Preparation of white titanium pigment double action crystal seed from metatitanic acid
A technology of double-effect crystal seed and metatitanic acid, which is applied in the direction of titanium dioxide, titanium oxide/hydroxide, fibrous filler, etc., can solve the problems of complicated preparation process, increased production cost, and product quality fluctuation, and achieve uniform particle size distribution , save investment, improve the effect of product grade
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Embodiment 1
[0077] Embodiment 1: described percentage is weight percentage; Said every part is weight part;
[0078] (1) Alkali soluble
[0079] Take [Fe 2 o 3 ]2 o 3 ]<0.01%, 128g of liquid caustic soda with a concentration of 30%, and the weight ratio of alkali to titanium is 1.2; the preheating temperature of metatitanic acid during alkali dissolution: 60°C, the preheating temperature of NaOH: 110°C; Adding speed: add dropwise for 5 minutes; then boil together, alkali cooking time: 120 minutes, add water after ripening: 180ml, temperature of sodium titanate after cooling: 55°C.
[0080] (2) washing
[0081] Pour the reactant into a Buchner funnel for water washing, and use desalted water with a resistivity greater than 100,000 ohm cm to wash away Na 2 SO 4 and excess NaOH, and at the same time, part of the alkali metal titanate is hydrolyzed to form orthotitanic acid during the water washing process. After adding 100ml of water to the reaction bottle, add the filter cake, start s...
Embodiment 2
[0086] Embodiment 2: described percentage is weight percentage; Said every part is weight part;
[0087] (1) Alkali soluble
[0088] Take [Fe 2 o 3 ]2 o 3 ]<0.01%, 176g of liquid caustic soda with a concentration of 30%, and the weight ratio of alkali to titanium is 1.65; the preheating temperature of metatitanic acid during alkali dissolution: 60°C, the preheating temperature of NaOH: 100°C; Adding speed: add dropwise for 5 minutes; then boil together, alkali cooking time: 120 minutes, add water after ripening: 160ml, temperature of sodium titanate after cooling: 60°C.
[0089] (2) washing
[0090] Pour the reactant into a Buchner funnel for water washing, and use desalted water with a resistivity greater than 100,000 ohm cm to wash away Na 2 SO 4 and excess NaOH, and at the same time, part of the alkali metal titanate is hydrolyzed to form orthotitanic acid during the water washing process. After adding 100ml of water to the reaction bottle, add the filter cake, start ...
Embodiment 3
[0095] Embodiment 3: described percentage is weight percentage; Said every part is weight part;
[0096] (1) Alkali soluble
[0097] Take [Fe 2 o 3 ]2 o 3 ]<0.01%, 160g of liquid caustic soda with a concentration of 30%, and the weight ratio of alkali to titanium is 1.5; the preheating temperature of metatitanic acid during alkali dissolution: 60°C, the preheating temperature of NaOH: 120°C; Adding speed: add dropwise for 5 minutes; then boil together, alkali cooking time: 120 minutes, add water after ripening: 180ml, temperature of sodium titanate after cooling: 60°C.
[0098] (2) washing
[0099] Pour the reactant into a Buchner funnel for water washing, and use desalted water with a resistivity greater than 100,000 ohm cm to wash away Na 2 SO 4 and excess NaOH, and at the same time, part of the alkali metal titanate is hydrolyzed to form orthotitanic acid during the water washing process. After adding 100ml of water to the reaction bottle, add the filter cake, start s...
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