Preparation and use of raw liquid of ceratin of animal hairs
A technology of keratin and animal hair, which is applied in the field of extracting animal hair keratin stock solution, can solve the problems of unusable industrial production and sewage environment, and achieve the effects of preventing oxidation, high yield and enhancing stability
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[0032] Example 1
[0033] At 20°C, sodium sulfite, cyclopentacarbamide, and sodium dodecylbenzene sulfonate are combined into a combined reducing agent at different concentrations of 0.3mol / L, 1.2mol / L, and 0.8mol / L, respectively. The above compound is put into the reactor of the biochemical equipment, under stirring conditions, the stirring speed is 30rpm, the normal pressure and the temperature is 20-60℃, the heating time is 7 minutes, the heating time of 60-110℃ is 9 minutes, 110-150 The temperature rise time is 7 minutes to make it react with each other. At this time, the pH value of the measured solution rises from 7 to 8, the reaction is over, and then stand for 50 minutes to obtain the combined reducing agent;
[0034] Weigh the raw wool (wool without textile value) and the mass-to-volume ratio of the above-mentioned combined reagent solution at a ratio of 5:5 (weigh in two times, each with a ratio of 1 / 4, 3 / 4). In this reagent solution, the temperature of the solution is r...
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[0036] Example 2:
[0037] Sodium sulfite, cyclopentacarbamide, and sodium dodecylbenzene sulfonate were combined into a solution at 20°C with different concentrations of 1.0mol / L, 4.5mol / L, 3.2mol / L, and the above compounds Put it into the reactor of biochemical equipment, under stirring conditions, stirring speed 35rpm, normal pressure and temperature 20-60℃, the heating time is 8 minutes, 60-110℃ heating time is 10 minutes, 110-150℃ heating The time is 8 minutes to make it react with each other. At this time, the pH value of the measuring solution rises from 7 to 8, the reaction is over, and then it is left standing for 60 minutes to obtain the combined reducing agent;
[0038]Weigh an appropriate amount (weigh in two times, each with a ratio of 1 / 4, 3 / 4) according to the mass product ratio of the raw material wool and the above-mentioned combined reagent solution at a ratio of 5:5, and place the raw material wool in the reagent solution. The temperature is increased stepwise b...
Example Embodiment
[0040] Example 3:
[0041] At 20 ℃, potassium sulfite, carboamide peroxide, and sodium n-tetradecyl sulfate are combined to prepare solutions at different concentrations of 0.5 mol / L, 1.8 mol / L, and 1.6 mol / L, respectively, under stirring conditions , The stirring speed is 50rpm, under normal pressure and the temperature is 20-60℃, the heating time is 8 minutes, the heating time of 60-110℃ is 9 minutes, and the heating time of 110-150℃ is 7.5 minutes to make it react with each other. The pH value of the solution rises from 7 to 8, the reaction is over, and then it is allowed to stand for 60 minutes to obtain the combined reducing agent;
[0042] Weigh an appropriate amount (weigh in two times, each with a ratio of 1 / 4, 3 / 4) according to the mass product ratio of the raw material wool and the above-mentioned combined reagent solution at a ratio of 5:5, and place the raw material wool in the reagent solution. The temperature is increased stepwise between 60-95℃±1℃, the heating rate ...
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