Nitrogen-enriched hollow hybrid carbon catalytic material as well as preparation method and application thereof
A carbon catalysis and enrichment technology, applied in chemical instruments and methods, physical/chemical process catalysts, separation methods, etc., can solve the problems of low nitrogen introduction, underdeveloped pore structure, and few applications, and achieve high nitrogen content. , Small environmental pollution, high activity effect
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Embodiment 1
[0079] A kind of method for preparing monodisperse Zn-ZIF, specifically finish according to the following steps:
[0080] Zinc nitrate hexahydrate (Zn(NO 3 ) 2 ·6H 2 O) and manganese nitrate (Mn(NO 3 ) 2 ) was dissolved in methanol to form a homogeneous metal solution; finally, the metal solution was quickly poured into a methanol solution containing 2-methylimidazole under stirring; left to react at room temperature for 24 hours, filtered, washed twice with water, and washed with methanol 3 times, and then dried at a temperature of 100°C for 8 hours to obtain Zn-ZIF;
[0081] Zn(NO 3 ) 2 ·6H 2 The concentration of O is 100mmol / L;
[0082] Mn(NO 3 ) 2 The concentration is 0mmol / L;
[0083] The concentration of 2-methylimidazole in the methanol solution of 2-methylimidazole described in the step is 500mmol / L;
[0084] The volume ratio of the metal solution described in the step to the methanol solution of 2-methylimidazole is 1:1.
[0085] figure 1 For the SEM fig...
Embodiment 2
[0087] A kind of method for preparing monodisperse Mn-Zn-ZIF, specifically finish according to the following steps:
[0088] Zinc nitrate hexahydrate (Zn(NO 3 ) 2 ·6H 2 O) and manganese nitrate (Mn(NO 3 ) 2 ) was dissolved in methanol to form a homogeneous metal solution; finally, the metal solution was quickly poured into a methanol solution containing 2-methylimidazole under stirring; left to react at room temperature for 24 hours, filtered, washed twice with water, and washed with methanol 3 times, and then dried at a temperature of 100°C for 8 hours to obtain Mn-Zn-ZIF;
[0089] Zn(NO 3 ) 2 ·6H 2 The concentration of O is 100mmol / L;
[0090] Mn(NO 3 ) 2The concentration is 10mmol / L;
[0091] The concentration of 2-methylimidazole in the methanol solution of 2-methylimidazole described in the step is 500mmol / L;
[0092] The volume ratio of the metal solution described in the step to the methanol solution of 2-methylimidazole is 1:1.
[0093] figure 2 For the ...
Embodiment 3
[0095] A kind of method for preparing monodisperse Mn-Zn-ZIF, specifically finish according to the following steps:
[0096] Zinc nitrate hexahydrate (Zn(NO 3 ) 2 ·6H 2 O) and manganese nitrate (Mn(NO 3 ) 2 ) was dissolved in methanol to form a homogeneous metal solution; finally, the metal solution was quickly poured into a methanol solution containing 2-methylimidazole under stirring; left to react at room temperature for 24 hours, filtered, washed twice with water, and washed with methanol 3 times, and then dried at a temperature of 100°C for 8 hours to obtain Mn-Zn-ZIF;
[0097] Zn(NO 3 ) 2 ·6H 2 The concentration of O is 100mmol / L;
[0098] Mn(NO 3 ) 2 The concentration is 20mmol / L;
[0099] The concentration of 2-methylimidazole in the methanol solution of 2-methylimidazole described in the step is 500mmol / L;
[0100] The volume ratio of the metal solution described in the step to the methanol solution of 2-methylimidazole is 1:1.
[0101] image 3 For the ...
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