Ultraviolet cross-linked organosilicone modified acrylate copolymer emulsion
A technology of acrylate and ultraviolet light, applied in the direction of coating, etc., can solve the problems of low slipperiness and anti-adhesiveness
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[0045] Example 1
[0046] 4-(2-hydroxy-3-allyloxy-propoxy) benzophenone 10 parts, vinyl triethoxy silane 10 parts, methyl methacrylate 19 parts, methyl acrylate 5 parts, acrylic acid 25 parts of butyl ester, 17 parts of isobutyl methacrylate, 8 parts of isobornyl acrylate, 3 parts of isooctyl methacrylate, 1 part of maleic acid and 2 parts of acrylic acid were used as monomer compositions. Among them, 4-(2-hydroxy-3-allyloxy-propoxy) benzophenone is a UV-active monofunctional monomer, and vinyl triethoxysilane is an alkoxysiloxane monofunctional Degree monomer, the others are the third monofunctional monomer.
[0047] A preparation method of UV-crosslinked silicone modified acrylate copolymer emulsion, the steps are:
[0048] (1) Put 100 parts of the above-mentioned monomer composition, 2 parts of nonylphenol polyoxyethylene ether sulfate ammonium salt, 1.5 parts of octylphenol polyoxyethylene ether and 20 parts of distilled water into the mixer, temperature control device, and con...
Example Embodiment
[0055] Example 2
[0056] 5 parts of 4-acryloxy benzophenone, 10 parts of methacryloxy propyl trimethoxysilane, 10 parts of methyl acrylate, 15 parts of methyl methacrylate, 5 parts of styrene, methacrylic acid 5 parts of isobutyl ester, 30 parts of n-butyl acrylate, 10 parts of isooctyl acrylate, 5 parts of octadecyl acrylate, 3 parts of 2-hydroxyethyl acrylate and 2 parts of methacrylic acid were used as monomer compositions. Among them, 4-acryloxybenzophenone is a UV-active monofunctional monomer, methacryloxypropyltrimethoxysilane is an alkoxysiloxane monofunctional monomer, and the others are the first Three monofunctional monomers.
[0057] A preparation method of UV-crosslinked silicone modified acrylate copolymer emulsion, the steps are:
[0058] (1) Put 100 parts of the above monomer composition, 1.5 parts of sodium lauryl sulfate, 3.5 parts of octylphenol polyoxyethylene ether and 20 parts of deionized water into a stirrer, a temperature control device, a condenser, and a...
Example Embodiment
[0065] Example 3
[0066] 2 parts of 4-(2-hydroxy-3-allyloxy-propoxy) benzophenone, 15 parts of methacryloxypropyltrimethoxysilane, 18 parts of styrene, 3 parts of n-propyl acrylate Parts, 32 parts of n-butyl acrylate, 5 parts of n-butyl methacrylate, 10 parts of isooctyl methacrylate, 10 parts of isodecyl acrylate, 2 parts of acrylamide and 3 parts of acrylic acid as monomer compositions. Among them, methacryloxypropyltrimethoxysilane is a UV-active monofunctional monomer, methacryloxypropyltrimethoxysilane is an alkoxysiloxane monofunctional monomer, and others It is the third monofunctional monomer.
[0067] A preparation method of UV-crosslinked silicone modified acrylate copolymer emulsion, the steps are:
[0068] (1) Put 100 parts of the above monomer composition, 2 parts of octylphenol polyoxyethylene ether and 15 parts of deionized water into a reactor equipped with a stirrer, a temperature control device, a condensation device, a dripping device and a thermometer. Stir at...
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