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Step-by-step hot isostatic pressing method for additive manufacturing of nickel-based superalloy

A nickel-based superalloy, hot isostatic pressing technology, applied in the field of additive manufacturing processing, can solve the problems of directional grain growth, difficulty in improving material properties, material instability, etc., to achieve increased density and tensile strength, Improve the density and mechanical properties, optimize the effect of the structure

Active Publication Date: 2022-06-28
CENT SOUTH UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The short interaction time of the high-speed high-energy laser in the local area leads to a large thermal gradient, which leads to the existence of high thermal stress and makes the material unstable
Rapid solidification of thin layers by high cooling rates will lead to directional grain growth, micro-segregation of high-concentration refractory elements, formation of non-equilibrium phases, including carbides and Laves phases, and will also inhibit the precipitation of γ″ phases, resulting in mechanical properties decline
It is difficult to improve the performance of the material by using the previous processing methods, and it is impossible to take advantage of the advantages of additive manufacturing

Method used

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  • Step-by-step hot isostatic pressing method for additive manufacturing of nickel-based superalloy
  • Step-by-step hot isostatic pressing method for additive manufacturing of nickel-based superalloy

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] (1) GH4169 nickel-based superalloy was prepared by selective laser melting technology;

[0033] (2) Carry out the first hot isostatic pressing under the conditions of a pressure of 80MPa, a temperature of 900°C, and a time of 2.5h; perform a second hot isostatic pressing under the conditions of a pressure of 80MPa, a temperature of 700°C, and a time of 9h;

[0034] (3) The processed additively manufactured GH4169 nickel-based superalloy was air-cooled to room temperature, and the cooling rate was 70°C / s.

[0035] The processed additively fabricated GH4169 nickel-based superalloy was observed by scanning electron microscopy, as figure 2 As shown, the precipitation of γ″ and σ phases can be clearly seen.

[0036] The processed additively manufactured GH4169 nickel-based superalloy was cut into block samples and tensile samples with a wire cutting machine, and the samples were ground and polished to test the density and mechanical properties. The test results are shown i...

Embodiment 2

[0038] (1) GH4169 nickel-based superalloy was prepared by selective laser melting technology;

[0039] (2) Carry out the first hot isostatic pressing under the conditions of a pressure of 90MPa, a temperature of 800°C, and a time of 3h; carry out the second hot isostatic pressing under the conditions of a pressure of 85MPa, a temperature of 700°C, and a time of 9h;

[0040] (3) The processed additively manufactured GH4169 nickel-based superalloy was air-cooled to room temperature, and the cooling rate was 70°C / s.

[0041] The treated additively manufactured GH4169 nickel-based superalloy was cut into block samples and tensile samples with a wire cutting machine, and the samples were ground and polished to test the density and mechanical properties. The test results are shown in Table 1.

Embodiment 3

[0043] (1) GH4169 nickel-based superalloy was prepared by selective laser melting technology;

[0044] (2) Carry out the first hot isostatic pressing under the conditions of a pressure of 80MPa, a temperature of 1000°C and a time of 3.5h; perform a second hot isostatic pressing under the conditions of a pressure of 90MPa, a temperature of 720°C and a time of 10h;

[0045] (3) The processed additively manufactured GH4169 nickel-based superalloy was air-cooled to room temperature, and the cooling rate was 70°C / s.

[0046] The treated additively manufactured GH4169 nickel-based superalloy was cut into block samples and tensile samples with a wire cutting machine, and the samples were ground and polished to test the density and mechanical properties. The test results are shown in Table 1.

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Abstract

The invention discloses a step-by-step hot isostatic pressing method for additive manufacturing of nickel-based superalloy and a preparation method thereof, and the method comprises the following steps: providing the nickel-based superalloy prepared by an additive manufacturing technology; carrying out first hot isostatic pressing at the sigma phase precipitation temperature T1 of the nickel-based high-temperature alloy; and carrying out second hot isostatic pressing at the gamma ''phase precipitation temperature T2 of the nickel-based high-temperature alloy. According to the method, diffusion of segregation elements is promoted, the organization structure is optimized, the organization is relatively uniform, and the density and the mechanical property are improved.

Description

technical field [0001] The invention belongs to the technical field of additive manufacturing and processing, and particularly relates to a step-by-step hot isostatic pressing method for additively manufacturing nickel-based superalloys. Background technique [0002] As one of nickel-based superalloys, GH4169 alloy has excellent corrosion resistance, heat resistance and strength properties under extreme thermal and mechanical conditions, and is commonly used in the manufacture of engine turbine disks, turbine rotor blades and other mechanically fastened components. However, both excessive tool wear and low material removal rates during machining make the alloy difficult to machine. In addition, many GH4169 elements are complex in shape, with labyrinthine or overhanging internal channels, which are difficult to manufacture by traditional processes (eg, forging, rolling, and casting). [0003] Selective Laser Melting (SLM) is a rapid prototyping additive manufacturing (AM) te...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/04B22F3/15B22F3/16B22F10/28B33Y10/00
CPCC22C1/0433B22F3/15B22F3/16B22F10/28B33Y10/00Y02P10/25
Inventor 袁铁锤周翔幸李瑞迪易出山黄敏刘若愚吕亮谌曲平马鑫罗强
Owner CENT SOUTH UNIV