water molecule cluster is about 5-6 water molecules, and the movement speed in the body is 11-13 water molecules in pure water or tap water Twice of that, the molecular activity is relatively high, so a large amount of small molecule water has different functions; high oxygen content, negative potential, can remove peroxides in the body, and have the effect of disease prevention and anti-aging; rich in ionic water minerals. Electrolyzed reduced water fully complies with the hygienic standards of drinking water in ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C25B11/031C25B11/052C25B11/054C25B11/061C25B11/089C25B1/04C25D3/66C25D5/48C23F1/36C25D5/50
CPCY02E60/36
Inventor 杜先明
Owner 山东海氢能源科技有限公司
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