Medical anti-microbial silver-plated dressing and preparation method thereof
A medical and coating technology, applied in applications, clothing, underwear, etc., can solve the problems of large amount of silver-plated fibers, complicated processing technology, and difficult processing, so as to reduce the amount of silver used, reduce costs, and improve antibacterial efficiency and utilization rate Effect
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Embodiment 1
[0023] Embodiment 1, preparation antibacterial silver-plated medical dressing
[0024] (1) Mix calcium alginate loose fibers and cotton fiber loose fibers at a mass ratio of 20:80, carding and acupuncture to prepare a dressing base material.
[0025] (2) immerse the formed dressing base material in mass concentration in 5% sodium hydroxide solution (the solid-liquid ratio of dressing base material and sodium hydroxide solution is 1kg: 1L), remove fiber surface oil agent; Then water ( The ratio of solid to liquid is 1kg: 3L), absolute ethanol (ratio of solid to liquid is 1kg: 1L) for rinsing, to wash off the sodium hydroxide and oil agent remaining in the dressing base material and dehydrate, after drying, put it in a vacuum in a magnetron sputtering device.
[0026] (3) The sputtering chamber in the magnetron sputtering device is evacuated to make the vacuum degree less than 2×10 -4 Pa, and filled with pure argon as the sputtering gas; pure silver is used as the magnetron sp...
Embodiment 2
[0030] Embodiment 2, prepare antibacterial silver-plated medical dressing
[0031] (1) Using carding equipment, the calcium alginate loose fibers are carded into a web, spread flat on the surface of the viscose fiber spunlace non-woven fabric, and are prepared into a dressing base material by acupuncture compounding using an acupuncture equipment; wherein, alginate The mass ratio of the calcium powder fiber to the viscose fiber spunlace nonwoven fabric is 10:90.
[0032] Steps (2), (3), and (4) are the same as in Example 1; there are the following changes in its process parameters: vacuuming ensures that the vacuum degree in the sputtering chamber is 6.0 × 10 -4 Pa; the substrate temperature is room temperature; the working gas argon is introduced to ensure that the pressure during sputtering is 5Pa; the target material is silver-copper alloy, and the silver content is 50%, and the distance between the substrate and the target is adjusted to 170mm , the sputtering power is 50...
Embodiment 3
[0035] Embodiment 3, prepare antibacterial silver-plated medical dressing
[0036] (1) Using carding equipment, the calcium alginate loose fiber is carded into a web, and spread on the surface of the cotton fiber fabric with the specification parameters: 13tex×13tex×185 (root / 10cm)×210 (root / 10cm). Pricking equipment is used for needle punching and compounding to prepare dressing base materials; wherein, the mass ratio of calcium alginate loose fibers to cotton fiber fabrics is 90:10.
[0037] Steps (2), (3), and (4) are the same as in Example 1; there are the following changes in its process parameters: vacuuming ensures that the vacuum degree in the sputtering chamber is 3.0 × 10 -4 Pa; the temperature of the substrate is room temperature; the working gas argon is introduced to ensure that the pressure during sputtering is 2Pa; the target material is pure silver, the distance between the substrate and the target is adjusted to 100mm, and the sputtering power is 40W. Time 1....
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