Copper-zinc-tin-sulfur quaternary compound, thin film solar cell formed by same, and preparation method thereof
A technology of thin-film solar cells and quaternary compounds, which is applied in the manufacture of circuits, electrical components, and final products, can solve problems such as hindering the photovoltaic performance of thin-film solar cells, difficult to control product stoichiometry, and difficult to remove organic solvents, and achieve stoichiometric The effect of easy control, adjustable, strong adhesion and low cost
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Embodiment 1
[0017] (1), preparation of copper-zinc-tin-sulfur quaternary compound powder:
[0018] Mix copper sulfide, zinc sulfide, and stannous sulfide in a molar ratio of 1:0.2:0.2, then add them to an appropriate amount of water, and mill them in a ball mill for more than one hour; ℃ treatment for more than two hours, that is, copper zinc tin sulfur quaternary compound powder;
[0019] (2), preparation of copper-zinc-tin-sulfur quaternary compound film:
[0020] Use the aluminum dihydrogen phosphate solution or the mixed solution of aluminum oxide and aluminum dihydrogen phosphate or the mixed solution of copper oxide and aluminum dihydrogen phosphate as the adhesive, mix the copper-zinc-tin-sulfur quaternary compound powder with the adhesive, and then coat the film , dried at 40°C, and then dried and cured at 400°C for more than one hour to obtain a copper-zinc-tin-sulfur quaternary compound film.
[0021] (3) Assembly of p-copper zinc tin sulfur quaternary compound / n-tin disulfide...
Embodiment 2
[0024] Mix copper sulfide, zinc sulfide, and stannous sulfide in a molar ratio of 1:0.8:0.8, then add them to an appropriate amount of water, and ball mill them in a ball mill for more than one hour; ℃ treatment for more than two hours to obtain copper-zinc-tin-sulfur quaternary compound powder; others are the same as in Example 1.
Embodiment 3
[0026] Mix copper sulfide, zinc sulfide, and stannous sulfide in a molar ratio of 1:0.5:0.5, then add them to an appropriate amount of water, and ball mill them in a ball mill for more than one hour; ℃ treatment for more than two hours to obtain copper-zinc-tin-sulfur quaternary compound powder; others are the same as in Example 1.
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