Ceramic composite material and preparation method thereof, bulletproof plate and armored protective equipment
A ceramic composite material, bulletproof plate technology, applied in protective equipment, armor, offensive equipment, etc., can solve the problems of increasing the overall weight, unable to meet the bulletproof requirements of armored protective equipment, and high density.
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[0065] One embodiment of the present invention provides a method for preparing a ceramic composite material, comprising the following steps S10-S30.
[0066] Step S10 , mixing the raw materials of the ceramic green body of the ceramic composite material to make slurry, drying and granulating to obtain granulated powder.
[0067] In some of these embodiments, in step S10, the step of mixing and pulping the raw materials includes the following steps S11-S12.
[0068] Step S11, mixing the main ceramic material, binder and solvent to obtain a mixture.
[0069] Step S12, mixing the first slurry obtained in step S11 with chopped carbon fibers to obtain a ceramic composite slurry.
[0070] Further, the viscosity of the ceramic composite slurry is 20mpa·s˜60mpa·s.
[0071] In one embodiment, in step S11, the solvent used is selected from water or an organic solvent, and further, the solvent is selected from at least one of water, acetone and absolute ethanol.
[0072] It should be ...
Embodiment 1
[0101]1. According to the mass percentage, the ceramic main material of the following components is provided: 70wt% silicon nitride powder, 15wt% silicon carbide powder, 5wt% boron carbide powder, 10wt% sintering aid (yttrium oxide and oxide Aluminum, the mass ratio of the two is 5:2); the ceramic main materials are mixed, ethanol is used as the ball milling solvent, PVB is added as the binder, silicon nitride balls are used as the ball milling medium, and the roller mill is used for ball milling. The ball milling time For 3 hours, a mixture was obtained. Then, the chopped carbon fibers accounting for 1% of the total mass of the silicon nitride powder, silicon carbide powder and boron carbide powder were ball milled for 1 h by a roller mill to obtain a ceramic slurry with a viscosity of 40 mPa·s. Among them, the purity of silicon nitride powder is 99.6%, the mass content of α-phase silicon nitride is 92%, the particle size D50 of silicon nitride powder is 0.6 micron; the lengt...
Embodiment 2
[0106] Step 1 is basically the same as Step 1 of Example 1, except that the main ceramic material includes: 65wt% silicon nitride powder, 20wt% silicon carbide powder, 5wt% boron carbide powder, 10wt% sintered Auxiliary; Other conditions are the same as step 1 of Example 1.
[0107] Steps 2) to 4 are basically the same as steps 2) to 4 of Example 1, and step 3) has a density of 1.75g / cm3 for the ceramic green body 3 ; Step 4 infiltration and sintering for 3 hours, the density of the obtained ceramic composite material is 2.96g / cm 3 .
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