Gas barrier laminate
A technology of gas-barrier laminates and gas-barrier layers, which is applied to coatings, layered products, rubber-layered products, etc., can solve problems such as shortened life and equipment performance, and achieve thinning and excellent gas-barrier properties , Excellent effect of optical isotropy
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[0155] The solvent used in the preparation of the above-mentioned curable resin composition is not particularly limited, and examples include: aliphatic hydrocarbon solvents such as n-hexane and n-heptane; aromatic hydrocarbon solvents such as toluene and xylene; dichloromethane , vinyl chloride, chloroform, carbon tetrachloride, 1,2-dichloroethane, monochlorobenzene and other halogenated hydrocarbon solvents; methanol, ethanol, propanol, butanol, propylene glycol monomethyl ether and other alcohol solvents; acetone , methyl ethyl ketone, 2-pentanone, isophorone, cyclohexanone and other ketone solvents; ethyl acetate, butyl acetate and other ester solvents; ethyl cellosolve and other cellosolve solvents; 1,3-di Ether solvents such as oxolane; etc.
[0156] Although content of the solvent in the said curable resin composition is not specifically limited, It is 0.1-1,000g normally with respect to 1g of polymer components (A), Preferably it is 1-100g. By appropriately adjusting ...
Embodiment 1
[0332] Curable resin composition 1 to be a base layer was prepared in the following procedure.
[0333]
[0334] As a polymer component, 100 parts by mass of polyimide resin (PI) pellets (manufactured by Kawamura Sangyo Co., Ltd., product name KPI-MX300F, Tg=354°C, weight average molecular weight: 280,000) were dissolved in methyl ethyl ketone (MEK) , a 15% by mass solution of PI was prepared. Next, 122 parts by mass of tricyclodecane dimethanol diacrylate (manufactured by Shin-Nakamura Chemical Industry Co., Ltd., A-DCP) as a curable monomer and bis(2 , 5 parts by mass of 4,6-trimethylbenzoyl)phenylphosphine oxide (manufactured by BASF Corporation, Irgacure 819), and curable resin composition 1 was prepared. In addition, the curable monomer and polymerization initiator used in this Example and other experimental examples do not contain a solvent, and all are raw materials whose solid content is 100%.
[0335] Next, use the first PET film (manufactured by Toyobo Co., Ltd.,...
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