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32 results about "Tin(II) sulfide" patented technology
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Tin(II) sulfide is a chemical compound of tin and sulfur. The chemical formula is SnS. Its natural occurrence concerns herzenbergite (α-SnS), a rare mineral. At elevated temperatures above 905K, SnS undergoes a second order phase transition to β-SnS (space group: cmcm, No. 63). in recent years, it has become evident that a new polymorph of SnS exist based upon the cubic crystal system, π-SnS (space group: P2₁3, No. 198).
Tin sulfide film solar battery
InactiveCN101378090AAbundant on EarthWide range of sourcesPhotovoltaic energy generationSemiconductor devicesHeterojunctionComposite film
A tin sulfide thin film solar cell comprises a conductive glass / metal gate electrode and a metal back electrode and is characterized in that uni-junction or multi-junction n-SnS2 or the composite thin film thereof and p-SnS or the composite thin film thereof are formed between the conductive glass / metal gate electrode and the metal back contact. The composite means the tin sulfide obtained by doping tin bromide (n-SnS2) and stannous sulfide (p-SnS). The solar cell is rich in material sources, safe and environment-friendly, convenient in processing and effectively solves the collection problem of current carriers with the aid of such electrodes as metallic tin by using SnS2 and SnS, which have the same components and different conduction types and liable to realize energy gap match, heterojunction transition and good transport property of the current carriers.
Owner:HEFEI UNIV OF TECH
Stannous sulfide nanometer photo-thermal agent and preparation method thereof
InactiveCN108175858AExcellent photothermal performanceGood chemical stabilityEnergy modified materialsNanomedicinePolyethylene glycolTreatment field
The invention provides a stannous sulfide nanometer photo-thermal agent. The stannous sulfide nanometer photo-thermal agent is prepared from a stannous sulfide nanometer sheet, and polyethylene glycolamine, wherein the polyethylene glycol amine is covered to the surface of the stannous sulfide nanometer sheet. The stannous sulfide nanometer photo-thermal agent has the advantages that the photo-thermal effect is obvious, the chemical stability is high, the toxicity is low, the rich raw materials are provided, the prices are low, the preparation method is simple, and the application prospect isbroad in the field of photo-thermal treatment. The invention also provides a preparation method of the stannous sulfide nanometer photo-thermal agent.
Owner:SHENZHEN UNIV
Preparation method of stannous sulfide/nitrogen-doped carbon composite ball-flower and application in lithium ion battery negative electrode
ActiveCN108539136AMultiple lithium storage active sitesExcellent electrochemical lithium storage performanceMaterial nanotechnologyCell electrodesCarbon compositesLyonium ion
The invention discloses a preparation method of stannous sulfide / nitrogen-doped carbon composite ball-flower. The preparation method comprises the following steps: S1, preparing an aqueous solution ofamino glucose hydrochloride and sodium stannate, wherein the concentration of amino glucose hydrochloride is 0.10 to 0.25 mol / L, and the concentration of stannate ions of sodium stannate is 0.02 to 0.07 mol / L; S2, adding L-cysteine into an aqueous solution of S1, and obtaining a mixed solution; S3, enabling the mixed solution to have hydrothermal reaction, and obtaining a precursor; and S4, calcining the precursor in an inertial gas atmosphere, and obtaining a stannous sulfide / nitrogen-doped carbon composite ball-flower. The prepared stannous sulfide / nitrogen-doped carbon composite ball-flower has large specific surface area, more lithium storage active sites, can provide more short lithium ion diffusion channels, can improve the electrochemical lithium storage performance, and has high specific capacity and excellent cycling stability in a lithium ion battery.
Owner:LINGNAN NORMAL UNIV
Copper-zinc-tin-sulfur quaternary compound, thin film solar cell formed by same, and preparation method thereof
InactiveCN101794826ARich sourcesThe stoichiometric ratio is easy to control and adjustableFinal product manufactureSemiconductor devicesHigh pressureTin(II) sulfide
The invention discloses a copper-zinc-tin-sulfur quaternary compound, a thin film solar cell formed by the same, and a preparation method thereof. The thin film solar cell comprises a conductive glass / metal gate electrode and a metal backing electrode, and is characterized in that: a p-copper-zinc-tin-sulfur quaternary compound thin film and an n-stannic sulfide thin film which form a p-n structure are arranged between the conductive glass / metal gate electrode and the metal backing electrode. The preparation method for the copper-zinc-tin-sulfur quaternary compound comprises the following steps: mixing copper sulfide, zinc sulfide and stannous sulfide in a mole ratio of 1:0.2-0.8:0.2-0.8; adding the mixture into an appropriate amount of water and performing ball grinding for more than 1 hour; transferring the obtained mixed liquid to a high-pressure autoclave; and performing hydro-thermal treatment for more than 2 hours at the temperature of between 120 and 280 DEG C to obtain copper-zinc-tin-sulfur quaternary compound powder. The thin film solar cell prepared by the invention has the advantages of strong adhesive force, low resistance and rich raw material sources; and the preparation method has the advantages of simple preparation process, low cost and environmental friendliness.
Owner:HEFEI UNIV OF TECH
Molybdenum disulfide and double-carbon-layer co-modified stannous sulfide nanospheres and preparation method thereof
InactiveCN109873149ASmall sizeControl shapeCell electrodesSecondary cellsTin dioxidePhosphomolybdic acid
The invention discloses molybdenum disulfide and double-carbon-layer co-modified stannous sulfide nanosphere and a preparation method thereof; the preparation method comprises the following steps of by taking sodium stannate and glucose as raw materials, preparing stannic oxide nanospheres by using a hydrothermal method, then dispersing the nanospheres into an aqueous solution containing phosphomolybdic acid and pyrrole, and carrying out stirring and complete mixing, so that phosphomolybdic acid and pyrrole are polymerized on the surface of the stannic oxide nanospheres to obtain a precursor template; and placing the precursor template in a tubular furnace, and carrying out high-temperature reaction with sulfur powder under an argon hydrogen atmosphere to obtain the molybdenum disulfide and double-carbon-layer co-modified stannous sulfide nanospheres. When the synthesized molybdenum disulfide and double-carbon-layer co-modified stannous sulfide nanospheres are used as the negative electrode material of a sodium ion battery, high electrochemical performance and high repeatability are shown, a guiding effect on the development of novel sodium-ion battery materials is achieved, and large-scale production and popularization can be realized easily.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
Preparation method for synthetizing three-dimensional stannous sulfide micro-flowers through complexing agent with aid of quaternary ammonium salt
InactiveCN103588241ASimple preparation processLow costTin compoundsQuaternary ammonium cationNitrogen gas
The invention discloses a preparation method for synthetizing three-dimensional stannous sulfide micro-flowers through a complexing agent with the aid of quaternary ammonium salt and belongs to the technical field of preparation of inorganic nano-materials. The method comprises the following steps: dissolving stannic chloride and the complexing agent into deionized water at a certain ratio while stirring to form a settled solution containing thiostannate radical complexing ions, then adding a shape and structure modifier and a sulfur source during stirring, and transferring the reaction system into a stainless-steel reaction kettle lined with polytetrafluoroethylene; placing the reaction kettle in a drying oven, performing hydrothermal reaction for a certain time at a certain temperature, then performing natural cooling to room temperature, rinsing obtained sediments with deionized water and absolute ethyl alcohol respectively, performing centrifugal separation, and performing drying in a vacuum drying oven; placing dried samples in a tube furnace, calcining the samples under nitrogen protection to obtain the stannous sulfide (SnS) micro-flowers. The synthetic method provided by the invention has the advantages of simple process, low cost and high yield; the synthetized stannous sulfide micro-flowers are relatively uniform in size and shape and have the average diameter of 5-18Mum.
Owner:ZHANJIANG NORMAL UNIV
Single-layer tin disulfide thin film and two-dimensional heterojunction and preparation method thereof
InactiveCN111106166ASmall sizeUniform thickness distributionSemiconductor devicesHeterojunctionThin membrane
The invention discloses a single-layer tin disulfide thin film and a two-dimensional heterojunction and a preparation method thereof. Stannous sulfide powder and sulfur powder are used as raw materials, a large-area single-layer tin disulfide semiconductor thin film is prepared and generated on a graphene substrate by using a chemical vapor deposition method, and a novel two-dimensional vertical heterostructure is constructed. The single-layer tin disulfide film prepared by the method is flat in structure and uniform in thickness, and the size can be effectively controlled by changing processconditions; the two-dimensional heterojunction is formed by the single-layer tin disulfide thin film and a graphene film with the single atomic layer thickness, so that the structural characteristicsof a material system can be improved, and the single-layer tin disulfide thin film can be applied to a micro-nano optoelectronic device.
Owner:XIAMEN UNIV
Stannous sulfide nanometer photo-thermal agent and preparation method thereof
ActiveCN108478793AExcellent photothermal performanceGood chemical stabilityTin compoundsEnergy modified materialsWater bathsTreatment field
The invention provides a stannous sulfide nanometer photo-thermal agent. The stannous sulfide nanometer photo-thermal agent comprises a stannous sulfide quantum dot, has obvious photo-thermal effects,high chemical stability and low toxicity, is prepared from abundant raw materials, has a low price, is prepared through simple processes and has a broad application prospect in the field of photo-thermal therapy. The invention also provides a preparation method of the stannous sulfide nanometer photo-thermal agent. The preparation method comprises grinding stannous sulfide blocks for 20 to 60 minutes, dispersing the powder in an organic solvent to obtain a dispersion liquid, carrying out ultrasound treatment on the dispersion liquid in a water bath at 5-10 DEG C for 8 to 12 hours to obtain the dispersion liquid subjected to ultrasonic treatment, centrifuging the dispersion liquid, collecting the precipitates and carrying out drying to obtain the stannous sulfide quantum dot. A preparationmethod of the stannous sulfide nanometer photo-thermal agent utilizes easily available raw materials, has simple processes and easily realizes large-scale production.
Owner:SHENZHEN UNIV
Stannous sulfide and indium sulfide thin film solar cell and preparation method thereof
InactiveCN105655421AImprove photoelectric conversion efficiencyWide range of choicesFinal product manufacturePhotovoltaic energy generationFilm resistanceLattice mismatch
The invention discloses a stannous sulfide and indium sulfide thin film solar cell and a preparation method thereof. The stannous sulfide and indium sulfide thin film solar cell sequentially comprises a base 1, a metal nanowire 2, an N type beta-indium sulfide window layer 3, a molybdenum disulfide buffer layer 4, a P type stannous sulfide absorption layer 5 and a metal electrode 6 from bottom to top. The stannous sulfide and indium sulfide thin film solar cell has the advantages that firstly characteristics of energy gaps of stannous sulfide, molybdenum disulfide and beta-indium sulfide are fully utilized, and stannous sulfide, molybdenum disulfide and beta-indium sulfide are respectively used as the absorption layer, buffer layer and window layer of the solar cell, so that full absorption of sunlight is benefited; secondly, the characteristic that stannous sulfide, molybdenum disulfide and beta-indium sulfide belong to sulfides is utilized, and lattice mismatching among stannous sulfide, and molybdenum disulfide and beta-indium sulfide is reduced, so that defect state density is reduced, recombination of photon-generated carriers is reduced, and transmission of the carriers is benefited; and thirdly, the metal nanowire is used for replacing the traditional conductive thin film, film resistance is greatly reduced, lateral collection of the carriers is benefited, and photoelectric conversion efficiency of the solar cell is greatly improved.
Owner:HUNAN NORMAL UNIVERSITY
A kind of sodium ion battery negative electrode sns/c composite material and preparation method thereof
ActiveCN106099069BSimple preparation processEasy to operateCell electrodesSecondary cellsCarbon layerNano structuring
The invention discloses a sodium-ion battery negative electrode SnS / C composite material and a preparation method thereof. The preparation method comprises the following steps: dissolving tin sulfide into a medium solution to obtain a solution I; adding an organic carbon source into the solution I and continuously stirring until the organic carbon source is uniformly dispersed, thereby obtaining a solution II; drying the solution II to obtain a solid powder precursor of the SnS / C composite material; roasting the solid powder precursor to obtain the porous SnS / C composite material. The tin sulfide in the composite material prepared by the preparation method has a nano structure with a controllable particle size, and a carbon layer coating the surface of the composite material is loose and porous, and is very beneficial for ion and electron transmission. According to the results, the composite material is used as a sodium-ion battery negative electrode material, has initial specific capacity of 620 mAh g<->1 under current density being 3A g<-1>, and has a specific capacity retention rate higher than 90% after 200 cycles. Compared with a conventional process for preparing stannous sulfide through thermal decomposition of tin sulfide, the preparation method has the advantages of being short in flow, simple in process, relatively low in energy consumption, high in controllable degree, easy for realizing large-scale production, and the like.
Owner:SOUTH CHINA UNIV OF TECH
A perovskite photovoltaic material with wide-range spectral absorption and its preparation method
ActiveCN105514277BIncrease contact areaImprove separation efficiencySolid-state devicesSemiconductor/solid-state device manufacturingChemical reactionComposite film
The invention discloses a wide-range spectral absorption perovskite photovoltaic material and a preparation method thereof. The method comprises: adding an additive to a perovskite reactant to form an inorganic particle hybrid perovskite precursor solution, and then The precursor solution is spin-coated on a substrate covered with an electron transport material, and a composite perovskite light-absorbing layer film is formed after heat treatment at 150° C.; wherein the additives include halides, carbon disulfide, zirconia nanoparticles, and n-hexylamine. Since the light-absorbing layer of the perovskite solar cell in this scheme uses nano-cuprous sulfide or stannous sulfide materials generated by chemical reactions and zirconia nanoparticles to co-dope the perovskite light-absorbing layer, the light-absorbing range of the perovskite layer is expanded. The battery efficiency is increased from 6% to more than 10%, and the method is simple and effective, and the cost is saved. Therefore, the method of the present invention for improving the performance of the light-absorbing layer of the perovskite solar cell has extremely high industrial application value.
Owner:ANHUI HUASUN ENERGY CO LTD
Preparation method for stannous sulfide/graphene compound photocatalyst
InactiveCN106563469AEnhanced light absorptionWide absorption spectrum rangePhysical/chemical process catalystsWater/sewage treatment by irradiationThioureaFiltration
The invention discloses a preparation method for a stannous sulfide / graphene compound photocatalyst. The preparation method includes the specific steps that 0.008-0.377 g of graphene oxide is added in 50 mL of ethanediol, is subjected to ultrasonic processing till being completely dispersed and is then magnetically stirred for 2 h; 1.127 g of SnCl2.2H2O is added in the solution mentioned above; then, 0.381 g of thiourea is added in the solution mentioned above under the magnetic stirring condition; magnetic stirring continues to be conducted for 2 h, and the mixed liquid is transferred in a polytetrafluoroethylene reaction kettle; hydrothermal reaction is conducted for 6 h at the temperature being 160 DEG C; the mixture is naturally cooled to the room temperature after the reaction is completed; filtration and separation are conducted; water washing is conducted three times, and ethyl alcohol washing is conducted three times; and then, drying is conducted, and the stannous sulfide / graphene compound photocatalyst is obtained. The prepared stannous sulfide / graphene compound photocatalyst can improve the light absorptivity, has the beneficial effects of being wide in absorption spectrum range, stable in performance, free of toxin, efficient, low in price, and the like, can be applied to degrading of organic pollutant which is difficult to biodegrade, and has high market application value.
Owner:HENAN NORMAL UNIV
Tin sulfide film solar battery
InactiveCN100587977CAbundant on EarthWide range of sourcesPhotovoltaic energy generationSemiconductor devicesHeterojunctionComposite film
A tin sulfide thin film solar cell comprises a conductive glass / metal gate electrode and a metal back electrode and is characterized in that uni-junction or multi-junction n-SnS2 or the composite thinfilm thereof and p-SnS or the composite thin film thereof are formed between the conductive glass / metal gate electrode and the metal back contact. The composite means the tin sulfide obtained by doping tin bromide (n-SnS2) and stannous sulfide (p-SnS). The solar cell is rich in material sources, safe and environment-friendly, convenient in processing and effectively solves the collection problemof current carriers with the aid of such electrodes as metallic tin by using SnS2 and SnS, which have the same components and different conduction types and liable to realize energy gap match, heterojunction transition and good transport property of the current carriers.
Owner:HEFEI UNIV OF TECH
Method for preparing nano stannous sulfide from tin-containing electronic waste by one-step method
ActiveCN112391533ARealize secondary useAchieve sustainable developmentTin compoundsNanotechnologyCalcium sulphidePhysical chemistry
The invention discloses a method for preparing nano stannous sulfide from tin-containing electronic waste by a one-step method. The method comprises the following steps that the tin-containing electronic waste and an additive composed of calcium sulfide and silicon dioxide are uniformly mixed and then are subjected to agglomeration, agglomerates are placed in a reducing atmosphere to be subjectedto reduction roasting at 750 DEG C-900 DEG C, roasted volatile matters enter a weak reducing atmosphere to be subjected to reduction roasting at 450 DEG C-700 DEG C, and nano stannous sulfide powder is obtained. According to the method, the tin-containing electronic waste serves as the raw material, tin is efficiently recycled, the high-purity nano stannous sulfide powder material is prepared, waste utilization is achieved, the economic additional value is high, and the method is easy to operate, low in production cost, environmentally friendly and capable of meeting the industrial productionrequirement.
Owner:CENT SOUTH UNIV
One-step method for preparing nano-tin sulfide from tin-containing electronic waste
ActiveCN112391533BRealize secondary useAchieve sustainable developmentTin compoundsNanotechnologySulfidationReducing atmosphere
The invention discloses a method for preparing nano-stannous sulfide from tin-containing electronic waste in one step. The method is to mix the tin-containing electronic waste with an additive composed of calcium sulfide and silicon dioxide to make agglomerates, and place the Reduction roasting is carried out at 750-900°C in a neutral atmosphere, and the roasted volatiles enter a weakly reducing atmosphere for reduction roasting at 450-700°C to obtain nano-stannous sulfide powder. The method uses tin-containing electronic waste as a raw material to efficiently recover tin and prepare a high-purity nano-tin sulfide powder material, which not only realizes waste utilization, but also has high economic added value, and the method is simple to operate, low in production cost, and environmentally friendly. Meet the requirements of industrial production.
Owner:CENT SOUTH UNIV
A drug delivery system based on stannous sulfide nanosheets and its preparation method
ActiveCN108114280BHigh clinical application valueLow carrier costOrganic active ingredientsEnergy modified materialsMedicineChemotherapeutic drugs
Owner:SHENZHEN UNIV
Synthesis method of a kind of graphitic carbon nitride/stannous sulfide nano-heterojunction
ActiveCN107233910BWidely used valueHigh purityPhysical/chemical process catalystsHeterojunctionSynthesis methods
The present invention relates to a kind of graphitic carbon nitride / tin sulfide (g-C 3 N 4 / SnS) nano-heterojunction synthesis method, comprising the following steps: 1) taking a certain amount of urea and putting it into a corundum crucible; 2) putting the corundum crucible filled with urea into a muffle furnace for calcination at a certain temperature, Get g‑C 3 N 4 ; 3) Weigh a certain amount of SnCl 2 2H 2 Dissolve O in deionized water, stir well and add a certain amount of g‑C 3 N 4 , continue to stir; 4) Weigh a certain amount of Na 2 S·9H 2 O dissolved in deionized water and added dropwise to g‑C 3 N 4 and SnCl 2 5) obtain the final product after separation, washing and drying. The synthesis technique of the present invention is simple, and g-C 3 N 4 In situ growth of SnS nanoparticles on nanosheets, the g‑C 3 N 4 / SnS nano-heterojunction has the characteristics of mesoporous structure and large specific surface area (80‑90m 2 / g), has excellent photocatalytic performance under visible light conditions.
Owner:LUOYANG INST OF SCI & TECH
A kind of stannous sulfide carbon composite material and its preparation method and application
ActiveCN113880130BLow priceImprove conductivityTin compoundsSecondary cellsOXALIC ACID DIHYDRATECarbon composites
The invention discloses a stannous sulfide carbon composite material, a preparation method and application thereof. The preparation method of the present invention adopts tin tetrachloride as a tin source, sucrose as a carbon source, cetyltrimethylammonium bromide and polyvinylpyrrolidone as active agents, oxalic acid as a template, and prepares tin dioxide carbon in a hydrothermal environment. The composite material is further reacted at high temperature in a tube furnace to form a tin-carbon composite material, and the tin-carbon composite material is further mixed with sulfur, and then calcined under the protection of an inert atmosphere to obtain a stannous sulfide-carbon composite material. The raw material price of the present invention is low, and the composite material structure is composed of primary nanoparticles to form secondary microparticles, which can shorten the diffusion path of sodium ions in the material by using primary nanoparticles. In addition, the carbon skeleton composed of secondary microparticles has a porous structure. On the one hand It can not only improve the conductivity of the stannous sulfide, but also effectively inhibit the volume change in the electrochemical reaction of the stannous sulfide, and maintain the structural stability of the electrode.
Owner:中博龙辉装备集团股份有限公司
Copper-zinc-tin-sulfur quaternary compound and thin-film solar cell composed of the same and preparation method thereof
InactiveCN101794826BRich sourcesThe stoichiometric ratio is easy to control and adjustableFinal product manufactureSemiconductor devicesHigh pressureCopper sulfide
The invention discloses a copper-zinc-tin-sulfur quaternary compound, a thin film solar cell formed by the same, and a preparation method thereof. The thin film solar cell comprises a conductive glass / metal gate electrode and a metal backing electrode, and is characterized in that: a p-copper-zinc-tin-sulfur quaternary compound thin film and an n-stannic sulfide thin film which form a p-n structure are arranged between the conductive glass / metal gate electrode and the metal backing electrode. The preparation method for the copper-zinc-tin-sulfur quaternary compound comprises the following steps: mixing copper sulfide, zinc sulfide and stannous sulfide in a mole ratio of 1:0.2-0.8:0.2-0.8; adding the mixture into an appropriate amount of water and performing ball grinding for more than 1 hour; transferring the obtained mixed liquid to a high-pressure autoclave; and performing hydro-thermal treatment for more than 2 hours at the temperature of between 120 and 280 DEG C to obtain copper-zinc-tin-sulfur quaternary compound powder. The thin film solar cell prepared by the invention has the advantages of strong adhesive force, low resistance and rich raw material sources; and the preparation method has the advantages of simple preparation process, low cost and environmental friendliness.
Owner:HEFEI UNIV OF TECH
Stannous sulfide and magnesium-doped zinc oxide thin film solar cell and preparation method thereof
InactiveCN105576052ASimple structureHigh yieldFinal product manufactureSemiconductor devicesMagnesium dopingFully developed
The invention discloses a stannous sulfide and magnesium-doped zinc oxide thin film solar cell and a preparation method thereof. The preparation method comprises the following steps of firstly taking a transparent conductive substrate, and sequentially depositing n-type magnesium-doped zinc oxide thin film lamination layers with different magnesium doping concentrations on the transparent conductive substrate by a magnetron sputtering method or an ultrasonic spraying method; secondly, depositing a p-type stannous sulfide thin film on the n-type magnesium-doped zinc oxide thin film lamination layers by a plasma enhanced chemical vapor deposition method, evaporating a layer of aluminum film on the p-type stannous sulfide thin film, and preparing the aluminum film into a porous aluminum oxide thin film by an electrochemical anodic oxidation method; and finally, respectively leading metal electrodes out of the p-type stannous sulfide thin film and the transparent conductive substrate by a silk screen printing method or by laser grooving. The preparation method has the advantages that the response range of a traditional stannous sulfide thin film solar cell to spectrum is expanded, the light scattering resistant capability of the porous aluminum oxide thin film is also fully developed, and the full-spectrum absorption rate and the photoelectric conversion efficiency of the solar cell are improved.
Owner:HUNAN NORMAL UNIVERSITY
A kind of stannous sulfide nano photothermal agent and preparation method thereof
Disclosed is a stannous sulfide nanometer photo-thermal agent, comprising stannous sulfide quantum dots. The preparation method therefor comprises: grinding a stannous sulfide block for 20-60 minutes, and then dispersing same in an organic solvent to obtain a dispersion; sonicating the dispersion in a water bath at 5ºC-10ºC for 8-12 hours so as to obtain a sonicated dispersion; and centrifuging the sonicated dispersion, and then collecting a precipitate and drying same to obtain stannous sulfide quantum dots. The stannous sulfide nanometer photo-thermal agent has a distinct photo-thermal effect, a high chemical stability and a low toxicity; the raw materials thereof are abundant, the price thereof is cheap, and the preparation method therefor is simple; and same has a broad application prospect in the field of photo-thermal therapy. The preparation method uses raw materials which are easy to obtain, has a sample preparation process, and easily achieves large-scale production.
Owner:SHENZHEN UNIV
A kind of preparation method of near-infrared stannous sulfide nanoparticles
ActiveCN108821332BReduce in quantityGood monodispersityTin compoundsNanotechnologyPhenanthrolineTin(II) sulfide
The invention discloses a preparation method of near-infrared stannous sulfide nano-particles. According to the method, phenanthroline tin is adopted as a tin resource, dimethyl disulfide is adopted as a sulfur resource, and in a surface modification agent, the stannous sulfide nano-particles with near-infrared fluorescence are prepared in one step. According to the preparation method of the near-infrared stannous sulfide nano-particles, the operation step is simple, the adopted agents are few, the cost is low, and implementation is easy; the whole preparation process meets the requirements ofgreen chemistry and is safe and environmentally friendly; the prepared stannous sulfide nano-particles have the advantages of being good in monodispersity, high in near-infrared fluorescence intensity, good in stability and the like.
Owner:苏州影睿光学科技有限公司
Preparation method, product and application of a two-dimensional ultrathin stannous sulfide nanosheet
ActiveCN109179489BLow costProduct quality is easy to controlMaterial nanotechnologyTin compoundsElectrolytic agentTin(II) sulfide
Owner:HANGZHOU NANOGEL NEW MATERIAL
A kind of preparation method of tin sulfide composite negative electrode material
ActiveCN110844933BImprove cycle lifeReduce manufacturing costTin compoundsCell electrodesSulfidationTin(II) sulfide
Owner:ENERGY RESOURCES INST HEBEI ACADEMY OF SCI
The preparation method of stannous sulfide nano sheet
InactiveCN105016378BSimple methodRapid responseMaterial nanotechnologyTin compoundsTin(II) sulfideMaterials science
The invention discloses a preparation method of a tin sulfide nanosheet. The preparation method comprises the following steps: uniformly mixing tin powder with sulfur powder in a mole ratio of 1 to 1 and pressing the mixed powder to form a press cake with density of 4-5g / cm<3>; putting the press cake in a graphite pot and putting the graphite pot in a copper pot anode in a reaction chamber of a direct-current arc discharge device, wherein a tungsten bar cathode and the copper pot anode are placed oppositely; filling argon after vacuumizing the reaction chamber and filling a copper pot with circulating cooling water, wherein the pressure of argon is 5-30kPa; in the discharge process, maintaining the voltage at 20-40V and the current at 80-120A and reacting for 3-5 minutes; then carrying out passivation for 6-8 hours in an argon environment and collecting black powder in the graphite pot, thus obtaining the tin sulfide nanosheet. The preparation method has the advantages of simple preparation process, high yield and high sample purity.
Owner:BOHAI UNIV
Tin sulfide/gold nanoparticle composite and its preparation method and application
ActiveCN107414073BHigh crystallinityImprove performanceMaterial nanotechnologyTransportation and packagingPhotovoltaic detectorsNanoparticle Complex
The invention discloses a stannous sulfide / gold nanoparticle composite and its preparation method and application. The preparation method is: mechanically stripping the stannous sulfide material, the thickness of the product is 50-100 nm, the size is several microns to more than ten microns, and the Standby after annealing; drop chloroauric acid aqueous solution onto the surface of mechanically stripped tin sulfide, deposit for 2‑5 min, blow off excess liquid with nitrogen, and react for 2‑5 at 120‑150 °C; after the reaction, quickly take out the sample, The obtained gold nanoparticles are assembled in the self-orientation of stannous sulfide, and the obtained gold nanoparticles have a size of tens of nanometers and good crystallinity, and have broad and important application prospects in the fields of photodetection devices, biosensing and the like.
Owner:NANJING UNIV OF POSTS & TELECOMM
A kind of method of low temperature liquid phase synthesis stannous sulfide
The invention provides a method for synthesizing stannous sulfide in a low-temperature liquid phase, which comprises the following steps: firstly, adding deionized water into polyvinylpyrrolidone, stirring and dissolving to obtain a polyvinylpyrrolidone solution. Next, weigh the sulfur source, anhydrous SnCl 2 , add dropwise hydrazine hydrate and ammonia water and stir. The sulfur source includes one of high-purity sulfur and thiourea. The polyvinylpyrrolidone solution was then added to the solution prepared in the previous step and placed in a reaction vessel to obtain a solid-liquid mixture, which was then put into a vacuum oven for reaction at a reaction temperature of 50° C. and a reaction time of 24 hours. Finally, the reaction vessel was taken out, the solid-liquid mixture was cooled and placed in a centrifuge tube, washed and centrifuged alternately with deionized water and absolute ethanol to obtain SnS crystal grains.
Owner:INST OF NEW MATERIALS & IND TECH WENZHOU UNIV
A preparation method for synthesizing three-dimensional stannous sulfide microflowers with quaternary ammonium salt auxiliary complexing agent
InactiveCN103588241BSimple preparation processLow costTin compoundsQuaternary ammonium cationSynthesis methods
The invention discloses a preparation method for synthesizing three-dimensional stannous sulfide micro-flowers with a quaternary ammonium salt auxiliary complexing agent, which belongs to the technical field of inorganic nanomaterial preparation; the step is to mix tin tetrachloride and complexing agent in a certain proportion under stirring Dissolve in deionized water to form a clear solution containing thiostannate complex ions, then add morphology and structure modifiers and sulfur sources under stirring, and transfer the reaction system to a stainless steel reactor lined with polytetrafluoroethylene placed in a drying oven, hydrothermally reacted at a certain temperature for a certain period of time, then naturally cooled to room temperature, rinsed the obtained precipitate with deionized water and absolute ethanol, centrifuged, and dried in a vacuum drying oven; after drying The sample is placed in a tube furnace, and calcined under nitrogen protection to obtain tin sulfide (SnS) micron flowers; the synthetic method of the present invention has the advantages of simple technique, low cost, and high yield, and the synthetic stannous sulfide The size and shape of micron flowers are relatively uniform, with an average diameter of 5 μm to 18 μm.
Owner:ZHANJIANG NORMAL UNIV
A kind of preparation method of stannous sulfide
The invention discloses a preparation method of stannous sulfide. The preparation method comprises the following steps: uniformly mixing metallic tin powder with sublimate powdered sulfur, adding mixed powder into an atmosphere reaction furnace with the temperature of 650 DEG C-1000 DEG C and performing a quick reaction on tin and sulfur to obtain liquid tin sulfide; controlling the furnace temperature at 650 DEG C-1000 DEG C, continuously preserving the temperature for 0.5-4h, distilling to remove redundant sulfur in the tin sulfide product and cooling to obtain the high-purity stannous sulfide. The method is simple in process, low in cost, high in synthesis speed of the product, high in product yield and high in purity; less waste residues and waste gas are generated, and the productionprocess is green and environmentally-friendly, therefore, the method has a relatively good industrial application prospect.
Owner:云南锡业集团(控股)有限责任公司研发中心
Stannous sulfide/gold nanoparticle compound and preparation method and application thereof
ActiveCN107414073AHigh crystallinityImprove performanceMaterial nanotechnologyTransportation and packagingPhotovoltaic detectorsArgon atmosphere
The invention discloses a stannous sulfide / gold nanoparticle compound and a preparation method and application thereof. The preparation method comprises the steps that a stannous sulfide material is subjected to mechanical exfoliation to obtain a product, the thickness of the product is 50-100 nm, the size of the product is from a few micrometers to a dozen of nanometers, and the product is annealed under an argon atmosphere for standby application; a chloroauric acid water solution is added on the surface of the stannous sulfide material subjected to mechanical exfoliation drop by drop, precipitation is conducted for 2-5 min, needless liquid is blown away by nitrogen, and reaction is conducted for 2-5 min at the temperature of 120-150 DEG C; and after reaction is completed, a sample is taken out quickly, gold nanoparticles are obtained and assembled on the stannous sulfide in an automatic orientation mode, the size of the gold nanoparticles is dozens of micrometers, and the crystallinity is good. The stannous sulfide / gold nanoparticle compound has wide and important application prospects in the fields of photoelectric detection devices, biosensing and the like.
Owner:NANJING UNIV OF POSTS & TELECOMM
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