Micro-current elastic dressing for chronic wound healing, and preparation method thereof
A chronic wound, micro-current technology, applied in pharmaceutical formulations, electrospinning, textile material processing, etc., can solve the problems of deterioration, high permeability, unsanitary cotton flocks, etc., to promote cell proliferation and differentiation, improve Piezoelectric effect, the effect of promoting wound healing
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[0027] The invention provides a micro-current elastic dressing for chronic wound healing and a preparation method thereof. Using polyvinylidene fluoride, water-based polyurethane and zinc acetate as raw materials, a composite nanofiber membrane with a core-shell structure is prepared by electrospinning technology. After hydrothermal reaction, the surface of the composite nanofibrous membrane is loaded with dense and highly oriented zinc oxide nanorods, and a microcurrent elastic dressing that promotes chronic wound healing, has high voltage effect and antibacterial properties is obtained.
[0028] The preparation method of the described micro-current elastic dressing for chronic wound treatment comprises the steps:
[0029] S1, preparation of spinning solution
[0030] S1.1. Spinning solution for nuclear layer: use N-N dimethylformamide (DMF) and acetone as solvent (mass ratio is 3:2), add a certain amount of water-based polyurethane solution, and mix well;
[0031] S1.2 Shel...
Embodiment 1
[0047] 1.1. Preparation of spinning solution
[0048] 1.1.1. Spinning liquid for core layer: use N-N dimethylformamide (DMF) and acetone as solvent (mass ratio 3:2), add 10% aqueous polyurethane solution, mix well and then spin ;
[0049] 1.1.2. Shell spinning solution: use DMF and acetone as solvents, add 0.112g of 1% zinc acetate powder, and disperse by ultrasonic for 60min. After the ultrasound was completed, 1.126 g of 10% 700,000 polyvinylidene fluoride powder was added to the mixed solution, and it was placed in a constant temperature heating magnetic stirrer at 85°C and stirred until it was completely dissolved. After uniformity, a mixed solution of zinc acetate with different mass fractions was obtained.
[0050] 1.2. Electrospinning
[0051] Using a high-voltage electrospinning machine, set the spinning voltage to 16-18kV, the receiving distance to 12-18cm, the spinning rate to 0.015-0.019mL / min, and choose 22G (inner diameter 0.41mm, outer diameter 0.72mm) / 17G (inn...
Embodiment 2
[0055] 2.1. Preparation of spinning solution
[0056] 2.2.1. Spinning solution for the core layer: use N-N dimethylformamide (DMF) and acetone as solvents (mass ratio 3:2), add 20% aqueous polyurethane solution, and mix well;
[0057] 2.2.2. Sheath spinning solution: DMF and acetone are also used as solvents, 0.227g of 2% zinc acetate powder is added, and ultrasonically dispersed for 60min. After the ultrasonication was completed, 1.136g of 10% 700,000 polyvinylidene fluoride powder was added to the mixed solution, placed in a constant temperature heating magnetic stirrer at 85°C and stirred until completely dissolved, and mixed solutions of zinc acetate with different mass fractions were obtained after uniformity.
[0058] 2.2. Electrospinning
[0059] Using a high-voltage electrospinning machine, set the spinning voltage to 16-18kV, the receiving distance to 12-18cm, the spinning rate to 0.015-0.019mL / min, and choose 22G (inner diameter 0.41mm, outer diameter 0.72mm) / 17G (i...
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