Hydrate inhibitor polymer and preparation method
A hydrate inhibitor and polymer technology, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve the problems of high cost, and achieve the effects of improving temperature resistance, strong adsorption, and simple and feasible preparation methods
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[0017] Example 1 Preparation method of EM / ACD / DMDAAC / NVP polymer
[0018] Take 3.8mL of 0.5g / mL dimethyldiallylammonium chloride (DMDAAC) aqueous solution in a 150mL beaker, accurately add 1.2g of ethyl methacrylate (EM) under magnetic stirring, and then stir at high speed for 10-20min Make it a lotion.
[0019] The above emulsion and 5 mL of NVP aqueous solution with a concentration of 0.5 g / mL were added to 50 mL of an allyl β-cyclodextrin (ACD) aqueous solution with a concentration of 0.01 g / mL. Then, 0.6g disodium ethylenediaminetetraacetic acid (EDTA) chelating agent, 0.6g potassium persulfate oxidizing agent and 0.6g sodium bisulfite reducing agent were added in sequence. Fully stir and mix on a magnetic stirrer, then fill with nitrogen for 40 minutes to remove oxygen, and react at 50°C for 9 hours to obtain EM / ACD / DMDAAC / NVP quaternary polymer.
[0020] Determine the intrinsic viscosity of the EM / ACD / DMDAAC / NVP polymer according to the standard described in GB12005.1-89, and...
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[0021] Example 2 The inhibitory effect of EM / ACD / DMDAAC / NVP polymer in drilling fluid hydrate
[0022] In order to evaluate the inhibitory effect of EM / ACD / DMDAAC / NVP polymers on hydrates in drilling fluids, a visual high-pressure fluid testing system was used. The system consists of an autoclave with sapphire double windows, a constant temperature bath, a temperature control system, a pressure control system and a measurement system.
[0023] Although the formation of hydrate can be observed through a window, the present invention uses sudden changes in pressure and temperature in the kettle to judge. Because the hydrate formation reaction is exothermic, the temperature will rise and the pressure will drop significantly. The experimentally determined hydrate formation time is the time from when gas is introduced into the kettle and the pressure is constant at 16Mpa to the point of pressure drop.
[0024] The polymer evaluation of the present invention is carried out separately in ...
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