Nano multi-layer composite solid lubricating film layer with long service life under space irradiation and preparation thereof

A nano-multilayer, solid-lubrication technology, applied in coating, vacuum evaporation coating, metal material coating process, etc., can solve the problems of not having resistance to space atomic oxygen erosion, electron proton irradiation, application of immovable parts, etc. Achieve excellent anti-space irradiation performance, ensure long-term reliable operation, and enhance the effect of anti-space irradiation performance

Active Publication Date: 2021-05-07
SHANGHAI AEROSPACE EQUIP MFG GENERAL FACTORY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this kind of film structure does not have the ability to resist space atomic oxygen erosion, ultraviolet radiation, and electron proton radiation, and cannot be applied to moving parts exposed to strong radiation space environments, which is fundamentally different from the present invention

Method used

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  • Nano multi-layer composite solid lubricating film layer with long service life under space irradiation and preparation thereof
  • Nano multi-layer composite solid lubricating film layer with long service life under space irradiation and preparation thereof

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Embodiment 1

[0043] This embodiment provides a long-life nanometer multi-layer composite solid lubricating film layer under space irradiation environment. MoS 2 Ti is alternately repeated 10 times, and the number of prepared functional layers is 20 layers. The content of Ag and Ni elements in the AgTiNi layer is 9:1, and Ti elements account for 10% of the total. MoS 2 MoS in Ti 2 The composition ratio with Ti is 9:1, and the total thickness of the film layer is 2.5 μm thick nano-multilayer composite solid lubricating film layer.

[0044] The specific preparation process of the long-life nano-multilayer composite solid lubricating film layer under the above-mentioned space irradiation environment is carried out according to the following steps:

[0045] 1) Sputter cleaning: attached figure 2 The coating layer equipment shown (the equipment includes sample turntable, air intake system, Ti target, two MoS 2 target and AgNi target), the 7 position is the Ti target, the 8 and 10 positions a...

Embodiment 2

[0053] The present invention is a long-life nanometer multi-layer composite solid lubricating film layer under space irradiation environment, the substrate is TC4, a Ti binding layer with a thickness of 10nm, a TiN bearing layer with a thickness of 1μm, an AgTiNi functional layer with a thickness of 80nm and MoS with a thickness of 120nm 2 Ti is alternately repeated 5 times, and the number of functional layers prepared is 10. The content of Ag and Ni elements in the AgTiNi layer is 9:1, and Ti elements account for 10% of the total. MoS 2 The proportion of Ti in Ti is 5%, and the total thickness of the film layer is about 2 μm thick nano-multilayer composite solid lubricating film layer.

[0054] The specific preparation process of the long-life nano-multilayer composite solid lubricating film layer under the above-mentioned space irradiation environment is carried out according to the following steps:

[0055] 1) Sputter cleaning: attached figure 2 In the coating layer equipm...

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Abstract

The invention discloses a nano multi-layer composite solid lubricating film layer with a long service life under space irradiation and preparation thereof. The nano multi-layer composite solid lubricating film layer composed of a Ti binding layer, a TiN bearing layer and an AgTiNi / MoS2Ti nano multi-layer lubricating functional layer is deposited on a titanium alloy substrate, an aluminum alloy substrate, a stainless steel substrate, a bearing steel substrate and the like by adopting a closed magnetic field unbalanced magnetron sputtering technology. The nano multi-layer composite film layer can reliably serve for a long time in strong space irradiation environments such as low-orbit high atomic oxygen density, medium-high-orbit high electron proton density and high ultraviolet irradiation dose, and is high in bearing capacity and low in friction coefficient, thus, the service life of a moving part of a spacecraft exposed in the space irradiation environments can be greatly prolonged, and the reliability of the moving part is improved. In addition, the preparation method has the characteristics that the process is environment-friendly and flexible, the film thickness is uniform, the compactness is good, the preparation process of the film layer is controlled in a programmed manner, the modulation period of the film layer is easy to regulate and control, and batch treatment can be realized, industrial production is easy to realize, and the good application prospect is achieved.

Description

technical field [0001] The invention relates to the fields of material surface vacuum coating technology and space environment engineering, in particular to a long-life nanometer multi-layer composite solid lubricating film under space irradiation environment and its preparation. Background technique [0002] Some materials in space vehicles (launch vehicles, etc.) and aircraft (artificial earth satellites, manned spacecraft, space stations, space probes, etc.) will produce friction and wear and cold welding effects during relative motion. Compared with ground applications, space The moving parts have their particularity in the service process. With the continuous development of my country's aerospace industry, the application of space moving parts is becoming more and more extensive and there are more and more types. Friction and wear are one of the main problems determining the life of space systems. Materials The tribological properties of the material are not entirely the ...

Claims

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Application Information

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IPC IPC(8): C23C14/35C23C14/02C23C14/06C23C14/16
CPCC23C14/352C23C14/025C23C14/165C23C14/0036C23C14/0641C23C14/0623
Inventor 鞠鹏飞李忠建藏旭升肖金涛陈妍邢明秀
Owner SHANGHAI AEROSPACE EQUIP MFG GENERAL FACTORY
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