Doping dye sensitized solar cell photo anode, preparation method and application thereof
A technology of solar cells and dye sensitization, applied in the field of solar cells, can solve the problems of unsatisfactory complexity and product performance, and achieve the effects of improving photoelectric conversion performance, suppressing dark current and good repeatability
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[0037] Example 1:
[0038] a. Preparation of doped SiO 2 TiO 2 Slurry:
[0039] Take 5g of P25 powder and add SiO 2 With TiO 2 Mix well, SiO 2 The quality is TiO 2 Add 1 mL of acetic acid to 2.5% of the mass in turn, add 5 mL of deionized water in 5 times of 1 mL each time, add 15 mL of absolute ethanol in 15 times of 1 mL each time, and add 15 mL of absolute ethanol in 6 times of 2.5 mL each time. Add anhydrous ethanol and stir for 3 minutes each time; then add 100 mL of anhydrous ethanol to obtain a slurry; stir the slurry magnetically for 10 minutes at a stirring speed of 300 revolutions / minute; then disperse by ultrasonic for 60 minutes; then add 20 g Terpineol, repeat the magnetic stirring and ultrasonic dispersion; then add 3g ethyl cellulose and 30g absolute ethanol to repeat the magnetic stirring and ultrasonic dispersion; finally in the rotary evaporator at 40 ℃ for 6 hours rotary distillation to obtain the screen printing Slurry, referred to as slurry B.
[0040] b. Prepa...
Example Embodiment
[0045] Example 2:
[0046] The preparation method of this embodiment is the same as that of embodiment 1, the difference is SiO 2 The addition amount is TiO 2 5% by mass, the paste that can be used for screen printing obtained in step a is denoted as paste C.
Example Embodiment
[0047] Example 3:
[0048] The preparation method of this embodiment is the same as that of embodiment 1, the difference is SiO 2 The addition amount is TiO 2 7.5% of the mass, the paste that can be used for screen printing obtained in step a is denoted as paste D.
[0049] The printed four-layer SiO obtained by scanning electron microscope (FE-SEM) analysis on the surface and section of the composite film 2 / TiO 2 The thickness of the slurry after sintering is about 17.9 μm. by Figure 4 , 5 It can be seen that the composite film is smooth, the nanoparticles are uniformly distributed, and form a network structure connected to each other. In the larger particles (TiO 2 ) Has a relatively small distribution (for SiO 2 ), this small particle not only adds TiO 2 The effective connection between particles also makes TiO 2 The bond with conductive glass is stronger.
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