Silicon carbide composite substrate for preparing nitride single crystal film
A technology of silicon carbide substrate and composite substrate, which is applied in the direction of single crystal growth, single crystal growth, crystal growth, etc. Thin and other problems, to shorten the production cycle, improve quality, reduce the effect of scrap rate
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[0037] First, the silicon carbide substrate is plasma cleaned. A mixture of hydrogen and nitrogen is introduced into the cleaning chamber, the flow ratio of hydrogen and nitrogen is 3:1; the microwave power is 800w; the cleaning temperature is 1000°C; the cleaning time is 60 minutes.
[0038] Put the cleaned silicon carbide substrate on the lifting platform in the reaction chamber, and adjust the height of the lifting platform so that the distance between the highest point on the upper surface of the silicon carbide substrate and the top wall of the reaction chamber is 5 μm. Then, evacuate to a pressure of 1*10 in the reaction chamber -6 After Pa, feed SiO gas and N at a flow ratio of 3:2 2 , when p(O 2 ) / pθ=10 -19 , p(SiO) / pθ=6.0*10 1.0 , that is, when the SiO partial pressure p(SiO)=6.0MPa (where p(O 2 ) is the partial pressure of oxygen, pθ is the standard atmospheric pressure), stop feeding SiO gas and nitrogen, and then heat the silicon carbide substrate to 2000°C to c...
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