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Novel antistatic heat-resistant glue and preparation method thereof

An anti-static and heat-resistant technology, applied in the direction of adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve the problems of electrostatic breakdown of displays, small size of light-emitting LEDs, falling off of product components, etc., to improve anti-static effect, the effect of improving heat resistance

Pending Publication Date: 2022-03-22
NINGBO DXC NEW MATERIAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Compared with traditional backlights, Mini-LED has more advantages and is suitable for high-end liquid crystal display solutions. However, due to the small size of the light-emitting LED, the display is prone to electrostatic breakdown during the preparation and assembly process, resulting in LED inactivation, and Compared with traditional displays, a large number of LEDs emit more heat during use, which can easily make ordinary adhesives less viscous and cause problems such as product components falling off

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Embodiment 1, a new type of antistatic heat-resistant glue, consists of the following components in parts by mass:

[0034] Acrylic resin 100 parts,

[0035] 20 parts of acrylonitrile-butadiene-styrene copolymer,

[0036] 6 parts of silicon dioxide,

[0037] As anti-aging agent 2, 5 parts of 4-dinitrophenols,

[0038] Chromium complex coupling 1 part,

[0039] 3 parts of ammonium dihydrogen phosphate as an antibacterial preservative,

[0040] 10 parts of absolute ethanol,

[0041] 15 parts of methyl silicone resin,

[0042] 20 parts of phenyl hydrogen-containing silicone resin,

[0043] 5 parts of dicumyl peroxide as crosslinking agent,

[0044] Polysiloxane defoamer 2 parts,

[0045] Zinc oxide 0.1 part,

[0046] 0.5 part of graphene sheet,

[0047] 3.5 parts of carbon nanotubes;

[0048] Silicon nitride 2 parts.

Embodiment 2

[0049] Embodiment 2, a new type of antistatic heat-resistant glue, consists of the following components in parts by mass:

[0050] Acrylic resin 100 parts,

[0051] 10 parts of acrylonitrile-butadiene-styrene copolymer,

[0052] 8 parts of silicon dioxide,

[0053] 2 parts of N-isopropyl-N`-phenyl-p-phenylenediamine as an anti-aging agent,

[0054] 4 parts of silane coupling agent,

[0055] 1 part of sorbic acid as an antibacterial preservative,

[0056] 1 part absolute ethanol,

[0057] 18 parts of methyl silicone resin,

[0058] 25 parts of phenyl hydrogen-containing silicone resin,

[0059] 1 part of benzoyl peroxide as a crosslinking agent,

[0060] 4 parts of polyether modified silicone oil defoamer,

[0061] 3 parts of zinc oxide,

[0062] 0.1 part of graphene sheet,

[0063] 1.5 parts of carbon nanotubes;

[0064] 0.1 parts of silicon nitride.

Embodiment 3

[0065] Embodiment 3, the new antistatic heat-resistant glue is composed of the following components in parts by mass:

[0066] Acrylic resin 100 parts,

[0067] 50 parts of acrylonitrile-butadiene-styrene copolymer,

[0068] 2 parts of silicon dioxide,

[0069] 1 part of 4,4'-dimethoxydiphenylamine as an anti-aging agent,

[0070] 5 parts of titanate coupling agent,

[0071] Ammonium sorbate 4 parts as an antibacterial preservative,

[0072] 5 parts of absolute ethanol,

[0073] 10 parts of methyl silicone resin,

[0074] 15 parts of phenyl hydrogen-containing silicone resin,

[0075] 2 parts of 2,5-dimethyl-2,5 di-tert-butylperoxyhexane as a crosslinking agent,

[0076] 1 part of trialkylmelamine as antifoaming agent,

[0077] 0.8 parts of zinc oxide,

[0078] 5 parts of graphene sheet,

[0079] 0.1 parts of carbon nanotubes;

[0080] 1 part of silicon nitride.

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Abstract

The novel antistatic heat-resistant glue is prepared from the following components in parts by mass: 100 parts of acrylic resin, 10-50 parts of an acrylonitrile-butadiene-styrene copolymer, 2-10 parts of silicon dioxide, 1-5 parts of an anti-aging agent, 1-5 parts of a coupling agent, 1-5 parts of an antibacterial preservative and 1-10 parts of absolute ethyl alcohol. The coating is prepared from the following components in parts by weight: 5-20 parts of methyl silicone resin, 10-30 parts of phenyl hydrogen-containing silicone resin, 1-5 parts of a cross-linking agent, 1-5 parts of a defoaming agent, 0.1-5 parts of zinc oxide, 0.1-5 parts of graphene sheets, 0.1-5 parts of carbon nanotubes and 0.1-5 parts of silicon nitride. According to the invention, zinc oxide, graphene sheets and carbon nanotubes are selected to form a three-dimensional conductive network through a point-line-plane conduction mode, so that the antistatic effect of the glue is effectively improved; the methyl silicone resin, the phenyl hydrogen-containing silicone resin and the silicon nitride filler are selected, so that the heat resistance and aging resistance of the glue are improved, the viscosity of the glue can be adjusted by adjusting the ratio of the methyl silicone resin to the phenyl hydrogen-containing silicone resin, and the glue can adapt to more application scenes.

Description

technical field [0001] The invention relates to a glue and a preparation method of the glue. Background technique [0002] With the advent of the intelligent age, the rapid development of the electronics industry and the semiconductor industry, and the increasingly high level of integrated electronic equipment, the requirements for antistatic performance and heat resistance of products are getting higher and higher. [0003] The Mini-LED backlight module uses Mini-LED as the backlight to reduce the size of the direct-type LED backlight module, and turns dozens of LED lamp beads into thousands, tens of thousands, or even more lights. beads. Compared with traditional backlights, Mini-LED has more advantages and is suitable for high-end liquid crystal display solutions. However, due to the small size of the light-emitting LED, the display is prone to electrostatic breakdown during the preparation and assembly process, resulting in LED inactivation, and Compared with tradition...

Claims

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Application Information

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IPC IPC(8): C09J133/00C09J183/04C09J183/05C09J11/04C09J11/06C09J11/08
CPCC09J133/00C09J11/04C09J11/06C09J11/08C08L2201/04C08L2201/08C08K2201/017C08K2201/011C08K2003/2296C08L55/02C08L83/04C08K3/22C08K3/042C08K3/041C08K3/34
Inventor 罗培栋罗秋萍赵程周云姣赵伯培
Owner NINGBO DXC NEW MATERIAL TECH