Method for testing Chinese medicinal composition for treating painful swelling of throat and constipation
A technology for constipation and sore throat, applied in the direction of drug combinations, pharmaceutical formulas, plant raw materials, etc., can solve the problems of low bioavailability, large swallowing volume, incomplete absorption, etc.
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Embodiment 1
[0067] Embodiment 1: Chinese medicine composition for treating sore throat and constipation. Preparation of Qingjiang Gel:
[0068] 1) Preparation prescription:
[0069]
[0070]
[0071] 2) Preparation method: according to claim 1, the raw material drug composition of the active ingredient is fed:
[0072] Rhubarb powder is made into the coarsest powder, mixed with Indigo Daisy, Scrophulariaceae, and Fritillaria, and extracted twice with 80% ethanol, each time for 1.5 hours, combined with the alcohol extract, recovered ethanol and concentrated into a paste, with a relative density of 1.30-1.35 , 60°C;
[0073] Moutan cortex is made into the coarsest powder, mixed with silkworm excrement, saponin, red peony root, Ophiopogon japonicus, forsythia, honeysuckle, banlangen, rehmannia root, Imperata rhizome, mint, licorice, and boiled twice with 10 times the amount of water, each time After 1.5 hours, collect the volatile oil, filter the water extract several times, combine ...
Embodiment 2
[0075] Embodiment 2: Qingjiang gel quality standard
[0076] [Prescription] Silkworm excrement 400 Rhubarb 400 Scrophulariaceae 400 Saponaria 400 Radix Paeoniae Rubra 400 Ophiopogon japonicus 400 Forsythia 400 Banlangen 400 Rehmannia glutinosa 400 Honeysuckle 400 Imperata rhizome 400 Peony bark 260 Indigo Daisy 200 Chuan Fritillaria 200 Mint 200 Licorice 132
[0077] [Preparation method] The above sixteen flavors, rhubarb powder into the coarsest powder, mixed with Qingdai, Scrophulariaceae, Chuan Fritillaria, add 8 times the amount of 80% ethanol to extract twice, each time for 1.5 hours, combine alcohol extracts, recover ethanol and concentrate Make a paste (relative density 1.30-1.35, 60°C). Moutan cortex is ground into the coarsest powder, mixed with silkworm excrement, saponins, red peony root, Ophiopogon japonicus, forsythia, honeysuckle, banlangen, rehmannia root, courgette root, mint, licorice, add 10 times the amount of water to decoct twice, each time After 1.5 hour...
Embodiment 3
[0098] Example 3: Drafting instructions for the quality standard draft of Qingjiang gel
[0099] This product is a gel made from silkworm excrement, rhubarb and other sixteen medicinal materials, which are extracted, mixed and made respectively. The relevant issues in the quality standard draft of Qingjiang Gel are explained as follows:
[0100] The gel under the item [properties] of this standard is in the form of gel, and after being separated from the packaging container, it can basically maintain the original shape, the tissue is soft and moderate, full of elasticity, fine and uniform, and there is no obvious floc.
[0101] Under this standard [identification]
[0102](1) For the TLC identification test of Radix Paeoniae Rubra in the prescription, paeoniflorin was used as the reference substance, and a negative sample lacking Radix Paeoniae Rubra was made according to the prescription ratio, and the negative control solution was prepared according to the preparation metho...
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