Asymetric membrane FeAl intermetallic compound porosint filter element and application thereof
A technology of intermetallic compounds and filter elements, which is applied in the fields of filtration and separation, chemical instruments and methods, and gas dust removal, can solve the problems of severe corrosion of washing equipment, long purification process, and fast decay of filtration capacity, and achieve good resistance to high temperature oxidation/ Vulcanization performance, expansion of the use environment range, and the effect of reducing penetration resistance
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Embodiment 1
[0050] The preparation of embodiment 1 filter element
[0051] The Fe powder with an average particle size of 100 μm and the Al powder with an average particle size of 90 μm are mechanically mixed according to the ratio of Fe-30at% Al (that is, the number of Fe atoms is 70% of the total number of atoms), and then they are molded at 240 MPa by ordinary molding. Press the sheet blank (¢350×4.0mm) under the pressure. Sintering is carried out in a vacuum atmosphere, and the vacuum degree is controlled at 1.0×10 -1 ~1.0×10 -2 Pa. First, sinter at 130°C for 45 minutes to remove the adsorbed moisture. Subsequently, medium-temperature solid phase diffusion was carried out at a temperature of 520° C. for 60 minutes. The final high-temperature component homogenization and structural stabilization treatment temperature is 1050°C, time is 120 minutes, cooling, and a FeAl intermetallic compound porous support with a maximum pore size of 35 μm and a porosity of 43% is obtained.
[0052...
Embodiment 2
[0055] The preparation of embodiment 2 filter element
[0056] Fe powder with an average particle size of 5 μm and Al powder with an average particle size of 10 μm are mechanically mixed according to the proportion of Fe-60at% Al, and then pressed into a sheet-shaped blank (¢300×3.5 mm). Sintering is carried out in a vacuum atmosphere, and the vacuum degree is controlled at 1.0×10 -1 ~1.0×10 -2 Pa. First, heat at 150°C for 50 minutes; then, carry out medium-temperature solid phase diffusion at 560°C for 120 minutes. The final high-temperature component homogenization and tissue structure stabilization treatment temperature is 1100° C., and the time is 30 minutes. A FeAl intermetallic compound porous support with a maximum pore size of 12 μm and a porosity of 38% was prepared.
[0057] Fe and Al powders with an average particle size of 1.0 μm were mixed in the proportion of Fe-60at% Al to obtain a powder mixture; ethylene glycol and polyvinyl alcohol were mixed in a mass r...
Embodiment 3
[0060] The preparation of embodiment 3 filter element
[0061]Fe powder with an average particle size of 40 μm and Al powder with an average particle size of 30 μm are mechanically mixed in the proportion of Fe-40at% Al, and then pressed under a pressure of 180 MPa by cold isostatic pressing, and the taper of the pressed core rod is 1.8 °, after manual demoulding, a tubular shaped blank (Φ50*300mm) with a slightly tapered inner diameter (3°) is obtained. Sintering is carried out in a vacuum atmosphere, and the vacuum degree is controlled at 1.0×10 -1 ~1.0×10 -2 Pa. First, heat at 120°C for 30 minutes to remove the adsorbed water; then, carry out medium-temperature solid-phase diffusion at 600°C for 120 minutes. The final temperature of the high-temperature component homogenization and structural stabilization treatment is 1200° C. for 90 minutes, and the FeAl intermetallic compound porous support is prepared.
[0062] Fe and Al powders with an average particle size of 1.5 ...
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