Low contact resistance type resistance paste
A technology of low contact resistance and resistance paste, which is applied in the direction of sliding contact resistors, resistors, adjustable resistors, etc., can solve the problems of contact point heating and sparking, resistor failure, etc., to achieve smooth surface and small contact resistance , the effect of strong process adaptability
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[0022] 1. Preparation of conductive powder
[0023] Preparation of Conductive Phase 1:
[0024] Step 1: Dissolve ruthenium nitrate in pure water to form Ru 3+ Solution A with an ion concentration of 1 mol / L; dissolve lead nitrate in pure water to form Pb 2+ Solution B with an ion concentration of 1 mol / L; adding graphyne into pure water to form a suspension C with a graphyne concentration of 5 g / L.
[0025] Step 2: Follow Ru 3+ with Pb 2+ The molar ratio was 1:1, 500 mL of solution A and 500 mL of solution B were added dropwise to 1000 mL of suspension C under stirring conditions. After the dropwise addition of solutions A and B, the stirring was stopped and allowed to stand for 24 hours.
[0026] Step 3: Extract the upper layer liquid of the sediment from the solution after standing, add pure water to the extracted liquid, stir for 10 minutes, and leave it for 24 hours.
[0027] Step 4: After repeating the operation of Step 3 twice, the bottom sediment was suction filter...
Embodiment 2
[0059] In Example 2 and Comparative Examples 1 and 2, graphite composite lead ruthenate and carbon black composite lead ruthenate are used as conductive phases to compare, and it is illustrated that graphdiyne composite lead ruthenate is used as conductive phase to obtain excellent temperature coefficient, electrostatic discharge, The package change rate and the contact resistance are small.
[0060] Example 2 is compared with Comparative Examples 3, 4, 5, and 6, which shows that when the chemical deposition method is used to prepare the graphdiyne composite lead ruthenate, it is necessary to pass the freeze-drying and vacuum calcination process, and it is applied in the resistance slurry to obtain excellent temperature coefficient. , The contact resistance is small.
[0061] Example 2 is compared with Comparative Examples 7 to 14, indicating that whether it is directly composited with ruthenium dioxide and lead oxide and graphdiyne, carbon black or graphite, or directly compo...
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