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Preparation method and system of nano silicon carbide particle reinforced aluminum-based gradient composite material

A nano-silicon carbide and particle-reinforced aluminum technology is applied in metal processing equipment, transportation and packaging. , the effect of high degree of mechanization

Pending Publication Date: 2022-01-21
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantages of micron-sized SiCp / Al composites are that the strength increases but the plasticity decreases significantly, and the high-temperature mechanical properties are not satisfactory, which has become a bottleneck problem restricting its development.
However, most of the additive phases used in existing gradient composites are usually in the micron-scale field, and there are few reports on the progress of preparing functionally graded aluminum matrix composites by adding nano-ceramic particles.
[0004] In addition, the production of nano-sized particle-reinforced aluminum-matrix composites is still in its infancy. The existing production lines for nano-sized particle-reinforced aluminum-based composites are not highly automated, with small production capacity and low production efficiency.

Method used

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  • Preparation method and system of nano silicon carbide particle reinforced aluminum-based gradient composite material
  • Preparation method and system of nano silicon carbide particle reinforced aluminum-based gradient composite material

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preparation example Construction

[0103] like Figure 22 , The present invention also relates to a preparation method of nano-silicon carbide particle reinforced aluminum-based gradient composite material, which adopts the above-mentioned preparation system of nano-silicon carbide particle-reinforced aluminum-based gradient composite material, and includes the following steps:

[0104] Step 1, solvent-assisted dispersion:

[0105] 1) Weigh the corresponding quality of nano-silicon carbide powder according to the predetermined volume fraction and pour it into the ultrasonic dispersion reaction cylinder 1 filled with absolute ethanol, and ultrasonically disperse it for 60min. In the mixing reaction cylinder 4, the 2014A1 alloy suspension is electromagnetically stirred by the magnetic stirrer 5; wherein,

[0106]

[0107] M 2 =M-M 1

[0108] Among them, M, M 1 and M 2 are the total weight of powder, the mass of nano-silicon carbide powder and the mass of 2014A1 alloy powder, ρ 1 and ρ 2 are the density...

Embodiment 1

[0120] Step 1, solvent-assisted dispersion:

[0121] 1) Weigh the corresponding quality of nano-silicon carbide powder according to the predetermined volume and pour it into a container filled with absolute ethanol for ultrasonic dispersion for 60min, while placing the corresponding quality 2014A1 alloy powder in a container filled with absolute ethanol. The alloy suspension is electromagnetically stirred;

[0122] 2) Add the suspension containing the silicon carbide reinforcement to the container containing the 2014A1 alloy suspension subsequently under magnetic stirring, continue magnetic stirring for 30min after adding, and let stand for settling;

[0123] 3) After the solution is clarified, pour out part of the clear liquid and dry it to obtain preliminary mixed powder;

[0124] Step 2, Mechanical Ball Milling:

[0125] The composite powder is mechanically ball-milled, and 1.0 wt% stearic acid is added in the process;

[0126] Step three, powder metallurgy:

[0127] Ac...

Embodiment 2

[0129] The steps are in Example 1 together;

[0130] Step 2 is the same as in Example 1;

[0131] Step three, powder metallurgy:

[0132] According to the method of step 1 and step 2, the nano-silicon carbide / 2014Al composite material powders with the volume of 3% and 5% of nano-silicon carbide were respectively prepared, and a layer of 3vol.% SiC / 2014A1 composite material powder was placed on the bottom layer of the mold. The head was cold-pressed for 2min under a pressure of 140MPa, the indenter was removed, a second layer of 5vol.% SiC / 2014A1 composite powder was placed, and the pressure was maintained under a pressure of 140MPa for 2min, until the two layers of composite powder with different SiC volume fractions were all put into And cold-pressed into billets.

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Abstract

The invention discloses a preparation method of a nano silicon carbide particle reinforced aluminum-based gradient composite material. The system comprises an ultrasonic dispersion reaction cylinder, an ultrasonic dispersion instrument, a lifting, overturning and clamping mechanism, a mixing reaction cylinder, a magnetic stirrer, a drying box, an industrial planetary ball mill, a gradient powder press, a vacuum furnace and a high-temperature furnace which are connected in sequence, the ultrasonic dispersion reaction cylinder is used for containing nano silicon carbide powder to be treated, the ultrasonic dispersion instrument is used for ultrasonically dispersing nano silicon carbide, and the mixing reaction cylinder is used for mixing turbid liquid containing silicon carbide reinforcement and 2014A1 alloy turbid liquid. Turbid liquid containing silicon carbide reinforcement in the reaction cylinder is ultrasonically dispersed through the lifting, overturning and clamping mechanism and added into the mixing reaction cylinder, the magnetic stirrer is used for stirring liquid in the mixing reaction cylinder, the drying box is used for drying preliminarily mixed powder, and the industrial planetary ball mill is used for grinding composite material powder, and the gradient powder press is used for extrusion forming of nanometer silicon carbide / 2014Al composite material powder. The tight combination of SiC and 2014A1 matrix is realized, elastic modulus, yield strength and tensile strength of the aluminum matrix are greatly improved, and plasticity of the composite material is not obviously sacrificed.

Description

technical field [0001] The invention relates to the technical field of aluminum alloy composite materials, in particular to a preparation method and system for nano-silicon carbide particle-reinforced aluminum-based gradient composite materials. Background technique [0002] Silicon carbide particle reinforced aluminum matrix composites have the advantages of low density, high specific modulus, high specific strength, low expansion, high thermal conductivity, good wear resistance, high damping and low cost. The civil field shows broad application prospects. The shortcomings of micron-sized SiCp / Al composites are that the strength increases but the plasticity decreases significantly, and the high-temperature mechanical properties are not satisfactory, which has become a bottleneck problem restricting its development. In recent years, it has been gradually proposed to use nano-SiC as a reinforcement to solve this problem. However, nano-sized SiC particles have high specific s...

Claims

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Application Information

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IPC IPC(8): B22F7/02B22F1/10B22F9/04B22F3/03B22F3/14B22F3/24
CPCB22F7/02B22F9/04B22F3/003B22F3/03B22F3/14B22F3/24B22F2009/043B22F2999/00B22F2003/248B22F2207/03
Inventor 陈良李志刚赵国群钱钊张存生
Owner SHANDONG UNIV
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