Sized and coated photo-thermal phase change composite yarn and preparation method thereof

A composite yarn and coating technology, which is applied in fiber types, textiles and papermaking, and fiber processing, can solve the problems of light-to-heat conversion synergistic phase change temperature adjustment functions, less functional research, and low production efficiency, etc. High heat conversion efficiency, simple preparation method, and long service life

Active Publication Date: 2021-10-22
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among the existing preparation methods, most of them focus on the unilateral research of porous matrix composite phase change heat storage materials and photothermal conversion materials, while the research on photothermal conversion synergistic phase change temperature regulation function is still relatively small.
At the same time, most of the research is aimed at the surface of fibers or fabrics, and there are relatively few functional studies using yarn as a carrier, and there are problems such as complex processes, cumbersome processes, and low production efficiency.

Method used

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  • Sized and coated photo-thermal phase change composite yarn and preparation method thereof
  • Sized and coated photo-thermal phase change composite yarn and preparation method thereof
  • Sized and coated photo-thermal phase change composite yarn and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0019] 1) Prepare 5.9% polyvinyl butyral / 5% zirconium carbide / 0.5% alumina suspension. Add polyvinyl butyral to absolute ethanol, stir mechanically until the solution is evenly mixed, then add zirconium carbide particles and alumina and continue stirring for a period of time, and finally ultrasonically treat to obtain uniformly dispersed 5% polyvinyl butyral / 5% zirconium carbide / 0.5% alumina suspension;

[0020] 2) Put a beaker containing a certain amount of paraffin into a magnetic stirrer in a water bath at 80°C and stir until the paraffin is completely melted, then set aside.

[0021] 3) Pour the molten paraffin and polyvinyl butyral / zirconium carbide / alumina suspension into the two sizing tanks of the sizing machine respectively, and then introduce the polyester yarn (20S / 2) through the yarn guide device first Go to the size tank (80°C) filled with molten paraffin, the sizing speed is 1.8m / min, and then pass through the size tank (room temperature) with polyvinyl butyral...

Embodiment 2

[0024] 1) Prepare 5.9% polyvinyl butyral solution. Add polyvinyl butyral to absolute ethanol, and mechanically stir until the solution is uniformly mixed to obtain a uniformly mixed 5.9% polyvinyl butyral solution;

[0025] 2) Put a beaker containing a certain amount of paraffin into a magnetic stirrer in a water bath at 80°C and stir until the paraffin is completely melted, then set aside.

[0026] 3) Pour the molten paraffin and polyvinyl butyral solutions into the two sizing tanks of the sizing machine respectively, and then introduce the polyester yarn into the sizing tank containing the molten paraffin through the yarn guide device, and then pass through A size tank equipped with polyvinyl butyral solution passes through pressing rollers, a drying room, and a winding device to obtain polyester / paraffin / PVB composite yarn (B yarn). The temperature of the polyvinyl butyral solution size tank is room temperature, the temperature of the molten paraffin slurry tank is 80°C, t...

Embodiment 3

[0029] 1) Prepare 5.9% polyvinyl butyral / 5% zirconium carbide / 0.5% alumina suspension. Add polyvinyl butyral to absolute ethanol, mechanically stir until the solution is evenly mixed, then add zirconium carbide particles and alumina and continue stirring for a period of time, and finally obtain uniformly dispersed 5.9% polyvinyl butyral by ultrasonic treatment / 5% zirconium carbide / 0.5% alumina suspension;

[0030] 2) Introduce polyester into a slurry tank equipped with 5.9% polyvinyl butyral / 5% zirconium carbide / 0.5% alumina suspension, and obtain polyester / PVB / ZrC / Al through pressing rollers, drying room, and winding device 2 o 3 / composite yarn;

[0031] 3) Put a beaker containing a certain amount of paraffin into a magnetic stirrer in a water bath at 80°C and stir until the paraffin is completely melted, then set aside.

[0032] 4) Pour the molten paraffin and the polyvinyl butyral / zirconium carbide / alumina suspension into the two sizing tanks of the sizing machine respe...

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Abstract

The invention relates to sized and coated photo-thermal phase change composite yarn and a preparation method thereof. The method comprises the following steps of 1, preparing a polyvinyl butyral / zirconium carbide / aluminum oxide suspension and a polyvinyl butyral solution; 2, preparing a molten paraffin material; and 3, by taking a polyvinyl butyral / zirconium carbide / aluminum oxide coating as a surface layer, paraffin as a middle layer and terylene / polyvinyl butyral / zirconium carbide / aluminum oxide composite yarn or pure terylene yarn as core yarn, preparing terylene / polyvinyl butyral / zirconium carbide / aluminum oxide / paraffin composite yarn through a coating method. The method has the advantages that 1, the photo-thermal conversion function is achieved, and the photo-thermal conversion efficiency is relatively high; 2, the phase change function is achieved, and the heat storage and temperature adjustment can be achieved; 3, the preparation method is simple, economic and rapid; and 4, the service life is long, and the shape stability is better.

Description

technical field [0001] The invention relates to a preparation method of a photothermal phase change composite yarn, more specifically, the invention relates to a sizing-coated photothermal phase change composite yarn and a preparation method thereof. Background technique [0002] The development of functional textile materials is a trend in the textile industry at present. With the development of economy and society, textile materials should have many functional features in addition to conventional warmth and covering, such as phase change temperature regulation, light-to-heat conversion, Conductive etc. [0003] Li et al. used zirconium carbide as the photothermal conversion material to prepare viscose composite fibers with photothermal effect by wet spinning method. The near-infrared light absorption rate of the composite fiber can reach 90%, and when irradiated with infrared light for 60s, its temperature can be increased by 39.4 °C compared with the original viscose fib...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/347D06M11/74D06M11/45D06M13/02D06M101/32
CPCD06M15/347D06M11/74D06M11/45D06M13/02D06M2101/32
Inventor 柯贵珍靳新亚李文斌王羽陈姝卉徐卫林
Owner WUHAN TEXTILE UNIV
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