Method and device for preparing metal-based composite material by electric current direct heating dynamic sinter hot pressing
A technology for composite material and preparation device, which is applied in the field of current direct heating dynamic sintering and hot pressing preparation of metal matrix composite materials, can solve problems such as technical and theoretical problems yet to be studied, and achieves shortening powder sintering time, improving production efficiency and saving energy. energy effect
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Embodiment 1
[0048] The present invention adopts electric current direct heating dynamic sintering hot pressing furnace, as figure 1 As shown, the current direct heating dynamic sintering hot-press furnace is composed of five parts, and the connection sequence is as follows: circuit control system, induction voltage regulator, dry-type transformer, hot-press furnace and computer data acquisition system.
[0049] Such as figure 2 As shown, the output terminal of the circuit control system is connected to the input terminal of the induction voltage regulator 1 , and the circuit control system provides a periodically changing working current, which is input to the induction voltage regulator 1 . The function of the induction voltage regulator 1 is to complete the first voltage regulation, and the input voltage can be changed by controlling the induction voltage regulator 1 . It can adjust the voltage from 220V to 100-500V. The input end of the dry-type transformer 16 is connected to the ou...
Embodiment 2
[0053] The preparation of the iron-based composite material reinforced with 10% SiC particles by volume percentage (with the addition of 0.5-1% zinc stearate by mass fraction) is carried out by pressing and forming by general powder metallurgy sintering method, in the protective atmosphere of decomposing ammonia Sintering, the sintering temperature is 1110-1150°C, heat preservation for 1-1.5 hours, its performance is shown in Table 2:
[0054] SiC volume number
[0055] Using the current direct heating dynamic sintering and hot pressing process of the present invention, the mechanical properties of the iron-based composite material containing 10% SiC by volume percentage prepared by direct heating and sintering for different times (interval 100s) under the output voltage of the induction transformer 360V are shown in Table 3:
[0056] Sintering time / (S)
[0057] It can be seen from Table 2 and Table 3 that the mechanical properties (tensile strength and hard...
Embodiment 3
[0059] For the current direct heating sintering process, if the mold is not treated, the current will pass through the mold and the sintered material at the same time. This process can be defined as an ordinary current dynamic hot pressing sintering process; and the current direct heating dynamic sintering hot pressing process of the present invention Through the processing of the mold, the current passes completely through the material to be sintered. The mechanical properties of the volume percentage 10% SiC iron-based composite material sintered by these two processes are shown in Table 4:
[0060]
[0061] It can be seen that the density and mechanical properties of the samples prepared by direct current heating dynamic sintering process are higher than those of ordinary current heating hot pressing sintering process. Therefore, the improvement of the mold set by this process is absolutely necessary.
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