A kind of sic/sic composite material high density multilayer matrix and preparation method
A composite material and matrix technology, which is applied in the field of composite material preparation, can solve problems such as consumption of crack energy, single structure, difficulty in meeting the high strength, toughness and stress requirements of aero-engines, and achieve the effect of reducing open porosity
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[0041] Step 1. Preparation of SiC / SiC preform:
[0042] In step 1.1, a SiC fiber braid is used to prepare a boron nitride (BN) interface phase on its surface, and the thickness of the interface phase is 300-500 nm.
[0043] In step 1.2, a CVI process is used to prepare a SiC matrix with a certain volume fraction in the SiC fiber preform obtained in step 1.1. Using trichloromethylsilane (MTS) as the precursor, hydrogen as the carrier gas, argon as the diluent gas, the flow ratio of the three is 1:5~50:2~20, the total pressure is 0.5~5kPa, and the deposition temperature is 873 ~1773K, the deposition time is about 600 hours. This results in a porosity of 28 to 36% and a density of 1.7 to 2.1 g / cm 3 Porous SiC / SiC composites for subsequent slurry impregnation.
[0044] Step 2. Configure 300-500nm SiC particle water-based slurry:
[0045] Step 2.1 Add SiC particles with a particle size of 300 to 500 nm and a volume fraction of 10 vol.% into HF acid, and magnetically stir at roo...
Embodiment 1
[0064] Step 1. Preparation of SiC / SiC preform:
[0065] In step 1.1, a SiC fiber braid is used to prepare a boron nitride (BN) interface phase on its surface, and the thickness of the interface phase is 300-500 nm.
[0066] In step 1.2, a CVI process is used to prepare a SiC matrix with a certain volume fraction in the SiC fiber preform obtained in step 1.1. Using trichloromethylsilane (MTS) as the precursor, hydrogen as the carrier gas, argon as the diluent gas, the flow ratio of the three is 1:5~50:2~20, the total pressure is 0.5~5kPa, and the deposition temperature is 873 ~1773K, the deposition time is about 600 hours. This results in a porosity of 28 to 36% and a density of 1.7 to 2.1 g / cm 3 Porous SiC / SiC composites for subsequent slurry impregnation.
[0067] Step 2. Configure 300-500nm SiC particle water-based slurry:
[0068] Step 2.1 Add SiC particles with a particle size of 300 to 500 nm and a volume fraction of 10 vol.% into HF acid, and magnetically stir at roo...
Embodiment 2
[0088] Step 1. Preparation of SiC / SiC preform:
[0089] In step 1.1, a SiC fiber braid is used to prepare a boron nitride (BN) interface phase on its surface, and the thickness of the interface phase is 300-500 nm.
[0090] In step 1.2, a CVI process is used to prepare a SiC matrix with a certain volume fraction in the SiC fiber preform obtained in step 1.1. Using trichloromethylsilane (MTS) as the precursor, hydrogen as the carrier gas, argon as the diluent gas, the flow ratio of the three is 1:5~50:2~20, the total pressure is 0.5~5kPa, and the deposition temperature is 873 ~1773K, the deposition time is about 600 hours. This results in a porosity of 28 to 36% and a density of 1.7 to 2.1 g / cm 3 Porous SiC / SiC composites for subsequent slurry impregnation.
[0091] Step 2. Configure 300-500nm SiC particle water-based slurry:
[0092] Step 2.1 Add SiC particles with a particle size of 300 to 500 nm and a volume fraction of 10 vol.% into HF acid, and magnetically stir at roo...
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