Camellia nitidissima tea polyphenols slow release microsphere particle and production method thereof
A technology for slow-release microspheres and camellia tea, which is applied in pharmaceutical formulations, medical preparations with non-active ingredients, plant raw materials, etc., can solve the problems of structural damage, oxidation, polymerization, condensation, poor fat solubility, etc., to reduce damage. , Improve the effect of active maintenance and large loss of active ingredients
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Embodiment 1
[0046] Remove impurities, rotten and diseased yellow leaves from the Jinhua tea leaves that have been picked for no more than 24 hours, clean them and cut them into small leaflets with a width of 1 to 2 cm, add 5 times the water and 0.05% of the weight of the feed liquid compound fruit pulp enzyme (Qingdao The KDN-F01 pulp enzyme produced by Kangdien Biotechnology Co., Ltd., the main component: mainly acid pectinase, containing hemicellulase such as xylanase and β-glucanase.), stirring and heating to 40 ℃, after keeping the temperature for 2 hours, quickly heat to 100 ℃ to inactivate the enzyme for 10 minutes. Then add pure water 5 times the weight of fresh leaves. When the temperature of the feed liquid reaches about 60°C, use an ultrasonic traditional Chinese medicine extraction unit (TCD-1000) to carry out vibration extraction. The extraction time is 65 minutes and the frequency is 25kHz. After the first ultrasonic oscillation is finished, filter, and then add 10 times of p...
Embodiment 2
[0048] Remove impurities, rotten and diseased yellow leaves from the golden camellia tea leaves that have been picked for no more than 24 hours, clean them, cut them into 1-2 cm wide leaflets, add 5 times the water to make a pulp. Heat the slurry obtained by beating to 40°C, add 0.05% pectinase (the NCB-PE200 compound pulp enzyme produced by Hunan Youtel Biochemical Co., Ltd., mainly composed of pectinase and cellulase) , and contains a certain amount of hemicellulase and β-glucanase.), after stirring at constant temperature for 2 hours, quickly heat to 100°C to inactivate the enzyme for 10 minutes. Then add pure water 5 times the weight of fresh leaves. When the temperature of the feed liquid reaches about 65°C, use an ultrasonic traditional Chinese medicine extraction unit (TCD-1000) to carry out vibration extraction. The extraction time is 60 minutes and the frequency is 50kHz. Filter after the first ultrasonic vibration leaching is finished, and then add 10 times of pure w...
Embodiment 3
[0050]Remove impurities, rotten and diseased yellow leaves from fresh golden camellia leaves that have been picked for no more than 24 hours, clean them and cut them into 1-2 cm wide leaflets, add 5 times the amount of water and 0.05% pectinase (Qingdao KDN-FO1 pulp enzyme produced by Kangdien Biotechnology Co., Ltd.). Stir and heat to 40°C, keep the temperature for 2 hours, then rapidly heat to 100°C to inactivate the enzyme for 10 minutes. Then add pure water 5 times the weight of fresh leaves. When the temperature of the feed liquid reaches about 70°C, use an ultrasonic traditional Chinese medicine extraction unit (TCD-1000) to carry out vibration extraction. The extraction time is 70 minutes and the frequency is 70kHz. Filter after the first ultrasonic vibration leaching is finished, and then add 10 times of pure water to the residue to carry out the second ultrasonic vibration leaching (leaching conditions are the same as the first time). Filter the extract through a 120...
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