Seaweed oligosaccharide synergistic urea and preparation method thereof
A technology of seaweed oligosaccharides and urea, which is applied in the direction of urea compound fertilizer, nitrogen fertilizer, fertilizer mixture, etc., can solve the problems of polluting the living environment, increasing production costs, and having no fertilizer effect, so as to improve the soil environment, improve safety, and improve immunity effect of ability
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Embodiment 1
[0014] Example 1 Preparation of algal oligosaccharide synergistic urea with alginic acid
[0015] Put alginic acid dry powder in a pressure vessel, add tap water to make the mass volume percentage of alginic acid reach 0.01-20.0%, stir, then add hydrogen peroxide with a mass volume percentage of 0.005-20.0%, stir, heat up to 121°C, and keep warm for 3 hours, then lower the temperature to 80°C, stir, adjust the pH to 6.5-9.0 with alkali, and concentrate to obtain a seaweed oligosaccharide solution. Then take a quantitative amount of seaweed oligosaccharide solution and add it to the urea aqueous solution in the conventional urea synthesis process, and then evaporate and granulate to obtain seaweed oligosaccharide synergistic urea.
[0016] The purpose of adding tap water is to allow the dry alginic acid powder to absorb water and expand, so that it can pass through the H of alginic acid (HALg) itself at high temperature. + Cut off the glycosidic bond, so that the seaweed polys...
Embodiment 2
[0018] Example 2 Preparation of seaweed oligosaccharide synergistic urea with potassium alginate
[0019] Put the dry powder of potassium alginate in a pressure vessel, add tap water to make the mass percentage of potassium alginate reach 0.01-20.0%, stir and dissolve, add hydrochloric acid or sulfuric acid with a mass percentage of 0.01-10.0%, and then add a mass percentage of 0.005- 20.0% hydrogen peroxide, stir, heat up to 121°C, keep warm for 3 hours, then cool down to 80°C, stir, adjust pH to 6.5-9.0 with alkali, and concentrate to obtain seaweed oligosaccharide solution. Then take a quantitative amount of seaweed oligosaccharide solution and add it to the urine in the conventional process of synthesizing urea, and then evaporate and granulate to obtain the seaweed oligosaccharide synergistic urea.
[0020] Weigh 10kg of potassium alginate dry powder, add 200kg of tap water, stir, add 2.0kg of sulfuric acid with a purity of 98%, then add 4.0kg of hydrogen peroxide with a ...
Embodiment 3
[0022] Example 3 Prepare seaweed oligosaccharide synergistic urea with kelp
[0023] Put the dried kelp into a pressure vessel, add tap water to make the seaweed polysaccharide in the kelp reach a mass percentage of 0.01-20.0%, stir, add hydrochloric acid or sulfuric acid with a mass percentage of 0.01-10.0%, and then add a mass percentage of 0.005- 20.0% hydrogen peroxide, stir, heat up to 121°C, keep warm for 3 hours, then cool down to 80°C, stir, filter, adjust the pH of the filtrate to 6.5-9.0 with alkali, and concentrate to obtain a seaweed oligosaccharide solution. Then take a quantitative amount of seaweed oligosaccharide solution and add it to the urine in the conventional process of synthesizing urea, and then evaporate and granulate to obtain the seaweed oligosaccharide synergistic urea.
[0024] Weigh 100kg of dried kelp and crush it, add 800kg of tap water, stir, add 9.0kg of sulfuric acid with a purity of 98%, then add 18.0kg of hydrogen peroxide with a purity of ...
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